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4.1 The nitrogen content as determined by this test method is normally considered to be related to the amount of hide substance (protein fiber) present in the leather sample. A factor of 5.62 is normally used to calculate the hide substance from the nitrogen content.4.1.1 The 5.62 factor represents the average result of many analyses of animal hides, but it cannot be considered to be accurate since it varies somewhat from hide to hide of the same type, from type of hide to type of hide, and also with the thickness of hide retained in the final leather (split thickness as compared to original hide thickness). As a result of these variations, the true factor for any given leather may be expected to vary from 5.44 to 5.80 or about ±3 %.34.2 A given leather sample may contain nitrogenous substances other than hide substance (protein fiber) which will be analyzed for by this test method, such as resins, dyestuffs, etc., that contain nitrogen. Therefore, although this test method is fairly accurate for determining the nitrogen content of leather, its use for determining hide substance may result in large errors.4.3 The hide substance value derived from this determination has a large bearing on other chemical determinations of a given leather. Any errors, such as those described in 4.1.1 and 4.2, will be carried over into these other analytical calculations.1.1 This test method covers the determination of the nitrogen content of all types of leather, wet blue and wet white. The nitrogen content is used to calculate the hide substance (protein fiber) content of leather, wet blue and wet white.NOTE 1: The original test method for leather was essentially a composite of Method 6441 of Federal Test Method Standard No. 311 and Method B5 of the American Leather Chemists Association.NOTE 2: Melamine, if present in bonded leather, could give an artificially high value for the calculation of protein fiber.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method measures the amount of unfixed chrome in Wet Blue. Results may vary according to the age of the Wet Blue.1.1 This test method covers the procedures to analyze and calculate unfixed chrome concentrations in Wet Blue.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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6.1 The environmental chamber method is an accelerated test for determining the resistance of Wet Blue and Wet White to the growth of fungi, the causal agent of mold. See Test Method D3273.3,46.2 The environmental chamber method is useful in estimating the performance of fungicides and should assist in the prediction of storage time before fungal growth begins.6.3 The environmental chamber method duplicates the natural environment in which Wet Blue or Wet White is inoculated with fungal spores and subsequently disfigured or discolored by fungi.6.4 The environmental chamber method measures the resistance of the treated Wet Blue or Wet White to the germination of spores and subsequent vegetative growth that spreads over the surface of a comparatively large Wet Blue or Wet White specimen over a period of four weeks.6.5 The environmental chamber can be kept inoculated with fungi representative of those found in tanneries by adding samples of Wet Blue and Wet White with fungal growth from currently operating tanneries.6.6 Control specimens of Wet Blue and Wet White without fungicide treatment can be added to the chamber periodically to increase levels of fungal growth in the chamber.6.7 Leaching of fungicide from the test specimen into the agar often causes a zone of inhibition of fungal growth in the Petri dish test, but in the environmental chamber any leaching of fungicide from the test specimen drips into the water contained in the chamber and thus does not cause the types of false readings observed in the Petri dish test.1.1 This environmental chamber method measures the resistance of the treated Wet Blue and Wet White to the germination of spores and subsequent vegetative growth over a period of four weeks. The test method is useful in estimating the performance of fungicides and should assist in the prediction of storage time of Wet Blue and Wet White before fungal growth begins. The apparatus is designed so it can be easily built or obtained by any interested party and duplicate the natural environment in which Wet Blue and Wet White is inoculated with fungal spores. Spores that germinate on untreated or treated Wet Blue and Wet White can produce fungal growth, resulting in disfigurement or discoloration, or both, of the Wet Blue and Wet White.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods are suitable for determining if impurities are present and establishing that the required pigments are present. These test methods may be used for manufacturing and purchasing quality control.1.1 These test methods cover procedures for the qualitative chemical analysis of pigments known commercially as copper phthalocyanine blue and green.1.2 The procedures appear in the following order:  SectionIdentification 5Moisture and Other Volatile Matter 6Detection of Basic Dye Derivatives 7Detection of Other Organic Coloring Matter 8Detection of Ultramarine Blue 9Detection of Iron Blue or Chrome Green 101.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D261-75(1999) Standard Specification for Iron Blue Pigment (Withdrawn 2005) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

1.1 This specification covers the dry pigment commercially known as Prussian blue, Chinese blue, Milori blue, or iron blue.

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5.1 The procedure described is for chromium in Wet Blue using Atomic Absorption or ICP. This method may be used to determine the chromium content in Wet Blue as an alternate to Test Method D6656.5.2 The chromium content of Wet Blue is related to the degree of tannage obtained, and hence may be a matter for specification in the purchase of Wet Blue. The procedure described provides adequate accuracy for this purpose.1.1 This test method covers the Atomic Absorption procedure, using nitrous oxide-acetylene flame, air-acetylene flame or ICP (Inductively coupled plasma) to analyze the chrome content of Wet Blue (and leather) on a moisture-free basis.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in Section 9 on Hazards and in 12.5 and 12.20.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method measures the amount of solvent-soluble (hexane or petroleum ether) materials in wet blue and wet white.1.1 This test method covers the quantitative extraction of all types of wet blue and wet white with hexane or petroleum ether.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Section 7.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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