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ASTM D1199-86(2020) Standard Specification for Calcium Carbonate Pigments Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers two types of high-content calcium carbonate pigments, Type PC and Type GC. Pigments shall be classified into six grades based on particle size, namely: Grade I (fine paint grade); Grade II (coarse paint grade); Grade III (filler grade); Grade IV (putty powder grade); Grade V (superfine grade); and Grade VI (ultrafine grade). Tests shall be conducted in accordance with the following test methods: calcium and magnesium reported as carbonate; moisture and other volatile matter; oil absorption; coarse particles; and dispersed color.1.1 This specification covers two types of high-content calcium carbonate pigments, as follows:1.1.1 Type PC—Calcium carbonate precipitate, prepared either by complete solution or by carbonation of lime.1.1.2 Type GC—Ground mineral product.1.2 Six grades of pigments, based on particle size (see 3.3) are covered.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 Some oils are formulated with organo-metallic additives, which act, for example, as detergents, antioxidants, and antiwear agents. Some of these additives contain one or more of these elements: calcium, phosphorus, sulfur, and zinc. This test method provides a means of determining the concentrations of these elements, which in turn provides an indication of the additive content of these oils.3.2 Several additive elements and their compounds are added to the lubricating oils to give beneficial performance (Table 2).3.3 This test method is primarily intended to be used at a manufacturing location for monitoring of additive elements in lubricating oils. It can also be used in central and research laboratories.1.1 This test method covers the quantitative determination of additive elements in unused lubricating oils, as shown in Table 1.1.2 This test method is limited to the use of energy dispersive X-ray fluorescence (EDXRF) spectrometers employing an X-ray tube for excitation in conjunction with the ability to separate the signals of adjacent elements.1.3 This test method uses interelement correction factors calculated from empirical calibration data.1.4 This test method is not suitable for the determination of magnesium and copper at the concentrations present in lubricating oils.1.5 This test method excludes lubricating oils that contain chlorine or barium as an additive element.1.6 This test method can be used by persons who are not skilled in X-ray spectrometry. It is intended to be used as a routine test method for production control analysis.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Some oils are formulated with organo-metallic additives which act as detergents, antioxidants, antiwear agents, and so forth. Some of these additives contain one or more of these elements: barium, calcium, phosphorus, sulfur, and zinc. These test methods provide a means of determining the concentration of these elements which in turn provides an indication of the additive content of these oils.4.2 Several additive elements and their compounds are added to the lubricating oils to give beneficial performance (see Table 2).1.1 These test methods cover the determination of barium, calcium, phosphorus, sulfur, and zinc in unused lubricating oils at element concentration ranges shown in Table 1. The range can be extended to higher concentrations by dilution of sample specimens. Additives can also be determined after dilution. Two different methods are presented in these test methods.1.2 Test Method A (Internal Standard Procedure)—Internal standards are used to compensate for interelement effects of X-ray excitation and fluorescence (see Sections 8 through 13).1.3 Test Method B (Mathematical Correction Procedure)—The measured X-ray fluorescence intensity for a given element is mathematically corrected for potential interference from other elements present in the sample (see Sections 14 through 19).1.4 The preferred concentration units are mass % barium, calcium, phosphorus, sulfur, or zinc.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Aspects of the biological response to calcium phosphate materials in soft tissue and bone have been reported from laboratory studies and clinical use (1-11).34.2 The requirements of this test method apply to calcium phosphate materials such as calcium hydroxyapatite (see Specification F1185), beta-tricalcium phosphate (see Specification F1088), and biphasic mixtures thereof with or without intentional addition of other minor (<10 %) components.4.3 This test method is limited to the laboratory evaluation of the dissolution rate of a calcium phosphate material. No correlation of the results to in-vivo performance is implied. Therefore, it is recommended that a control material be included in the evaluation. The control material can be a standardized material such as NIST SRM 2910 or a historical control.1.1 This test method covers calcium phosphate materials intended for use in surgical implant applications.1.2 The material(s) shall be representative of that produced for sale. It shall have been produced and processed under standard manufacturing conditions.1.3 The materials may be in the form of powders, granules, spall material, fabricated forms, or coatings; and may be porous, nonporous, textured, and other implantable topographical substrate form representative of the end-use product.1.4 The calcium phosphate material may constitute the only material in a substrate or it may be one of multiple materials so long as all other materials present do not dissolve under the test conditions described in this test method.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method for the chemical analysis of metals and alloys is primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.1.1 This test method covers the chemical analysis of magnesium ferrosilicon having chemical compositions within the following limits:Element Composition Range, % Aluminum 2.0 maxCalcium 0.25 to 3.00Carbon 0.50 maxCerium 1.0 maxChromium 0.50 maxMagnesium 2.00 to 12.00Manganese 1.0 maxSilicon 40.00 to 55.00Sulfur 0.025 maxTitanium 0.2 max1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For general precautions to be observed in this test method, refer to Practices E50.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM F1658-95 Test Method for Shear Testing of Calcium Phosphate Coatings (Withdrawn 2000) Withdrawn, Replaced 发布日期 :  1970-01-01 实施日期 : 

1.1 This test method covers shear testing of continuous calcium phosphate coatings adhering to dense metal substrates at ambient temperatures. It assesses the degree of adhesion of coatings to substrates, or the internal cohesion of a coating in shear, parallel to the surface plane.1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This test method covers the procedure for the performance of calcium phosphate ceramic coatings in shear and bending fatigue modes. In the shear fatigue mode this test method evaluates the adhesive and cohesive properties of the coating on a metallic substrate. In the bending fatigue mode, this test method evaluates both the adhesion of the coating as well as the effects that the coating may have on the substrate material. These test methods are limited to testing in air at ambient temperature. These test methods are not intended for application in fatigue tests of components or devices; however, the test method that most closely replicates the actual loading configuration is preferred. 1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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This specification covers unfabricated and fabricated forms of high purity hydrated calcium sulfate hemihydrate or dihydrate for surgical implants. The requirements of this specification apply to calcium sulfate combined with two molecules of water or two calcium sulfate molecules with one water mole but does not include calcium sulfate anhydrite and calcium sulfate forms that contain reinforcing phases, medicaments, biological agents, and other such additives. All covered materials should conform to the requirements for set time, compressive strength, and in vitro degradation.1.1 This specification covers material requirements for unfabricated and fabricated forms of hydrated calcium sulfate intended for surgical implants. Fabricated forms may include pressed and cast surgical implants in various geometric shapes. The calcium sulfate hemihydrate in the unfabricated form can be converted with the addition of water or other water-containing solutions to a fabricated calcium sulfate dihydrate form.1.2 The requirements of this specification apply to calcium sulfate combined with two molecules of water or two calcium sulfate molecules sharing one water molecule.Approximate chemical formulae:Calcium Sulfate DihydrateCaSO4·2H2O Calcium Sulfate HemihydrateCaSO4·1/2H2O or CaSO4·H2O·CaSO41.3 This specification specifically excludes calcium sulfate anhydrite and calcium sulfate forms that contain additives such as reinforcing phases, medicaments, biological agents, and so forth.1.4 The presence of processing aids does not exclude a product from the physical and mechanical requirements of this specification.1.5 Some provisions of Specification C59/C59M and Test Methods C472 apply. Special requirements that are detailed in this specification are included to characterize the material which will be used in surgical implants.1.6 The biological response to calcium sulfate in bone tissue has been well characterized by a history of clinical use (1-14)2 and by laboratory studies (15-18).1.7 The following precautionary caveat pertains only to the test method portion, Sections 4, 5, and 6, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The shear test method is recommended for shear testing of calcium phosphate and metallic/substrate combinations and can provide information on the adhesive or cohesive strength of coatings under a uniaxial shear stress.5.2 The test method may be useful for comparative evaluation of adhesive or cohesive strengths of a variety of types of coatings. Information developed using this test method may be useful for certain quality control and design purposes.5.3 The test method should not be considered to provide an intrinsic values for utilization directly in making calculations such as determining the ability of a coating to withstand specified environmental stresses.5.4 Processing variables, such as substrate preparation prior to coating, surface texture, coating technique variables or post-coating heat treatment, or heat may introduce a significant effect on the results of the shear test. The specimen being evaluated must be representative of the actual end-use coating.1.1 This test method covers shear testing of continuous calcium phosphate coatings and metallic coatings adhering to dense metal substrates at ambient temperatures. It assesses the degree of adhesion of coatings to substrates, or the internal cohesion of a coating in shear, parallel to the surface plane.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The water content of soil is used throughout geotechnical engineering practice, both in the laboratory and in the field. Results are sometimes needed within a short time period and in locations where it is not practical to install an oven or to transport samples to an oven. This test method is used for these occasions.5.2 The results of this test have been used for field control of compacted embankments or other earth structures such as in the determination of water content for control of soil moisture and dry density within a specified range.5.3 This test method requires specimens consisting of soil having all particles smaller than the 4.75 mm (No. 4) sieve size.5.4 This test method may not be as accurate as other accepted methods such as Test Method D2216. Inaccuracies may result because specimens are too small to properly represent the total soil, from clumps of soil not breaking up to expose all the available water to the reagent and from other inherent procedural, equipment or process inaccuracies. Therefore, other methods may be more appropriate when highly accurate results are required, or when the use of test results is sensitive to minor variations in the values obtained.NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method outlines procedures for determining the water (moisture) content of soil by chemical reaction using calcium carbide as a reagent to react with the available water in the soil producing a gas. A measurement is made of the gas pressure produced when a specified mass of wet or moist soil is placed in a testing device with an appropriate volume of reagent and mixed.1.2 This test method is not intended as a replacement for Test Method D2216; but as a supplement when rapid results are required, when testing is done in field locations, or where an oven is not practical for use. Test Method D2216 is to be used as the test method to compare for accuracy checks and correction.1.3 This test method is applicable for most soils. Calcium carbide, used as a reagent, reacts with water as it is mixed with the soil by shaking and agitating with the aid of steel balls in the apparatus. To produce accurate results, the reagent must react with all the water which is not chemically hydrated with soil minerals or compounds in the soil. Some highly plastic clay soils or other soils not friable enough to break up may not produce representative results because some of the water may be trapped inside soil clods or clumps which cannot come in contact with the reagent. There may be some soils containing certain compounds or chemicals that will react unpredictably with the reagent and give erroneous results. Any such problem will become evident as calibration or check tests with Test Method D2216 are made. Some soils containing compounds or minerals that dehydrate with heat (such as gypsum) which are to have special temperature control with Test Method D2216 may not be affected (dehydrated) in this test method.1.4 This test method is limited to using calcium carbide moisture test equipment made for 20 g, or larger, soil specimens and to testing soil which contains particles no larger than the 4.75 mm (No. 4) Standard sieve size.1.5 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are mathematical conversions, which are provided for information purposes only and are not considered standard.1.5.1 Cited sieve sizes are the standard sieve sizes given in Table 1 of Specification E11.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026 unless superseded by this standard.1.6.1 The procedures used to specify how data are collected, recorded or calculated in this standard are regarded as the industry standard. In addition they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazards statements, see Section 7.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E449-18 Standard Test Methods for Analysis of Calcium Chloride Active 发布日期 :  1970-01-01 实施日期 : 

3.1 Calcium chloride is available in various forms and purities. A major use is the de-icing and dust control of roads. It is also used in the coal industry for dustproofing and freezeproofing, in foods, in electrolytic cells, and in refrigeration brines. The test methods listed in 1.2 provide procedures for analyzing calcium chloride to determine if it is suitable for its intended use.1.1 These test methods cover the analysis of calcium chloride and solutions.1.2 Procedures are given for the determination of calcium chloride, magnesium chloride, potassium chloride, sodium chloride, and calcium hydroxide. The test methods appear in the following order:  SectionsCalcium Chloride 8 to 17Magnesium Chloride, Potassium Chloride,and Sodium Chloride 18 to 28Calcium Hydroxide 29 to 361.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 Review the current Safety Data Sheet (SDS) for detailed information concerning toxicity, first aid procedures, handling, and safety precautions.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 5.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Although Test Method D4017 is widely used for the determination of water in paints and related materials, this method may overcome some of the variability found in the Karl Fischer method.4.2 Control of water content is often important in controlling the performance of paints, and it is critical in determining volatile organic compound (VOC) content when VOC content is measured by difference from total volatile matter and water content as required in certain federal and state regulations.1.1 This test method describes the determination of the total water content of paints using a calcium hydride reaction test kit, or water content between 2 and 85 % water.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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