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4.1 For ferromagnetic materials, magnetic particle examination is widely specified for the detection of surface and near surface discontinuities such as cracks, laps, seams, and linearly oriented nonmetallic inclusions. Such examinations are included as mandatory requirements in some forging standards such as Specification A508/A508M.4.2 Use of direct current or rectified alternating (full or half wave) current as the power source for magnetic particle examination allows detection of subsurface discontinuities.AbstractThis test method covers the procedures for the standard practice of performing magnetic particle examination on steel forgings. The inspection medium shall consist of finely divided ferromagnetic particles, whose size, shape and magnetic properties, both individually and collectively, shall be taken into account. Forgings may be magnetized in the longitudinal or circular direction by employing the surge or continuous current flow methods. Magnetization may be applied by passing current through the piece or by inducing a magnetic field by means of a central conductor, such as a prod or yoke, or by coils. While the material is properly magnetized, the magnetic particles may be applied by either the dry method, wet method, or fluorescent method. The parts shall also be sufficiently demagnetized after inspection so that residual or leakage fields will not interfere with future operations to which the steel forgings shall be used for. Indications to be evaluated are grouped into three broad classes, namely: surface defects, which include laminar defects, forging laps and folds, flakes (thermal ruptures caused by entrapped hydrogen), heat-treating cracks, shrinkage cracks, grinding cracks, and etching or plating cracks; subsurface defects, which include stringers of nonmetallic inclusions, large nonmetallics, cracks in underbeads of welds, and forging bursts; and nonrelevant or false indications, which include magnetic writing, changes in section, edge of weld, and flow lines.1.1 This practice2 covers a procedure for magnetic particle examination of steel forgings. The procedure will produce consistent results upon which acceptance standards can be based. This practice does not contain acceptance standards or recommended quality levels.1.2 Only direct current or rectified alternating (full or half wave) current shall be used as the electric power source for any of the magnetizing methods. Alternating current is not permitted because its capability to detect subsurface discontinuities is very limited and therefore unsuitable.1.2.1 Portable battery powered electromagnetic yokes are outside the scope of this practice.NOTE 1: Guide E709 may be utilized for magnetic particle examination in the field for machinery components originally manufactured from steel forgings.1.3 The minimum requirements for magnetic particle examination shall conform to practice standards of Practice E1444/E1444M. If the requirements of this practice are in conflict with the requirements of Practice E1444/E1444M, the requirements of this practice shall prevail.1.4 This practice and the applicable material specifications are expressed in both inch-pound units and SI units. However, unless the order specifies the applicable “M” specification designation [SI units], the material shall be furnished to inch-pound units.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of the ASTM Committee A01 on Steel, Stainless Steel and Related Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.1.1 These test methods cover the chemical analysis of high-temperature, electrical, magnetic, and other similar iron, nickel, and cobalt alloys having chemical compositions within the following limits:    Element Composition Range, %               Aluminum 0.005 to 18.00    Beryllium 0.001 to  0.05    Boron 0.001 to  1.00    Calcium 0.002 to   0.05    Carbon 0.001 to  1.10    Chromium 0.10  to 33.00    Cobalt 0.10  to 75.00    Columbium (Niobium) 0.01  to  6.0    Copper 0.01  to 10.00    Iron 0.01  to 85.00    Magnesium 0.001 to  0.05    Manganese 0.01  to  3.0    Molybdenum 0.01  to 30.0    Nickel 0.10  to 84.0    Nitrogen 0.001 to  0.20    Phosphorus 0.002 to  0.08    Silicon 0.01  to  5.00    Sulfur 0.002 to  0.10    Tantalum 0.005 to 10.0    Titanium 0.01  to  5.00    Tungsten 0.01  to 18.00    Vanadium 0.01  to  3.25    Zirconium 0.01  to  2.50  1.2 The test methods in this standard are contained in the sections indicated below:  Sections   Aluminum, Total, by the 8-Quinolinol Gravimetric Method (0.20 %   to 7.00 %) 100 – 107Carbon, Total, by the Combustion-Thermal Conductivity Method—Discontinued 1986 124 – 134Carbon, Total, by the Combustion Gravimetric Method (0.05 % to 1.10 %)—Discontinued 2014 79 – 89Chromium by the Atomic Absorption Spectrometry Method   (0.006 % to 1.00 %) 165 – 174Chromium by the Peroxydisulfate Oxidation—Titration Method (0.10 % to 33.00 %)  175 – 183Chromium by the Peroxydisulfate-Oxidation Titrimetric Method—   Discontinued 1980 116 – 123Cobalt by the Ion-Exchange-Potentiometric Titration Method (2 %   to 75 %)  53 – 60Cobalt by the Nitroso-R-Salt Spectrophotometric Method (0.10 %    to 5.0 %)  61 – 70Copper by Neocuproine Spectrophotometric Method (0.01 % to   10.00 %)  90 – 99Copper by the Sulfide Precipitation-Electrodeposition Gravimetric Method (0.01 % to 10.00 %)  71 – 78Iron by the Silver Reduction Titrimetric Method (1.0 % to 50.0 %) 192 –199Manganese by the Metaperiodate Spectrophotometric Method   (0.05 % to 2.00 %)  9 – 18Molybdenum by the Ion Exchange—8-Hydroxyquinoline Gravi- metric Method (1.5 % to 30 %) 184 – 191Molybdenum by the Thiocyanate Spectrophotometric Method   (0.01 % to 1.50 %) 153 – 164Nickel by the Dimethylglyoxime Gravimetric Method (0.1 % to 84.0 %) 135 – 142Phosphorus by the Molybdenum Blue Spectrophotometric Method   (0.002 % to 0.08 %) 19  – 30Silicon by the Gravimetric Method (0.05 % to 5.00 %) 46  – 52Sulfur by the Gravimetric Method—Discontinued   1988 Former 30  – 36Sulfur by the Combustion-Iodate Titration Method (0.005 % to 0.1 %)—Discontinued 2014 37  – 45Sulfur by the Chromatographic Gravimetric Method—Discontinued   1980 108 – 115Tin by the Solvent Extraction–Atomic Absorption Spectrometry   Method (0.002 % to 0.10 %) 143  – 1521.3 Methods for the determination of carbon and sulfur not included in this standard can be found in Test Methods E1019.1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single method and therefore this standard contains multiple methods for some elements. The user must select the proper method by matching the information given in the and Interference sections of each method with the composition of the alloy to be analyzed.1.5 Units—The values stated in SI units are to be regarded as standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special “Warning” paragraphs throughout these test methods.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 This test method provides a satisfactory means of determining various ac magnetic properties of amorphous magnetic materials.3.2 The procedures described herein are suitable for use by producers and users of magnetic materials for materials specification acceptance and manufacturing control.3.3 The procedures described herein may be adapted for use with specimens of other alloys and other toroidal forms.1.1 This test method covers tests for various magnetic properties of amorphous materials at power frequencies [25 to 400 Hz] using a toroidal test transformer. The term “toroidal test transformer” is used to describe the test device, reserving the term “specimen” to refer to the material used in the test. The test specimen consists of toroidally wound flat strip.1.2 This test method covers the determination of core loss, exciting power, rms and peak exciting current, several types of ac permeability, and related properties under ac magnetization at moderate and high inductions at power frequencies [25 to 70 Hz].1.3 With proper instrumentation and specimen preparation, this test method is acceptable for measurements at frequencies from 5 Hz to 100 kHz. Proper instrumentation implies that all test instruments have the required frequency bandwidth. Also see Annex A2.1.4 This test method also provides procedures for calculating impedance permeability from measured values of rms exciting current and for calculating ac peak permeability from measured peak values of total exciting current at magnetic field strengths up to about 10 Oe [796 A/m].1.5 Explanations of symbols and brief definitions appear in the text of this test method. The official symbols and definitions are listed in Terminology A340.1.6 This test method shall be used in conjunction with Practice A34/A34M.1.7 The values and equations stated in customary (cgs-emu and inch-pound) units or SI units are to be regarded separately as standard. Within this standard, SI units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E709-21 Standard Guide for Magnetic Particle Testing Active 发布日期 :  1970-01-01 实施日期 : 

5.1 The magnetic particle method of nondestructive testing indicates the presence of surface and near-surface discontinuities in materials that can be magnetized (ferromagnetic). This method can be used for production examination of parts/components or structures and for field applications where portability of equipment and accessibility to the area to be examined are factors. The ability of the method to find small discontinuities can be enhanced by using fluorescent particles suspended in a suitable vehicle and by introducing a magnetic field of the proper strength whose orientation is as close as possible to 90° to the direction of the suspected discontinuity (see 4.3.2). A smoother surface or a pulsed current improves mobility of the magnetic particles under the influence of the magnetic field to collect on the surface where magnetic flux leakage occurs.1.1 This guide2 covers techniques for both dry and wet magnetic particle testing, a nondestructive method for detecting cracks and other discontinuities at or near the surface in ferromagnetic materials. Magnetic particle testing may be applied to raw material, semifinished material (billets, blooms, castings, and forgings), finished material and welds, regardless of heat treatment or lack thereof. It is useful for preventive maintenance testing.1.1.1 This guide is intended as a reference to aid in the preparation of specifications/standards, procedures and techniques.1.2 This guide is also a reference that may be used as follows:1.2.1 To establish a means by which magnetic particle testing, procedures recommended or required by individual organizations, can be reviewed to evaluate their applicability and completeness.1.2.2 To aid in the organization of the facilities and personnel concerned in magnetic particle testing.1.2.3 To aid in the preparation of procedures dealing with the examination of materials and parts. This guide describes magnetic particle testing techniques that are recommended for a great variety of sizes and shapes of ferromagnetic materials and widely varying examination requirements. Since there are many acceptable differences in both procedure and technique, the explicit requirements should be covered by a written procedure (see Section 21).1.3 This guide does not indicate, suggest, or specify acceptance standards for parts/pieces examined by these techniques. It should be pointed out, however, that after indications have been produced, they must be interpreted or classified and then evaluated. For this purpose there should be a separate code, specification, or a specific agreement to define the type, size, location, degree of alignment and spacing, area concentration, and orientation of indications that are unacceptable in a specific part versus those which need not be removed before part acceptance. Conditions where rework or repair is not permitted should be specified.1.4 This guide describes the use of the following magnetic particle method techniques.1.4.1 Dry magnetic powder (see 8.4),1.4.2 Wet magnetic particle (see 8.5),1.4.3 Magnetic slurry/paint magnetic particle (see 8.5.7), and1.4.4 Polymer magnetic particle (see 8.5.8).1.5 Personnel Qualification—Personnel performing examinations in accordance with this guide should be qualified and certified in accordance with ASNT Recommended Practice No. SNT-TC-1A, ANSI/ASNT Standard CP-189, NAS 410, or as specified in the contract or purchase order.1.6 Nondestructive Testing Agency—If a nondestructive testing agency as described in Specification E543 is used to perform the examination, the nondestructive testing agency should meet the requirements of Specification E543.1.7 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.8 Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues.  Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury or mercury containing products, or both, into your state or country may be prohibited by law.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers quenched and tempered carbon and alloy steel forgings for magnetic retaining rings for turbine generators. Specimens shall be manufactured by melting process and vacuum degassing. Forgings shall also undergo preliminary machining prior to heat treatment (quenching and tempering) for mechanical properties testing. Steel materials shall conform to tensile and notch toughness requirements, which include tensile strength, yield strength, elongation, reduction of area, and Charpy V-notch impact strength. Heat and product analyses shall be performed as well wherein specimens shall conform to chemical requirements of carbon, manganese, phosphorus, sulfur, nickel, chromium, molybdenum, and vanadium. Nondestructive tests such as magnetic particle test and ultrasonic inspection may also be performed.1.1 This specification covers quenched and tempered carbon and alloy steel forgings for magnetic retaining rings for turbine generators.1.2 Supplementary requirements of an optional nature are provided. These shall apply only when specified by the purchaser.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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