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AbstractThese test methods cover determination of the total normal emittance of surfaces by means of portable, inspection-meter instruments. At least two different types of instruments are commercially available for performing this measurement. Test Method A uses an instrument which measures radiant energy reflected from the specimen and Test Method B utilizes an instrument which measures radiant energy emitted from the specimen. Both test methods are limited in accuracy by the degree to which the emittance properties of calibrating standards are known and by the angular emittance characteristics of the surfaces being measure. Test Method A is normally subject to a small error caused by the difference in wavelength distributions between the radiant energy emitted by the two cavities at different temperatures, and that emitted by a blackbody at the specimen temperature. Test Method B also has nongray errors since the detector is not at absolute zero temperature. Test Method A is subject to small errors that may be introduced if the orientation of the sensing component is changed between calibration and specimen measurements. This type of error results from minor changes in alignment of the optical system. Test Method A is subject to error when curved specular surfaces of less than about a certain radius are measured. These errors can be minimized by using calibrating standards that have the same radius of curvature as the test surface. Test Method A can measure reflectance on specimens that are either opaque or semi-transparent in the wavelength region of interest. However, if emittance is to be derived from the reflectance data on a semi-transparent specimen, a correction must be made for transmittance losses. Test Method B is subject to several possible significant errors. These may be due to variation of the test surface temperature during measurements, differences in temperature between the calibrating standards and the test surfaces, changes in orientation of the sensing component between calibration and measurement, errors due to irradiation of the specimen with thermal radiation by the sensing component, and errors due to specimen curvature. Test Method B is limited to emittance measurements on specimens that are opaque to infrared radiation in the wavelength region of interest. 1.1 These test methods cover determination of the total normal emittance (Note 1) of surfaces by means of portable, as well as desktop, inspection-meter instruments. Note 1: Total normal emittance (εN) is defined as the ratio of the normal radiance of a specimen to that of a blackbody radiator at the same temperature. The equation relating εN to wavelength and spectral normal emittance [εN(λ)] is where: L b(λ, T)   =   Planck's blackbody radiation function = c1λ−5(ec2/λT − 1)−1, c1   =   3.7415 × 10−16W·m 2, c2   =   1.4388 × 10−2 m·K, T   =   absolute temperature, K, λ   =   wavelength, m,   =   σT4, and σ   =   Stefan-Boltzmann constant = 5.66961 × 10 −8 W·m−2·K−4 1.2 These test methods are intended for measurements on large surfaces, or small samples, or both, when rapid measurements must be made and where a nondestructive test is desired. They are particularly useful for production control tests. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Once the extent and type of oiling has been defined and documented using proper procedures (see Guides F1686 and F1687), decisions are made on the appropriate course of action for site cleaning and restoration. In some cases, natural recovery (accompanied by monitoring) can be the preferred approach whereas in other cases, active response may be preferred and appropriate. This guide summarizes the principal response techniques available for shoreline, wetland, and terrain habitats.4.2 This guide is intended to minimize the potential for added impact to the environment from use of response techniques in an overly-aggressive manner or in unsuitable conditions or habitats.4.3 In Section 5, typical considerations, which can limit the applicability of a given technique are addressed in Constraints. An example that is applicable to all techniques other than natural recovery, is special permission will likely be needed for any response operations at sites with known culturally or historically important resources. Also, in Section 5, a synopsis of main trade-offs from use of a particular technique is provided in Environmental Effects.1.1 This guide describes methods to clean and remediate stranded oil on marine and lake shorelines, on river banks and other inland water body shorelines, and terrestrial habitats. The primary goal of any countermeasure is to aid recovery while minimizing additional impact.1.2 This guide describes 22 different tactics that are available for consideration. These options range from natural recovery to active physical or biochemical intervention.1.3 The tactics listed might not be appropriate under all possible circumstances, and multiple countermeasures could be appropriate on the same shoreline, river bank, lake shore or terrestrial habitat.1.4 This guide describes technical considerations for selecting appropriate response countermeasures or techniques.1.5 Selection of specific countermeasures for use during a spill response is guided by properties of the oil, degree of oiling, site accessibility, geomorphology, substrate and vegetation type, mobility of available equipment, hydrologic (coastal and inland) and meteorological conditions, and the presence of sensitive natural and archeological resources. It is advisable to consult with appropriate regulatory authorities since certain response options may require government authorization or approval, or both.1.6 This guide does not address response to submerged, sunken or buried oil.1.7 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents: therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Geomembranes are used as barriers to prevent liquids from leaking from landfills, ponds, and other containments. For this purpose, it is desirable that the geomembrane have as little leakage as practical.4.2 The liquids may contain contaminants that, if released, can cause damage to the environment. Leaking liquids can erode the subgrade, causing further damage. Leakage can result in product loss or otherwise prevent the installation from performing its intended containment purpose.4.3 Geomembranes are often assembled in the field, either by unrolling and welding panels of the geomembrane material together in the field, unfolding flexible geomembranes in the field, or a combination of both.4.4 Geomembrane leaks can be caused by poor quality of the subgrade, poor quality of the material placed on the geomembrane, accidents, poor workmanship, manufacturing defects, and carelessness.4.5 Experience demonstrates that geomembranes can have leaks caused during their installation and placement of material(s) on the geomembrane.4.6 Electrical leak location methods are an effective and proven quality assurance measure to locate leaks. Such methods have been used successfully to locate leaks in electrically insulating geomembranes such as polyethylene, polypropylene, polyvinyl chloride, chlorosulfonated polyethylene, and bituminous geomembranes installed in basins, ponds, tanks, ore and waste pads, and landfill cells.4.7 The principle behind these techniques is to place a voltage across a sufficiently electrically insulating geomembrane and then locate areas where electrical current flows through leaks in the geomembrane (as shown schematically in Fig. 1). Other electrical leak paths such as pipe penetrations, flange bolts, steel drains, and batten strips on concrete and other extraneous electrical paths should be electrically isolated or insulated to prevent masking of leak signals caused by electrical short-circuiting through those preferential electrical paths. The only electrical paths should be through leaks in the geomembrane. These electrical detection methods for locating leaks in geomembranes can be performed on exposed geomembranes, on geomembranes covered with water, or on geomembranes covered with an earthen material layer.FIG. 1 Schematic of the Electrical Leak Location Method (Earthen Material-Covered Geomembrane System is Shown)1.1 This guide is intended to assist individuals or groups in assessing different options available for locating leaks in installed geomembranes using electrical methods. For clarity, this guide uses the term “leak” to mean holes, punctures, tears, knife cuts, seam defects, cracks, and similar breaches in an installed geomembrane (as defined in 3.2.6).1.2 This guide does not cover systems that are restricted to seam testing only, nor does it cover systems that may detect leaks non-electrically. It does not cover systems that only detect the presence, but not the location, of leaks.1.3 (Warning—The electrical methods used for geomembrane leak location could use high voltages, resulting in the potential for electrical shock or electrocution. This hazard might be increased because operations might be conducted in or near water. In particular, a high voltage could exist between the water or earth material and earth ground, or any grounded conductor. These procedures are potentially very dangerous, and can result in personal injury or death. The electrical methods used for geomembrane leak location should be attempted only by qualified and experienced personnel. Appropriate safety measures must be taken to protect the leak location operators as well as other people at the site.)1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice provides one way for a laboratory to develop data-based Type A estimates of uncertainty as referred to in Section A22 in Form and Style for ASTM Standards.4.2 Laboratories accredited under ISO/IEC 17025 are required to present uncertainty estimates for their test results. This practice provides procedures that use test results to develop uncertainty estimates for an individual laboratory.4.3 Generally, these test results will be from a single sample of stable and homogeneous material known as a control or check sample.4.4 The true value of the characteristic(s) of the control sample being measured will ordinarily be unknown. However, this methodology may also be used if the control sample is a reference material, in which case the test method bias may also be estimated and incorporated into the uncertainty estimate. Many test methods do not have true reference materials available to provide traceable chains of uncertainty estimation.4.5 This practice also allows for ongoing monitoring of the laboratory uncertainty. As estimates of the level of uncertainty change, possibly as contributions to uncertainty are identified and minimized, revision to the laboratory uncertainty will be possible.AbstractThis practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on a control sample. This practice provides one method for a laboratory to estimate Measurement Uncertainty in accordance with Section A22.3 in Form and Style for ASTM Standards. This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart to monitor the estimate of uncertainty.This practice provides one way for a laboratory to develop data-based Type A estimates of uncertainty as referred to in Section A22 in Form and Style for ASTM Standards.1.1 This practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on a control sample. This practice provides one method for a laboratory to estimate Measurement Uncertainty in accordance with Section A22.3 in Form and Style for ASTM Standards.1.2 Uncertainty as defined by this practice applies to the capabilities of a single laboratory. Any estimate of uncertainty determined through the use of this practice applies only to the individual laboratory for which the data are presented.1.3 The laboratory uses a well defined and established test method in determining a series of test results. The uncertainty estimated using this practice only applies when the same test method is followed. The uncertainty only applies for the material types represented by the control samples, and multiple control samples may be needed, especially if the method has different precision for different sample types or response levels.1.4 The uncertainty estimate determined by this practice represents the intermediate precision of test results. This estimate seeks to quantify the total variation expected within a single laboratory using a single established test method while incorporating as many known sources of variation as possible.1.5 This practice does not establish error estimates (error budget) attributed to individual factors that could influence uncertainty.1.6 This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart to monitor the estimate of uncertainty.1.7 The system of units for this standard is not specified. Dimensional quantities in the standard are presented only as illustrations of calculation methods. The examples are not binding on products or test methods treated.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Petrographic examinations are made for the following purposes:5.1.1 To determine the mineralogy of the material that may be observed by petrographic methods (in this method, by use of XRD) and that may have a bearing on the performance of the material in its intended use.5.1.2 To determine the relative amounts of the constituents of the sample which is essential for proper evaluation of the sample when the constituents may differ significantly in properties that have a bearing on the performance of the material in its intended use.5.1.3 This method helps to evaluate mineral aggregate sources for suitability as a material to be used for construction, renovation, or modification of equine surfaces. The information gathered will allow for the comparison of the composition of new mineral sources with samples of other mineral aggregate from one or more sources, for which test data or performance records are available.5.2 This method may be used by a petrographer employed directly by those for whom the examination is made. The employer should tell the petrographer, in as much detail as necessary, the purposes and objectives of the examination, the kind of information needed, and the extent of examination desired. Pertinent background information, including results of prior testing, should be made available. The petrographer’s advice and judgment should be sought regarding the extent of the examination.5.3 This method may form the basis for establishing arrangements between a purchaser of consulting petrographic service and the petrographer. In such a case, the purchaser and the consultant should together determine the kind, extent, and objectives of the examination and analyses to be made and should record their agreement in writing. The agreement may stipulate specific determinations to be made, observations to be reported, funds to be obligated, or a combination of these or other conditions.1.1 X-Ray diffraction (XRD) is a tool for identifying minerals, such as quartz and feldspar, and types of clay present in bulk samples of equine surfaces. Determining the mineralogy of a given bulk sample provides insight into surface properties, such as abrasion resistance by comparing the relative differences of hardness of the various mineral fractions such as quartz or feldspar or the plasticity differences in clay minerals such as smectite or kaolinite. XRD techniques are qualitative in nature and only semi-quantitative.1.2 Particle size distribution analyses methods including hydrometer tests to determine proportions of sand, silt, and clay fractions based upon particle size but are not able to distinguish particles by shape or mineralogy of materials. In addition to a qualitative detection of minerals present in a sample, XRD methods are also semi-quantitative and also yield important data on the relative proportion of particular minerals present.1.3 XRD techniques are generally semi-quantitative in nature. Even so, such semiquantitative data is useful in determining relative proportions of each mineral type. This method is also semi-qualitative in nature as it is geared for the determination or mineral groups. For example, it will determine the relative amount of alkali feldspars (such as K-feldspar or Nafeldspar) from Plagioclase-feldspar but not necessarily if the Plagioclase-feldspar is albite or anorthite nor whether the K-feldspar is orthoclase of microcline. Likewise, it will differentiate smectite from mica from kaolinite but not whether the smectite is montmorillonite or saponite. More precise determination of mineral species by XRD is possible but involves more advanced preparation and treatment methods than what is within the scope of this standard.1.4 The XRD method herein primarily makes use of “Glass Slide Method” but may be subject to modification depending on the user’s needs.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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6.1 This test method provides standard procedures for experimentally determining the XEC for use in the measurement of residual and applied stresses using x-ray diffraction techniques. It also provides a standard means of reporting the precision of the XEC.6.2 This test method is applicable to any crystalline material that exhibits a linear relationship between stress and strain in the elastic range, that is, only applicable to elastic loading.6.3 This test method should be used whenever residual stresses are to be evaluated by x-ray diffraction techniques and the XEC of the material are unknown.1.1 This test method covers a procedure for experimentally determining the x-ray elastic constants (XEC) for the evaluation of residual and applied stresses by x-ray diffraction techniques. The XEC relate macroscopic stress to the strain measured in a particular crystallographic direction in polycrystalline samples. The XEC are a function of the elastic modulus, Poisson’s ratio of the material and the hkl plane selected for the measurement. There are two XEC that are referred to as 1/2 S2hkl and S1 hkl.1.2 This test method is applicable to all x-ray diffraction instruments intended for measurements of macroscopic residual stress that use measurements of the positions of the diffraction peaks in the high back-reflection region to determine changes in lattice spacing.1.3 This test method is applicable to all x-ray diffraction techniques for residual stress measurement, including single, double, and multiple exposure techniques.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is intended to be used for compliance with compositional specifications for manganese content in iron ores, concentrates, and agglomerates. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.1.1 These test methods cover the determination of manganese in iron ores, concentrates, and agglomerates. The following two test methods are included:  Sections Test Method A (Pyrophosphate (Potentiometric))  8 – 15 Test Method B (Periodate (Spectrophotometric)) 16 – 221.2 Test Method A covers the determination of manganese in the range from 2.5 % to 15.0 %. Test Method  B covers the determination of manganese in the range of 0.01 % to 5.00 %.NOTE 1: The lower limit for this test method is set at 50 % relative error for the lowest grade material tested in the interlaboratory study in accordance with Practice E1601.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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