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5.1 The purpose of this practice is to evaluate the homogeneity of a lot of material selected as a candidate for development as a reference material or certified reference material, or for a L/B selected for some other purpose (see Appendix X1 – Appendix X4 for examples).5.2 This practice is applicable to the testing of samples taken at various stages during production. For example, continuous cast materials, ingots, rolled bars, wire, etc., could be sampled at various stages during the production process and tested.1.1 This practice is suitable for testing the homogeneity of a metal lot or batch (L/B) in solid form by spark atomic emission spectrometry (Spark-AES). It is compliant with ISO Guide 35—Certification of Reference Materials: General and Statistical Principles. It is primarily intended for use in the development of reference materials but may be used in any other application where a L/B is to be tested for homogeneity. It is designed to provide a combined study of within-unit and between-unit homogeneity of such a L/B.1.2 This practice is designed primarily to test for elemental homogeneity of a metal L/B by Spark-AES. However, it can be adapted for use with other instrumental techniques such as X-ray fluorescence spectrometry (XRF) or atomic absorption spectrometry (AAS).Note 1—This practice is not limited to elemental analysis or techniques. This practice can be applied to any property that can be measured, for example, the property of hardness as measured by the Rockwell technique.1.3 The criteria for acceptance of the test specimens must be previously determined. That is, the maximum acceptable level of heterogeneity must be determined on the basis of the intended use of the L/B.1.4 It is assumed that the analyst is trained in Spark-AES techniques including the specimen preparation procedures needed to make specimens ready for measurements. It is further assumed that the analyst is versed in and has access to computer-based data capture and analysis. The methodology of this practice is best utilized in a computer based spreadsheet.1.5 This practice can be applied to one or more elements in a specimen provided the signal-to-background ratio is not a limiting factor.1.6 This practice includes methods to correct for systematic drift of the instrument with time. (Warning—If drift occurs, erroneous conclusions will be obtained from the data analysis.)1.7 This practice also includes methods to refine estimates of composition and uncertainty through the use of a type standard or multiple calibrants.1.8 It further provides a means of reducing a nonhomogeneous set to a homogeneous subset.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This practice covers the form and style for specifications under the jurisdiction of ASTM Subcommittee B02.07 Refined Nickel and Cobalt and Their Alloys. Anyone preparing new or revising existing specifications for this subcommittee shall follow the practices and procedures outlined herein.1.2 This practice is a supplement to the current edition of Form and Style for ASTM Standards (Form Manual)2. If there is a conflict between the documents, then this should be brought to the attention of B02.07. Until the conflict is resolved, the more stringent requirement of the two documents takes precedent.1.3 The word “specifications” will be used throughout this document to describe B02.07 standards because the majority of B02.07 standards are categorized as such. Nevertheless, the instruction herein applies to any standards under the jurisdiction of B02.07.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D5063-90(2012) Standard Guide for Use of Certification of Coating Conformance Form (Withdrawn 2021) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

This guide for certification of coating conformance form provides procurement information concerning products being furnished in accordance with a specific coating specification and additional requirements contained in the purchase order. The certification form is divided into four headings: General Type and Description(I), Buyer Information(II), Seller Information (III), and Certification (IV). The first heading consists of the following information: generic type, manufacturer's designation, specification number, formula number, component number, component identification, and color. The second heading consists purchase order number, release number, part number, item number, and stock number. The third heading consists of seller's representative, batch number, lot number, date of manufacture, and date of certification expiration. The last heading is a paragraph describing the certification.1.1 This certification of coating conformance form provides procurement information concerning products being furnished in accordance with a specific coating specification and additional requirements contained in the purchase order (see Fig. 1).CERTIFICATION OF COATING CONFORMANCE FORM Number:Date:I. GENERAL TYPE AND DESCRIPTION: Generic Type: Manufacturer's Designation: Specification Number: Formula Number: Number of Components: Component Identification (if applicable): Color:II. BUYER INFORMATION: Name and Address: Purchase Order Number: Release Number (if applicable): Part Number (if applicable): Item Number (if applicable): Stock Number (if applicable):III. SELLER INFORMATION: Name and Address: Seller's Representative: (Include Telephone Number) Batch Number: Lot No.: Date of Manufacture: Date of Expiration of Certification:IV. CERTIFICATION:This is to certify that the above material being furnished has been manufactured in accordance with the specification and meets all specification requirements contained in the above purchase order. NAME AND TITLE SIGNATURE DATEFIG. 1 Certification Form1.2 The completed form can be utilized to help evaluate the acceptability of the paint being furnished.

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This specification covers the requirements for Halon 1301, or halogenated hydrocarbon compound Bromotrifluoromethane (CF3Br) as a fire-fighting medium. The fire-fighting equipment or hardware that employs Halon 1301, the conditions of employing such equipment (for example, handhelds, fixed installations, etc.), and the storage or transportation of Halon 1301, are not addressed in this specification. The material shall be tested for purity, methanol impurity, acidity, water content, halogen ion content, nonvolatile residue, suspended matter and sediment, and fixed or nonabsorbable gases in the vapor phase.1.1 This practice covers the sampling, for the determination of chemical composition (Note 1) of nonferrous metals and alloys, excluding aluminum, in cast form for remelting or mechanical working.1.1.1 Refer to Practice E255 for copper and copper alloys.NOTE 1: The selection of correct portions of material and the preparation of a representative sample from such portions are necessary prerequisites to every analysis, the analysis being of no value unless the sample actually represents the average composition of the material from which it was selected.1.2 When agreed upon between the purchaser and the manufacturer, the heat sample and analysis may be accepted as representative of the composition of the metal. In such cases, each lot must be properly identified with the heats from which it was made.1.3 This practice is intended to cover the general principles of sampling applicable to nonferrous metals in cast form and is not intended to supersede or replace existing specification requirements for sampling of a particular material.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is designed to compare sealing characteristics of gasket materials under controlled conditions by providing a precise measure of leakage rate at different press loads up to 32 MPa (4640 psi).5.2 This test method is suitable for measuring leakage rates from 0.1 mL/min to as high as 5 L/min for gases.5.3 This test method evaluates leak rates after time periods (typically 30 min) that result in a steady state leakage rate condition. Holding gasket materials under load and internal fluid pressure until steady state is achieved is required to obtain reproducible results.5.4 If the fluid being used in the test causes changes, such as swelling, in the gasket material, it may affect results and diminish repeatability.1.1 This test method covers a means of evaluating the sealing properties of sheet, composite, and solid form-in-place gasket materials (see Classification F104 or F868) at room temperature, and may be used for fluid (gas or liquid) leak rate measurements. It utilizes relatively short hold times and is not intended to predict long-term performance in application.1.2 This test method is suitable for evaluating the sealing characteristics of a gasket material under different press loads by measuring the leakage rate. This test method may be used as an acceptance test when the producer and user have agreed to specific test conditions for the following parameters: (1) test medium, (2) internal pressure of the medium, (3) press load on the gasket specimen, and (4) the surface finish of the platens.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers GALFAN, zinc-aluminum-mischmetal (Zn-5Al-MM) alloy (UNS Z38510) in ingot form for remelting for use in the production of hot-dip coatings on steel. The alloys may be made by any approved process and shall be free from dross, slag, or other harmful contamination. The alloys shall conform to the requirements as to chemical composition prescribed for aluminum, cerium and lanthanum, iron, silicon, lead, cadmium, tin, zinc, and other elements. Sampling for chemical analysis of the alloy in standard ingot form shall be done either by drilling, sawing, or melting, and shall meet the requirements specified for selection of portion, sample preparation, and size of sample and storage. Determination of the chemical composition shall be performed by ICP argon plasma spectrometric or other methods. X-ray fluorescence spectrometry may be used for determination of cerium and lanthanum.1.1 This specification covers GALFAN, zinc-5 % aluminum-mischmetal (Zn-5Al-MM) alloy (UNS Z38510)3 in ingot form for remelting for use in the production of hot-dip coatings on steel. Alloy composition is specified in Table 1.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers three types of zinc-aluminum (Zn-Al) alloys in ingot form for re-melting for use in the production of hot-dip coatings on steel: Type 5 (95/5 Zn/Al), Type 10 (90/10 Zn/Al), and Type 15 (85/15 Zn/Al). Requirements prescribed by this specification cover ordering information; chemical, physical, and mechanical requirements; sampling for determination of chemical composition; methods for chemical analysis; material and manufacturing requirements; dimensions, mass, shapes, and sizes; workmanship, finish, and appearance; inspection and certification; product and package marking; and packaging and preparation for delivery.1.1 This specification covers certain zinc-aluminum (Zn-Al) alloys in ingot form for re-melting for use in the production of hot-dip coatings on steel. Alloy compositions are specified below and in Table 1.ASTM Common UNSType 5 95/5 Zn/Al Z30507Type 10 90/10 Zn/Al Z30600Type 15 85/15 Zn/Al Z30706NOTE 1: The zinc-aluminum alloys in Specification B997 are intended to be used primarily to create a molten zinc-aluminum bath and differ from the master alloys in Specification B860 which are intended primarily to adjust the concentration of certain elements in molten zinc galvanizing baths.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is particularly applicable where the fluid has too high a viscosity or where a component is too volatile for a specific gravity balance determination.1.1 This test method covers the measurement of density (weight per gallon) of adhesives, and components thereof, when in liquid form.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers the chemical requirements for commercial high fluidity zinc-aluminum alloys in ingot form for remelting for the manufacture of thin wall pressure die castings. A table designates and specifies the requirements for aluminum, magnesium, copper, iron, lead, cadmium, tin, and zinc. The ingots shall conform to the requirements as to chemical composition as prescribed in this table. The specification also covers methods for the determination of chemical composition; dimensions, mass, and permissible variation; and shapes and sizes.1.1 This specification covers a commercial zinc-aluminum alloy in ingot form for remelting for the manufacture of thin wall pressure die castings as designated and specified in Table 1.1.2 Systems of nomenclature used to designate zinc and zinc-aluminum (ZA) alloys used for casting are described in Appendix X1.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers two commercial zinc alloys, namely: Slush Casting Alloy A (Z34510) and Slush Casting Alloy B (Z30500), in ingot form for remelting for the manufacture of castings. This slush casting alloys are used primarily for the manufacture of hollow castings such as lighting fixtures, lamp bases, and small statues. The alloys may be made by any approved process, shall be of uniform quality, and shall be free from dross, slag, or other harmful contamination. The ingot shall be reasonably free of surface corrosion and adhering foreign matter. Casting alloys in black/red and black/orange color codes shall conform to the chemical composition requirements prescribed for copper, aluminum, lead, cadmium, tin, iron, magnesium, and zinc. The requirements for chemical composition verification such as number of samples, methods of sampling, and method of chemical analysis are given.1.1 This specification covers commercial zinc alloys in ingot form for remelting for the manufacture of castings from the alloys as specified and designated as shown in Table 1.1.2 Slush casting alloys are used primarily for the manufacture of hollow castings such as lighting fixtures, lamp bases, and small statues.1.3 This specification covers two zinc alloys which are specified and designated as follows:UNS ASTMZ34510 Slush Casting Alloy AZ30500 Slush Casting Alloy B1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Test Method D1578 for testing any spun yarn for breaking strength is considered satisfactory for acceptance testing of commercial shipments since the method has been used extensively in the trade.5.1.1 In case of a dispute arising from differences in reported test results when using Test Method D1578 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens which are as homogeneous as possible and which are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test for unpaired data and an acceptable probability level chosen by the two parties before testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.5.2 This test method is not suitable for yarns that stretch more than 5 % when the force is increased from 2.5 to 7.5 mN/tex or 0.03 to 0.08 gf/denier, because (a ) they require special precautions as to tension in reeling, and (b) users of such yarns are more interested in their elastic behavior at low forces than in their ultimate breaking strength.5.3 For Option 1, it is advisable to use a tensile testing machine of the proper capacity to break skeins with 80 turns. If it is necessary to break skeins having only 40 or 20 turns, convert the observed results to an 80-turn basis by multiplying by factors of 2 or 4, respectively. (The available literature does not show that any significant error is introduced by the use of these factors.)5.4 The circumference of the skeins used to determine the breaking load is not critical, and as a consequence, close control of the tension at which the skeins are wound is not necessary. If, however, the same skeins are to be used to determine yarn number for any purpose, the skeins must be reeled under controlled tension on a reel meeting the requirements given in Test Method D1907.5.5 For some purposes it may be advisable to convert the skein breaking strength observed for yarn of one number to the estimated skein breaking strength of a different yarn number. Factors for making such a conversion for cotton yarns are given in 11.2. No corresponding factors have been developed for yarns spun from other fibers.5.6 The results obtained from different options are not fully comparable because the breaking force per wrap increases slightly as the perimeter of the skein is reduced. The skein breaking tenacity observed for 1 m skeins may be as much as 4 % higher, and from 1-yd skeins 5 % higher, than that observed for 1.5-yd skeins. These relationships may vary with the type of yarn or with yarn unevenness and should not be used as conversion factors. With a reasonable number of specimens, this method provides a useful index that combines the effects of unevenness and single strand strength.5.7 This method is rarely, if ever, used for filament yarns because their uniformity makes it possible to obtain reliable results economically by the single-strand method.1.1 This test method covers the determination of the breaking strength of yarn in skein form. The observed breaking strength is expressed in units of force, and equations are provided to convert breaking strength to skein breaking tenacity and to skein break factor.NOTE 1: For the determination of the breaking strength and elongation of yarn by the single strand method, refer to Test Method D2256.1.2 This test method is applicable to spun yarns, either single or plied, composed of any fiber or blend of fibers, but is not suitable for yarns which stretch more than 5 % when the tension is increased from 2.5 to 7.5 mN/tex or 0.03 to 0.08 gf/denier.1.3 This test method provides three options based on the perimeter of the reel, the number of wraps in the skein, and the machine speed or time-to-break.1.3.1 Option 1—Eighty, forty, or twenty turns on a 1.50 m or 1.5-yd reel, broken at 300 mm/min or 12 in./min.1.3.2 Option 2—Fifty turns on a 1.00 m or 1-yd reel, broken at 300 mm/min or 12 in./min.1.3.3 Option 3—Fifty turns on a 1 m reel, broken in 20 s.NOTE 2: Option 1 is in general use in the United States, Option 2 is used for woolen yarns, and Option 3 has been proposed in the International Standards Organization (ISO) for international use.NOTE 3: Metric reels are available with 1 and 1.125 m circumferences. Data from the two reels will be about 1 % different (see 5.6). ISO uses a 1 m circumference reel.1.4 This test method is frequently combined with the determination of linear density carried out on the same skeins. Special precautions for reeling such skeins are noted.1.5 Where appropriate, this test method states all requirements in SI units. The traditional units are inch-pound and are exact values.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The test method is intended to evaluate the effects of evaporation, settlement, and early autogenous shrinkage on the plastic shrinkage cracking performance of fiber reinforced concrete up to and for some hours beyond the time of final setting (see Terminology C125).5.2 The measured values obtained from this test may be used to compare the performance of concretes with different mixture proportions, concretes with and without fibers, concretes containing various amounts of different types of fibers, and concretes containing various amounts and types of admixtures. For meaningful comparisons, the evaporative conditions during test shall be sufficient to produce an average crack width of at least 0.5 mm in the control specimens (2, 3) (see Note 2). In addition, the evaporation rate from a free surface of water shall be within ± 5 % for each test.NOTE 2: To achieve evaporation rates that result in a crack of at least 0.5 mm in the control specimens, it may be necessary to use an evaporation rate higher than that discussed in Note 1.5.3 This method attempts to control atmospheric variables to quantify the relative performance of a given fresh concrete mixture. Since many other variables such as cement fineness, aggregate gradation, aggregate volume, mixing procedures, slump, air content, concrete temperature and surface finish can also influence potential cracking, attention shall be paid to keep these as consistent as possible from mixture to mixture.1.1 This test method compares the surface cracking of fiber reinforced concrete panels with the surface cracking of control concrete panels subjected to prescribed conditions of restraint and moisture loss that are severe enough to produce cracking before final setting of the concrete.1.2 This test method can be used to compare the plastic shrinkage cracking behavior of different concrete mixtures containing fiber reinforcement.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers commercial zinc and zinc-aluminum alloys in ingot form for remelting for the manufacture of pressure die castings, foundry castings and continuous cast bar stock. Seven alloy compositions are specified, which includes Z33521, Z33522, Z35530, Z35540, for zinc alloys and Z35635, Z35630, Z35840, for zinc-aluminum alloys. The material shall be of uniform quality and reasonably free from dross, adhering foreign matter, and surafce oxide. The determination of chemical composition shall be made in accordance with suitable analytical methods.1.1 This specification covers commercial zinc and zinc-aluminum (ZA) alloys in ingot form for remelting for the manufacture of pressure die castings, foundry castings and continuous cast bar stock as designated and specified in Table 1. Seven alloy compositions are specified, designated as follows:Common Traditional ASTMA UNSA       Alloy 3 Zamak 3 AG 40A Z33524Alloy 7 Zamak 7 AG 40B Z33526Alloy 5 Zamak 5 AC 41A Z35532Alloy 2 Zamak 2 AC 43A Z35544ZA-8 ZA-8  ... Z35637ZA-12 ZA-12 ... Z35632ZA-27 ZA-27 ... Z35842ACuZinc52 ACuZinc5 ... Z465401.2 Zinc alloys Z33524, Z33526, Z35532, Z46540, and Z35544 are used primarily for remelting in the manufacture of pressure die castings. Zinc-aluminum alloys Z35637, Z35632, and Z35842 are used for remelting in the manufacture of both foundry and pressure die castings. Castings made from these ingots are specified in Specification B86, Standard Specification for Zinc and Zinc-Aluminum Alloys for Foundry and Die Castings.1.3 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.1.4 Systems of nomenclature used to designate zinc and zinc-aluminum (ZA) alloys used for casting are described in Appendix X1.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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