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5.1 This guide references requirements that are intended to control the quality of NDT data. The purpose of this guide, therefore, is not to establish acceptance criteria and therefore approve composite materials or components for aerospace service.5.2 Following the discretion of the cognizant engineering organization, NDT for fracture control of composite and bonded materials should follow additional guidance described in MIL-HDBK-6870, NASA-STD-(I)-5019, or MSFC-RQMT-3479, or a combination thereof, as appropriate (not covered in this guide).5.3 Certain procedures referenced in this guide are written so they can be specified on the engineering drawing, specification, purchase order, or contract, for example, Practice E1742/E1742M (Radiography).5.4 Acceptance Criteria—Determination about whether a composite material or component meets acceptance criteria and is suitable for aerospace service should be made by the cognizant engineering organization. When examinations are performed in accordance with the referenced documents in this guide, the engineering drawing, specification, purchase order, or contract should indicate the acceptance criteria.5.4.1 Accept/reject criteria should consist of a listing of the expected kinds of imperfections and the rejection level for each.5.4.2 The classification of the articles under test into zones for various accept/reject criteria should be determined from contractual documents.5.4.3 Rejection of Composite Articles—If the type, size, or quantities of defects are found to be outside the allowable limits specified by the drawing, purchase order, or contract, the composite article should be separated from acceptable articles, appropriately identified as discrepant, and submitted for material review by the cognizant engineering organization, and dispositioned as (1) acceptable as is, (2) subject to further rework or repair to make the materials or component acceptable, or (3) scrapped when required by contractual documents.5.4.4 Acceptance criteria and interpretation of result should be defined in requirements documents prior to performing the examination. Advance agreement should be reached between the purchaser and supplier regarding the interpretation of the results of the examinations. All discontinuities having signals that exceed the rejection level as defined by the process requirements documents should be rejected unless it is determined from the part drawing that the rejectable discontinuities will not remain in the finished part.5.5 Life Cycle Considerations—The referenced NDT practices and test methods have demonstrated utility in quality assurance of PMCs during the life cycle of the product. The modern NDT paradigm that has evolved and matured over the last twenty–five years has been fully demonstrated to provide benefits from the application of NDT during: (a) product and process design and optimization, (b) on-line process control, (c) after manufacture inspection, (d) in-service inspection, and (e) health monitoring.5.5.1 In-process NDT can be used for feedback process control since all tests are based upon measurements which do not damage the article under test.5.5.2 The applicability of NDT procedures to evaluate PMC materials and components during their life cycle is summarized in Tables 3 and 4.(A) Applicable to composites used in storage and distribution of fluids and gases, for example, filament-wound pressure vessels.5.6 General Geometry and Size Considerations—Part contour, curvature, and surface condition may limit the ability of certain tests to detect imperfections with the desired accuracy.5.7 Reporting—Reports and records should be specified by agreement between purchaser and supplier. It is recommended that any NDT report or archival record contain information, when available, about the material type; method of fabrication; manufacturer’s name; part number; lot; date of lay-up or of cure, or both; date and pressure load of previous tests (for pressure vessels); and previous service history (for in-service and failed composite articles). Forwards and backwards compatibility of data, data availability, criticality (length of data retention), specification change, specification revision and date, software and hardware considerations will also govern how reporting is performed.1.1 This guide provides information to help engineers select appropriate nondestructive testing (NDT) methods to characterize aerospace polymer matrix composites (PMCs). This guide does not intend to describe every inspection technology. Rather, emphasis is placed on established NDT methods that have been developed into consensus standards and that are currently used by industry. Specific practices and test methods are not described in detail, but are referenced. The referenced NDT practices and test methods have demonstrated utility in quality assurance of PMCs during process design and optimization, process control, after manufacture inspection, in-service inspection, and health monitoring.1.2 This guide does not specify accept-reject criteria and is not intended to be used as a means for approving composite materials or components for service.1.3 This guide covers the following established NDT methods as applied to PMCs: Acoustic Emission (AE, Section 7); Computed Tomography (CT, Section 8); Leak Testing (LT, Section 9); Radiographic Testing, Computed Radiography, Digital Radiography, and Radioscopy (RT, CR, DR, RTR, Section 10); Shearography (Section 11); Strain Measurement (Contact Methods, Section 12); Thermography (Section 13); Ultrasonic Testing (UT, Section 14); and Visual Testing (VT, Section 15).1.4 The value of this guide consists of the narrative descriptions of general procedures and significance and use sections for established NDT practices and test methods as applied to PMCs. Additional information is provided about the use of currently active standard documents (an emphasis is placed on applicable standard guides, practices, and test methods of ASTM Committee E07 on Nondestructive Testing), geometry and size considerations, safety and hazards considerations, and information about physical reference standards.1.5 To ensure proper use of the referenced standard documents, there are recognized NDT specialists that are certified in accordance with industry and company NDT specifications. It is recommended that a NDT specialist be a part of any composite component design, quality assurance, in-service maintenance, or damage examination.1.6 This guide summarizes the application of NDT procedures to fiber- and fabric-reinforced polymeric matrix composites. The composites of interest are primarily, but not exclusively, limited to those containing high modulus (greater than 20 GPa (3×106 psi)) fibers. Furthermore, an emphasis is placed on composites with continuous (versus discontinuous) fiber reinforcement.1.7 This guide is applicable to PMCs containing, but not limited to, bismaleimide, epoxy, phenolic, poly(amide imide), polybenzimidazole, polyester (thermosetting and thermoplastic), poly(ether ether ketone), poly(ether imide), polyimide (thermosetting and thermoplastic), poly(phenylene sulfide), or polysulfone matrices; and alumina, aramid, boron, carbon, glass, quartz, or silicon carbide fibers.NOTE 1: Per the discretion of the cognizant engineering organization, composite materials not developed and qualified in accordance with the guidelines in CMH-17, Volumes 1 and 3 should have an approved material usage agreement.1.8 The composite materials considered herein include uniaxial laminae, cross-ply laminates, angle-ply laminates, and sandwich constructions. The composite components made therefrom include filament-wound pressure vessels, flight control surfaces, and various structural composites.1.9 For current and potential NDT procedures for finding indications of discontinuities in the composite overwrap and thin-walled metallic liners in filament-wound pressure vessels, also known as composite overwrapped pressure vessels (COPVs), refer to Guides E2981 and E2982, respectively.1.10 For a summary of the application of destructive ASTM standard practices and test methods (and other supporting standards) to continuous-fiber reinforced PMCs, refer to Guide D4762.1.11 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.12 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.13 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers glass fiber reinforced gypsum (GRG) composites suitable for producing GRG parts for non-loading bearings, thin sections, and ornamental shapes for architectural embellishment of interior building construction. Both the neat alpha gypsum cement and the resulting composite materials should conform to the specified physical and mechanical properties such as hardness, flexural strength, impact resistance, coefficient of linear thermal expansion, humidified deflection, surface burning characteristics, and nail pull resistance.1.1 This specification covers glass fiber reinforced gypsum (GRG) composites having minimum properties and quality suitable to allow the production of GRG parts for non-loading bearing, thin section, ornamental shapes for architectural embellishment of interior building construction.1.2 The values stated in either inch-pound units or SI [metric] are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system shall be independent of the other. Values from the two systems shall not be combined.1.3 The text of this standard references footnotes which provide explanatory material. These footnotes shall not be considered as requirements of the standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is used to determine the time to sustained flaming and heat release of materials and composites exposed to a prescribed initial test heat flux in the cone calorimeter apparatus.5.2 Quantitative heat release measurements provide information that can be used to compare wall or ceiling coverings and constructions and for input to fire models.5.3 Heat release measurements provide useful information for product development by giving a quantitative measure of specific changes in fire performance caused by component and composite modifications.5.4 Heat release data obtained by this test method will be inappropriate if the product will not spread flame over its surface under the fire exposure conditions of interest.5.5 Variations in substrates, mounting methods, and adhesives used to laminate composite products will potentially affect the test responses. These variables must be controlled during any comparative experiments.5.6 Test Limitations—The test data are invalid if any of the following occur:5.6.1 Explosive spalling,5.6.2 The specimen swells sufficiently prior to ignition to touch the spark plug or swells up to the plane of the heater base during combustion, or5.6.3 The surface laminate rolls or curls when placed under the radiant heater.5.7 The specimens are subjected to one or more specific sets of laboratory conditions in this procedure. If different test conditions are substituted or the end-use conditions are changed, it is not always possible by or from this test to predict changes in the fire-test-response characteristics measured. The results are therefore valid only for the fire test exposure conditions described in this procedure.1.1 This fire-test-response test method covers determination of the ignitability and heat release rate of composites consisting of a wall covering or ceiling covering, a substrate, and all laminating adhesives, coatings, and finishes. Heat release information cannot be used alone to evaluate the flammability of wall coverings or ceiling coverings. The data are intended to be used for modeling or with other data to evaluate a material.1.2 This test method provides for measurement of the time to sustained flaming, heat release rate, peak and total heat release, and effective heat of combustion at a constant initial test heat flux of 35 kW/m2. Heat release data at different heat fluxes are also obtained by this test method. The specimen is oriented horizontally, and a spark ignition source is used.1.3 The fire-test-response characteristics are determined using the apparatus and procedures described in Test Method E1354.1.4 The tests are conducted on bench-scale specimens combining the components used in the actual installation.1.5 The values stated in SI units are to be regarded as the standard. See IEEE/ASTM SI-10.1.6 Fire testing of products and materials is inherently hazardous, and adequate safeguards for personnel and property shall be used in conducting these tests. This test method potentially involves hazardous materials, operations, and equipment.1.7 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.8 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests. Specific information about hazard is given in Section 6.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is designed to produce tensile property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors that influence the tensile response and should be reported include the following: material, methods of material preparation and lay-up, specimen stacking sequence, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, time at temperature, and volume percent reinforcement. Properties, in the test direction, which may be obtained from this test method include the following:5.1.1 Ultimate tensile strength,5.1.2 Ultimate tensile strain,5.1.3 Tensile modulus of elasticity, and5.1.4 Poissons ratio.1.1 This test method covers the determination of the tensile properties of metal matrix composites reinforced by continuous and discontinuous high-modulus fibers. Nontraditional metal matrix composites as stated in 1.1.6 also are covered in this test method. This test method applies to specimens loaded in a uniaxial manner tested in laboratory air at either room temperature or elevated temperatures. The types of metal matrix composites covered are:1.1.1 Unidirectional—Any fiber-reinforced composite with all fibers aligned in a single direction. Continuous or discontinuous reinforcing fibers, longitudinal and transverse properties.1.1.2 0°/90° Balanced Crossply—A laminate composed of only 0 and 90° plies. This is not necessarily symmetric, continuous, or discontinuous reinforcing fibers.1.1.3 Angleply Laminate—Any balanced laminate consisting of ± theta plies where theta is an acute angle with respect to a reference direction. Continuous reinforcing fibers without 0° reinforcing fibers (that is, (±45)ns, (±30)ns, and so forth).1.1.4 Quasi-Isotropic Laminate—A balanced and symmetric laminate for which a constitutive property of interest, at a given point, displays isotropic behavior in the plane of the laminate. Continuous reinforcing fibers with 0° reinforcing fibers (that is, (0/±45/90)s, (0/±30)s, and so forth).1.1.5 Unoriented and Random Discontinuous Fibers.1.1.6 Directionally Solidified Eutectic Composites.1.2 The technical content of this standard has been stable since 1996 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this standard, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards. The standard therefore should not be considered to include any significant changes in approach and practice since 1996. Future maintenance of the standard will only be in response to specific requests and performed only as technical support allows.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended primarily for the testing of flat panel composites and sandwich core panels to an acceptance criteria most typically specified in a purchase order or other contractual document.5.2 Basis of Application—There are areas in this practice that require agreement between the cognizant engineering organization and the supplier, or specific direction from the cognizant engineering organization.1.1 This practice establishes two procedures for ultrasonic testing (UT) of flat panel composites and flat sandwich core panels (parallel surfaces). Typical as-fabricated lay-ups include uniaxial, cross ply and angle ply laminates; as well as honeycomb sandwich core materials. These procedures can be used throughout the life cycle of the materials; product and process design optimization, on line process control, after manufacture inspection, and in service inspection. Contact methods such as angle-beam techniques using shear waves, or surface-beam techniques using Lamb waves, are not discussed.1.2 Ultrasonic testing is a common subsurface method for detection of laminar oriented discontinuities. Two techniques can be considered based on panel surface accessibility; pulse echo for one sided and through transmission (bubblers/squirters) for two sided. As used in this practice, both require the use of a pulsed straight-beam ultrasonic longitudinal wave followed by observing indications of either the reflected (pulse-echo) or received (through transmission) wave. The general types of anomalies detected by both techniques include foreign materials, delamination, disbond/un-bond, fiber de-bonding, inclusions, porosity, and voids.1.3 This practice provides two ultrasonic test procedures. Each has its own merits and requirements for inspection and shall be selected as agreed upon in a contractual document.1.3.1 Test Procedure A, Pulse Echo (non-contacting and contacting), is at a minimum a single transducer transmitting and receiving a longitudinal wave in the range of 0.5 to 20 MHz (see Fig. 1). This procedure requires access to only one side of the specimen. This procedure can be conducted by automated or manual means. Automated and manual test results may be imaged or recorded.FIG. 1 Test Procedure A, Pulse Echo Apparatus Set-up1.3.2 Test Procedure B, Through Transmission, is a combination of two transducers. One transmits a longitudinal wave and the other receives the longitudinal wave in the range of 0.5 MHz to 20 MHz (see Fig. 2). This procedure requires access to both sides of the specimen. This procedure is automated and the examination results are recorded.FIG. 2 Test Procedure B, Through Transmission Apparatus Set-up1.4 This practice does not specify accept-reject criteria.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Shearography is commonly used during product process design and optimization, process control, after manufacture inspection, and in service inspection, and can be used to measure static and dynamic axial (tensile and compressive) strain, as well as shearing, Poisson, bending, and torsional strains. The general types of defects detected by shearography include delamination, deformation under load, disbond/unbond, microcracks, and thickness variation.5.2 Additional information is given in Guide E2533 about the advantages and limitations of the shearography technique, use of related ASTM documents, specimen geometry and size considerations, calibration and standardization, and physical reference standards.5.3 For procedures for shearography of filament-wound pressure vessels, otherwise known as composite overwrapped pressure vessels, consult Guide E2982.5.4 Factors that influence shearography and therefore shall be reported include but are not limited to the following: laminate (matrix and fiber) material, lay-up geometry, fiber volume fraction (flat panels); facing material, core material, facing stack sequence, core geometry (cell size); core density, facing void content, and facing volume percent reinforcement (sandwich core materials); processing and fabrication methods, overall thickness, specimen alignment, specimen conditioning, specimen geometry, and test environment (flat panels and sandwich core materials). Shearography has been used with excellent results for composite and metal face sheet sandwich panels with both honeycomb and foam cores, solid monolithic composite laminates, foam cryogenic fuel tank insulation, bonded cork insulation, aircraft tires, elastomeric and plastic coatings. Frequently, defects at multiple and far side bond lines can be detected.1.1 This practice describes procedures for shearography of polymer matrix composites and sandwich core materials made entirely or in part from fiber-reinforced polymer matrix composites. The composite materials under consideration typically contain continuous high modulus (greater than 20 GPa (3 × 106 psi)) fibers, but may also contain discontinuous fiber, fabric, or particulate reinforcement.1.2 This practice describes established shearography procedures that are currently used by industry and federal agencies that have demonstrated utility in quality assurance of polymer matrix composites and sandwich core materials during product process design and optimization, manufacturing process control, after manufacture inspection, and in service inspection.1.3 This practice has utility for testing of polymer matrix composites and sandwich core materials containing but not limited to bismaleimide, epoxy, phenolic, poly(amideimide), polybenzimidazole, polyester (thermosetting and thermoplas- tic), poly(ether ether ketone), poly(ether imide), polyimide (thermosetting and thermoplastic), poly(phenylene sulfide), or polysulfone matrices; and alumina, aramid, boron, carbon, glass, quartz, or silicon carbide fibers. Typical as-fabricated geometries include uniaxial, cross-ply and angle-ply laminates; as well as honeycomb and foam core sandwich materials and structures.1.4 This practice does not specify accept-reject criteria and is not intended to be used as a means for approving polymer matrix composites or sandwich core materials for service.1.5 To ensure proper use of the referenced standards, there are recognized nondestructive testing (NDT) specialists that are certified according to industry and company NDT specifications. It is recommended that an NDT specialist be a part of any composite component design, quality assurance, in-service maintenance, or damage examination activity.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification covers poly(ether ketone ketone) materials, commonly referred to as PEKK, which are suitable for molding, extrusion, composites, powder coating and additive manufacturing. Only materials in this Class 6-8 are covered by this specification. This classification system provides requirements for the use of regrind or reprocessed materials.1.2 This specification covers thermoplastic resin materials supplied in pellet as well as powder form.1.3 This specification applies only to PEKK copolymers, without any additional fillers or inorganic additives, alloys, or treatments for modification of attributes.1.4 This classification system and subsequent line callout (specification) are intended to provide means of calling out poly(ether ketone ketone) materials used in the fabrication of end items or parts.1.5 Poly(ether ketone ketone) (PEKK) is a member of the poly (aryl ether ketone) or PAEK polymer family. PEKK has a broad range of repeat unit combinations of Isophthaloyl and Terephthaloyl repeat units. This standard classifies the polymer options.1.6 The values stated in SI units, as detailed in IEEE/ASTM S-10, are to be regarded as the standard. The values given in parentheses are for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this standard.NOTE 2: PEKK is a thermoplastic polymer. Testing conditions can affect the technical results. Specimens prepared by techniques different than prescribed in this specification can have properties that vary from the values specified.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method can be used to obtain the tensile force capacity and ultimate tensile strain of FRP material used for the strengthening of other structural materials such as, metals, timber, and reinforced concrete. The principal test variables could be the FRP constituents and fabrication method or the size or type of FRP laminate. The obtained tensile properties can be used for material specifications, quality control and assurance, structural design and analysis, and research and development.5.2 This test method focuses on the FRP material itself, irrespective of the gripping method. Therefore, maximum force and strain data associated with failure or pullout at either grip are disregarded. The force capacity and maximum strain measurements are based solely on test specimens that fail in the gauge section.1.1 This test method describes the requirements for sample preparation, tensile testing, and results calculation of flat fiber reinforced polymer (FRP) composite materials used for the strengthening of structures made of materials such as metals, timber, masonry, and reinforced concrete. The method may be used to determine the tensile properties of wet lay-up and pre-impregnated FRP composites fabricated on site or manufactured in a factory setting. The FRP composite may be of either unidirectional (0-degrees) or cross-ply (0/90 type) reinforcement. For cross-ply laminates, the construction may be achieved using multiple-layers of unidirectional fibers at either 0 or 90 degrees, or one or more layers of stitched or woven 0/90 fabrics. The composite material forms are limited to continuous fiber or discontinuous fiber-reinforced composites in which the laminate is balanced and symmetric with respect to the test direction. The method only covers the determination of the tensile properties of the FRP composite material. Other components used to attach the FRP material to the substrate, such as the primer, putty, and adhesive in externally bonded strengthening systems, are excluded from the sample preparation and testing detailed in this document. This test method refers to Test Method D3039/D3039M for conduct of the tests.1.2 The values stated in either SI units or inch-pound units are to be regarded as standard. Within the text, the inch-pound units are shown in brackets. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 This practice covers the procedures for computing material property characteristic values for polymeric composite materials intended for use in civil engineering structural applications. A characteristic value represents a statistical lower bound on the material property structural member resistance factors for civil engineering design codes for composite structures.4.2 This practice may be used to obtain characteristic values for stiffness and strength properties of composite materials obtained from measurements using applicable test methods.1.1 This practice covers the procedures for computing characteristic values of material properties of polymeric composite materials intended for use in civil engineering structural applications. The characteristic value is a statistically-based material property representing the 80 % lower confidence bound on the 5th-percentile value of a specified population. Characteristic values determined using this standard practice can be used to calculate structural member resistance values in design codes for composite civil engineering structures and for establishing limits upon which qualification and acceptance criteria can be based.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is designed to determine the glass transition temperature of continuous fiber reinforced polymer composites using the DMA method. The DMA Tg value is frequently used to indicate the upper use temperature of composite materials, as well as for quality control of composite materials.1.1 This test method covers the procedure for the determination of the dry or wet (moisture conditioned) glass transition temperature (Tg) of polymer matrix composites containing high-modulus, 20 GPa (> 3 × 106 psi), fibers using a dynamic mechanical analyzer (DMA) under flexural oscillation mode, which is a specific subset of the Dynamic Mechanical Analysis (DMA) method.1.2 The glass transition temperature is dependent upon the physical property measured, the type of measuring apparatus and the experimental parameters used. The glass transition temperature determined by this test method (referred to as “DMA Tg”) may not be the same as that reported by other measurement techniques on the same test specimen.1.3 This test method is primarily intended for polymer matrix composites reinforced by continuous, oriented, high-modulus fibers. Other materials, such as neat resin, may require non-standard deviations from this test method to achieve meaningful results.1.4 The values stated in SI units are standard. The values given in parentheses are non-standard mathematical conversions to common units that are provided for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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7.1 The electrical and mechanical characteristics of circuits produced from flexible composites of copper foil with dielectric materials will, to a large extent, depend on the properties of the dielectric portion of the composite. Measurement of these properties is essential for predicting performance of the circuit.1.1 These test methods cover procedures for testing flexible materials consisting of copper foil combined with either dielectric film or with treated or impregnated fabric to form flexible composites used in the manufacture of flexible or multilayer circuitry, or both.1.2 The procedures appear as follows:Procedure Section ASTM Reference MethodConditioning 5  Flex Life of the Composite 20 – 25  Peel Strength of the Composite 11 – 19  Specimen Preparation 6 D1825Strain Relief Due to Etching 26 – 32  Testing of the Dielectric Portion of      the Composite 7 – 10 D1825, D2305, D902  1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is used to determine the time to sustained flaming and heat release of materials and composites exposed to a prescribed initial test heat flux in the cone calorimeter apparatus.5.2 Quantitative heat release measurements provide information that can be used for upholstery and mattress product designs and product development.5.3 Heat release measurements provide useful information for product development by yielding a quantitative measure of specific changes in fire performance caused by component and composite modifications. Heat release data from this test method will not be predictive of product behavior if the product does not spread flame over its surface under the fire exposure conditions of interest.5.4 Test Limitations—The test data are invalid if either of the following conditions occur: (1) explosive spalling; or (2) the specimen swells sufficiently prior to ignition to touch the spark plug, or the specimen swells up to the plane of the heater base during combustion.1.1 This fire-test-response test method can be used to determine the ignitability and heat release from the composites of contract, institutional, or high-risk occupancy upholstered furniture or mattresses using a bench scale oxygen consumption calorimeter.1.2 This test method provides for measurement of the time to sustained flaming, heat release rate, peak and total heat release, and effective heat of combustion at a constant initial test heat flux of 35 kW/m2. This test method is also suitable to obtain heat release data at different heat fluxes. The specimen is oriented horizontally, and a spark ignition source is used.1.3 The times to sustained flaming, heat release, and effective heat of combustion are determined using the apparatus and procedures described in Test Method E1354.1.4 The tests are performed on bench-scale specimens combining the furniture or mattress outer layer components. Frame elements are not included.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.1.8 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Susceptibility to delamination is one of the major design concerns for many advanced laminated composite structures. Knowledge of a laminated composite material’s resistance to interlaminar fracture is useful for product development and material selection. Furthermore, a measurement of the mode II interlaminar fracture toughness that is independent of specimen geometry or method of force introduction is useful for establishing design allowables used in damage tolerance analyses of composite structures. Knowledge of both the non-precracked and precracked toughnesses allows the appropriate value to be used for the application of interest.5.2 This test method can serve the following purposes:5.2.1 To establish quantitatively the effect of fiber surface treatment, local variations in fiber volume fraction, and processing and environmental variables on GIIc of a particular composite material;5.2.2 To compare quantitatively the relative values of GIIc for composite materials with different constituents;5.2.3 To compare quantitatively the values of GIIc obtained from different batches of a specific composite material, for example, to use as a material screening criterion or to develop a design allowable; and5.2.4 To develop delamination failure criteria for composite damage tolerance and durability analyses.1.1 This test method covers the determination of the mode II interlaminar fracture toughness, GIIc, of unidirectional fiber-reinforced polymer matrix composite laminates under mode II shear loading using the end-notched flexure (ENF) test (Fig. 1).FIG. 1 ENF Test Fixture and Specimen Nomenclature1.2 This method is limited to use with composites consisting of unidirectional carbon-fiber- and glass-fiber-reinforced laminates. This limited scope reflects the experience gained in round robin testing. This test method may prove useful for other types and classes of composite materials; however, certain interferences have been noted (see Section 6).1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.3.1 Within the text the inch-pound units are shown in brackets.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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