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This test method was developed to evaluate the wear performance of engine oils in turbocharged and intercooled four-cycle diesel engines. Obtain results from used oil analysis and component measurements before and after test.The test method may be used for engine oil specification acceptance when all details of the procedure are followed.1.1 This test method covers an engine test procedure for evaluating diesel engine oils for performance characteristics, including lead corrosion and wear of piston rings and cylinder liners. This test method is commonly referred to as the Mack T-9.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Annex A5 for specific safety precautions.

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5.1 This test method was developed to provide for the enforcement of 26 CFR 48.4082-1(b), which mandates that all tax-exempt diesel fuels be dyed with an amount of Solvent Red 164 at a concentration that is spectrally equivalent to 3.9 lb/103 bbl (11.1 mg/L) of Solvent Red 26. It is employed to verify that the correct amount of Solvent Red 164 is being added to tax-exempt product at terminals or refineries prior to sale, and to detect the presence of Solvent Red 164 in taxed product intended for on-road use.5.1.1 Solvent Red 26 is the azo dye shown in Fig. 1. It is the standard against which the concentration of Solvent Red 164 is measured because it is available in a certified pure form. Solvent Red 164 is identical in structure to Solvent Red 26 except that it has hydrocarbon (alkyl) chains incorporated to increase its solubility in diesel and burner fuels. The exact composition of Solvent Red 164 will vary from manufacturer to manufacturer and lot to lot depending upon the extent of alkylation that occurs during production; however, its visible spectrum is virtually identical to the spectrum of Solvent Red 26. Solvent Red 164 is employed in the field (instead of Solvent Red 26) to dye tax-exempt diesel and burner fuels because of its higher solubility and relatively low cost.FIG. 1 Structure of Solvent Red 261.1 This test method covers the procedure for determining the concentration of dye Solvent Red 164 in commercially available diesel and burner fuels using visible spectroscopy.NOTE 1: This test method is suitable for all No. 1 and No. 2 grades in Specifications D396 and D975 and for grades DMA and DMB in Specification D2069.1.2 The concentration ranges specified for the calibration standards are established in response to the Internal Revenue Service dyeing requirements which state that tax-exempt diesel fuel satisfies the dyeing requirement only if it contains the dye Solvent Red 164 (and no other dye) at a concentration spectrally equivalent to 3.9 lb of the solid dye standard Solvent Red 26 per thousand bbl (11.1 mg/L) of diesel fuel.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Some fuel dilution of the engine oil may take place during normal operation. However, excessive fuel dilution is of concern in terms of possible performance problems. This method provides a means to determine the magnitude of the fuel dilution, providing the user with the ability to predict performance and to take appropriate action.1.1 This test method covers the use of gas chromatography to determine the amount of diesel fuel in used engine lubricating oil. This test is limited to SAE 30 oil. The diesel fuel diluent is analyzed at concentrations up to 12 % by mass.NOTE 1: This test method may be applicable to higher viscosity grade oils. However, such oils were not included in the program used to develop the precision statement.1.2 This test method is limited to gas chromatographs equipped with flame ionization detectors and temperature programmable ovens.NOTE 2: The use of other detectors and instrumentation has been reported. However, the precision statement applies only when the instrumentation specified is employed.1.3 There is some overlap of the boiling ranges of diesel fuel and SAE 30 engine oils. Moreover, the boiling range of SAE 30 oils from various sources can vary appreciably. As a result, the calibration can be altered by as much as 2 %, in terms of fuel dilution. When testing unknown or mixed brands of used engine oil, it should be realized that the precision of the method may be poorer than the precision obtained when calibrating with a new oil representative of the used oil being tested.1.4 The values stated in SI units are to be regarded as the standard. The values stated in inch-pound units are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory requirements prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The aromatic hydrocarbon content of motor diesel fuels is a factor that can affect their cetane number and exhaust emissions.5.2 The United States Environmental Protection Agency (USEPA) regulates the aromatic content of diesel fuels. California Air Resources Board (CARB) regulations place limits on the total aromatics content and polynuclear aromatic hydrocarbon content of motor diesel fuel, thus requiring an appropriate analytical determination to ensure compliance with the regulations. Producers of diesel fuels will require similar determinations for process and quality control. This test method can be used to make such determinations.5.3 This test method is applicable to materials in the boiling range of motor diesel fuels and is unaffected by fuel coloration. Test Method D1319, which has been mandated by the USEPA for the determination of aromatics in motor diesel fuel, excludes materials with final boiling points greater than 315 °C (600 °F) from its scope. Test Method D2425 is applicable to the determination of both total aromatics and polynuclear aromatic hydrocarbons in diesel fuel, but is much more costly and time consuming to perform.5.4 Results obtained by this test method have been shown to be statistically more precise than those obtained from Test Method D1319 for typical diesel fuels, and this test method has a shorter analysis time.3 Results from this test method for total polynuclear aromatic hydrocarbons are also expected to be at least as precise as those of Test Method D2425.1.1 This test method covers the determination of the total amounts of monoaromatic and polynuclear aromatic hydrocarbon compounds in motor diesel fuels and blend stocks by supercritical fluid chromatography (SFC). The range of aromatics concentration to which this test method is applicable is from 1 % to 75 % by mass. The range of polynuclear aromatic hydrocarbon concentrations to which this test method is applicable is from 0.5 % to 50 % by mass.1.2 This test method includes relative bias for Test Method D5186 versus Test Method D1319 and Test Method D6591 versus Test Method D5186 for diesel fuels. The applicable ranges of the correlation ranges are presented in the Relative Bias section. The correlations are applicable only in the stated ranges and only to diesel fuels.1.3 This test method and correlations were developed for diesel samples not containing biodiesel; the presence of biodiesel will interfere with the results. The correlation equations are only applicable between these concentration ranges and to diesel fuels that do not contain biodiesel.1.4 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Comparison of brake horsepower developed and of specific fuel consumption rates from engine to engine may be made by use of data based upon a standard for composition of an engine assembly.4.2 The purchaser of the engine assembly will be fully advised of the minimum scope of assembly which the purchaser may rightfully expect to be encompassed by a response to a request for quotation and to be delivered in response to a purchase order unless the engine builder in the proposal or in the offer to sell has clearly advised otherwise.4.3 It will be made apparent to the purchaser that additional auxiliary and accessory equipment will be needed to supplement the defined engine assembly when full consideration is given to the application of the engine assembly as a prime mover in a specific vessel.1.1 This guide covers performance and minimum scope of assembly of all medium speed marine diesel engines intended for main propulsion of single or multiple screw propelled marine vessels or for vessels using other than screw propeller-type main propulsion.1.2 This guide is intended to supplement the regulations of legally constituted regulating authorities. In the event of any conflict, which may become apparent after publication of this guide, with such legally constituted regulations, the latter shall take precedence, as may be applicable within the jurisdiction of such authorities and specific to each case, unless such latter regulations are formally waived by proper cognizant authority.1.3 This guide is not intended to relieve the purchaser of the obligation fully to advise the engine builder of all of the purchaser’s unique operational considerations to allow those considerations to be satisfied.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification deals with nationally recognized requirements for the cautionary information to be placed on the label of portable kerosine and diesel containers for consumer use. It is not the intent of this specification to preclude any other labeling requirements, such as those set forth in Federal Hazardous Substances Act (FHSA) or other applicable regulations and standards. Information on warning labels which appear on the containers will help ensure the proper information is being presented to the consumer, concerning methods of handling kerosine and diesel fuels.1.1 This specification establishes nationally recognized requirements for the cautionary information to be placed on the label of portable kerosine and diesel containers for consumer use. It is not the intent of this specification to preclude any other labeling requirements, such as those set forth in Federal Hazardous Substances Act (FHSA) or other applicable regulations and standards.

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5.1 These are accelerated engine oil tests (known as the 1K and 1N test procedures), performed in a standardized, calibrated, stationary single-cylinder diesel engine using either mass fraction 0.4 % sulfur fuel (1K test) or mass fraction 0.04 % sulfur fuel (1N test), that give a measure of (1) piston and ring groove deposit forming tendency, (2) piston, ring and liner scuffing and (3) oil consumption.5.2 The 1K test was correlated with vehicles equipped with certain multi-cylinder direct injection engines used in heavy duty and high speed service prior to 1989, particularly with respect to aluminum piston deposits, and oil consumption, when fuel sulfur was nominally mass fraction 0.4 %. These data are given in Research Report RR:D02-1273.95.3 The 1N test has been used to predict piston deposit formation in four-stroke cycle, direct injection, diesel engines that have been calibrated to meet 1994 U.S. federal exhaust emission requirements for heavy-duty engines operated on fuel containing less than mass fraction 0.05 % sulfur. See Research Report RR:D02-1321.95.4 These test methods are used in the establishment of diesel engine oil specification requirements as cited in Specification D4485 for appropriate API Performance Category oils (API 1509).5.5 These test methods are also used in diesel engine oil development.1.1 These test methods cover the performance of engine oils intended for use in certain diesel engines. They are performed in a standardized high-speed, single-cylinder diesel engine by either the 1K (0.4 % mass fuel sulfur) or 1N (0.04 % mass fuel sulfur) procedure.3 The only difference in the two test methods is the fuel used. Piston and ring groove deposit-forming tendency and oil consumption are measured. Also, the piston, the rings, and the liner are examined for distress and the rings for mobility. These test methods are required to evaluate oils intended to satisfy API service categories CF-4 and CH-4 for 1K, and CG-4 for 1N of Specification D4485.1.2 These test methods, although based on the original Caterpillar 1K/1N procedures,3 also embody TMC information letters issued before these test methods were first published. These test methods are subject to frequent change. Until the next revision of these test methods, TMC will update changes in these test methods by the issuance of information letters which shall be obtained from TMC (see Annex A1 – Annex A4).1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3.1 Exception—Where there is no direct SI equivalent such as screw threads, national pipe threads/diameters, tubing size, or single source equipment specified. Also Brake Specific Fuel Consumption is measured in kilograms per kilowatthour.1.4 The following is the Table of Contents:    SectionIntroduction   1Referenced documents 2Terminology 3Summary of Test Methods 4 5Apparatus 6  General Laboratory Requirements 6.1  Test Engine 6.2  Test Engine Accessories and Parts 6.3Reagents and Materials 7Test Oil Sample Requirements 8Preparation of Apparatus 9  Engine Inspection 9.1  Engine Pre-Test Lubrication System Flush 9.2  Engine Pre-Test Measurements and Inspections 9.3  Engine Assembly 9.4  Pressure Testing of Fuel System Assembly 9.5Calibration of Engine Test Stand 10  General Requirements and Frequency of Calibration 10.1  Runs 10.2  Specified Test Parameters 10.3  Calibration Test Acceptance Criteria 10.4  Action on Rejection of Calibration Test 10.5  Test Numbering 10.6  Reference Oils 10.7  Severity Adjustments 10.8Engine Operating Procedure 11  Engine Run-In 11.1  Cool-Down Procedure 11.2  Warm-Up Procedure 11.3  Operating Conditions and Oil Additions 11.4  Measurement of Oil Consumption 11.5  Sampling Used Oil 11.6  Shutdowns, Lost Time and Off Tolerance Conditions 11.7  Recording of Exhaust Temperature 11.8  Air-Fuel Ratio Measurement 11.9  Recording of Engine Conditions 11.10  Humidity Requirements/Calibration/Measurement 11.11Inspections, Photographs and Measurements 12  Reference to Reporting Form 12.1  Pre-Test Measurements of Engine Parts 12.2  Post-Test Information 12.3  Oil Inspections 12.4Report 13  General Directions 13.1  Electronic Transmission of Test Results (Optional) 13.12  Reporting Calibration Test Results 13.13Precision and Bias 14Keywords 15  ANNEXES  ASTM Test Monitoring Center Organization Annex A1ASTM Test Monitoring Center: Calibration Procedures Annex A2ASTM Test Monitoring Center: Maintenance Activities Annex A3ASTM Test Monitoring Center: Related Information Annex A4Specifications for Test Engine and Engine Build Annex A5Intake Air System Details Annex A6Exhaust System Details Annex A7Cooling System Details Annex A8Oil System Modifications and Instrument Locations Annex A9Other Pressure and Temperature Measurement Locations Annex A10Oil Consumption Linear Regression Method Annex A11Test Fuel Specifications Annex A12Lubrication System, Flush Apparatus and Procedure Annex A13Engine Operating Conditions Annex A14Procedure for Rating Piston and Liner Annex A15Calculation of Percent Offset and Percent Deviation Annex A161K/1N Test Reporting Annex A17Parts List by Part Number (P/N) and Warranty Annex A18Safety Precautions Annex A19  APPENDIXES  Humidity Data Appendix X1Statistical Equations for Mean and Standard Deviation Appendix X2Examples of Forms for Reporting Appendix X3Optional Recording of Oil Pass Limits Appendix X41.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements appear throughout the text. Being engine tests, these test methods do have definite hazards that shall be met by safe practices (see Annex A19 on Safety Precautions).1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1. Scope 1.1 This Standard describes the technical requirements and procedures necessary for the design, performance and testing of new or unused flameproof, diesel-powered, non-rail-bound, self- propelled machines for use in gassy underground mines.

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1. Scope 1.1 This Standard describes the technical requirements and procedures necessary for the design, performance, and testing of new or unused non- rail-bound, diesel-powered, self-propelled machines for use in non-gassy underground mines. 1.2 This

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5.1 In the United States, high sulfur content (defined by the United States Environmental Protection Agency (USEPA)) middle distillate products and diesel fuel used for off-road purposes, other than aviation turbine fuel, are required by government agencies to contain red dye. The dye concentration required to be present in high-sulfur and off-road diesel products is regulated by the United States Environmental Protection Agency and the United States Internal Revenue Service, respectively.5.2 Some fuels that are readily exchanged in the market have a color specification. The color of the base fuel is masked by the presence of the red dye. This test method provides a means of estimating the base color of Number 1 and Number 2 diesel fuel and heating oil in the presence of red dye.5.3 The test method provides a means to indicate conformance to contractual and legal requirements.1.1 This test method covers the determination of the red dye concentration of diesel fuel and heating oil and the estimation of the ASTM color of undyed and red-dyed diesel fuel and heating oil. The test method is appropriate for use with diesel fuel and heating oil of Grades 1 and 2 described in Specifications D396, D975, D2880, and D3699. Red dye concentrations are determined at levels equivalent to 0.1 mg/L to 20 mg/L of Solvent Red 26 in samples with ASTM colors ranging from 0.5 to 5. The ASTM color of the base fuel of red-dyed samples with concentration levels equivalent to 0.1 mg/L to 20 mg/L of Solvent Red 26 is estimated for the ASTM color range from 0.5 to 5. The ASTM color of undyed samples is estimated over the ASTM color range of 0.5 to 5.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Some process catalysts used in petroleum and chemical refining can be poisoned when trace amounts of sulfur bearing materials are contained in the feedstocks. This test method can be used to determine sulfur in process feeds sulfur in finished products, and can also be used for purposes of regulatory control.1.1 This test method covers the determination of total sulfur in liquid hydrocarbons, boiling in the range from approximately 25 °C to 400 °C, with viscosities between approximately 0.2 cSt and 20 cSt (mm2/s) at room temperature.1.2 Three separate interlaboratory studies (ILS) on precision, and three other investigations that resulted in an ASTM research report, have determined that this test method is applicable to naphthas, distillates, engine oil, ethanol, Fatty Acid Methyl Ester (FAME), and engine fuel such as gasoline, oxygen enriched gasoline (ethanol blends, E-85, M-85, RFG), diesel, biodiesel, diesel/biodiesel blends, and jet fuel. Samples containing 1.0 mg/kg to 8000 mg/kg total sulfur can be analyzed (Note 1).NOTE 1: Estimates of the pooled limit of quantification (PLOQ) for the precision studies were calculated. Values ranged between less than 1.0 mg/kg and less than 5.0 mg/kg (see Section 9 and 16.1).1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For warning statements, see 3.1, 7.3, 7.4, Section 8, and 9.1.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Biodiesel is a fuel commodity primarily used as a blending component with diesel fuel. It is important to check the concentration of biodiesel in the diesel fuel in order to make sure it is either not below the minimum allowable limit and or does not exceed the maximum allowable limit.5.2 This test method is applicable for quality control in the production and distribution of diesel fuel and biodiesel blends.1.1 This test method determines fatty acid methyl esters (FAME or biodiesel) in diesel fuel oils. FAME can be quantitatively determined from 1.0 % to 30.0 % by volume. This test method uses linear variable filter (LVF) array based mid-infrared spectroscopy for monitoring FAME concentration.NOTE 1: See Section 6 for a list of interferences that could affect the results produced from this method.1.2 This test method uses a horizontal attenuated total reflectance (HATR) crystal and a univariate calibration.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method provides for the precise measurement of the total sulfur content of samples within the scope of this test method with minimal sample preparation and analyst involvement. The typical time for each analysis is five minutes.4.2 Knowledge of the sulfur content of diesel fuels, gasolines, and refinery process streams used to blend gasolines is important for process control as well as the prediction and control of operational problems such as unit corrosion and catalyst poisoning, and in the blending of products to commodity specifications.4.3 Various federal, state, and local agencies regulate the sulfur content of some petroleum products, including gasoline and diesel fuel. Unbiased and precise determination of sulfur in these products is critical to compliance with regulatory standards.1.1 This test method covers the determination of total sulfur by monochromatic wavelength-dispersive X-ray fluorescence (MWDXRF) spectrometry in single-phase gasoline, diesel fuel, refinery process streams used to blend gasoline and diesel, jet fuel, kerosine, biodiesel, biodiesel blends, and gasoline-ethanol blends.NOTE 1: Volatile samples such as high-vapor-pressure gasolines or light hydrocarbons might not meet the stated precision because of the evaporation of light components during the analysis.1.2 The range of this test method is between the pooled limit of quantitation (PLOQ) value (calculated by procedures consistent with Practice D6259) of 3.2 mg/kg total sulfur and the highest level sample in the round robin, 2822 mg/kg total sulfur.1.3 Samples containing oxygenates can be analyzed with this test method provided the matrix of the calibration standards is either matched to the sample matrices or the matrix correction described in Section 5 or Annex A1 is applied to the results. The conditions for matrix matching and matrix correction are provided in the Interferences section (Section 5).1.4 Samples with sulfur content above 2822 mg/kg can be analyzed after dilution with appropriate solvent (see 5.4). The precision and bias of sulfur determinations on diluted samples has not been determined and may not be the same as shown for neat samples (Section 15).1.5 When the elemental composition of the samples differ significantly from the calibration standards used to prepare the calibration curve, the cautions and recommendation in Section 5 should be carefully observed.1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard information, see 3.1.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers requirements and test methods for materials, dimensions, workmanship, ring stiffness, flattening, joint systems, and a form of marking for polyethylene (PE) pipe of profile wall construction and with bell and spigot, heat fusion, extrusion welded or electrofusion joints for use in gravity flow applications, such as for sewers and drains. The PE profile wall pipe products cover six standard ring stiffness constant (RSC) classifications, namely 40, 63, 100, and 160, 250 and 400. These are referred to as RSC 40, RSC 63, RSC 100, RSC 160, RSC 250 and RSC 400. Referee testing, ring stiffness constant testing, flattening test, and joint tightness test shall be performed to meet the requirements prescribed.This specification establishes nationally recognized performance requirements common to both kerosine and diesel portable containers for reuse by the consumer. Only color and marking are differentiated. The test medium specified for chemical resistance is kerosine due to the more aggressive nature of kerosine on elastomers and other materials of construction. Cautionary standards for handling and disposal of hazardous materials should be observed. Containers containing kerosene should not be opened in the presence of open flame or other sources of ignition. The stability test, handle strength test, drop strength test, hydrostatic pressure test, aging test, permeability test, immersion test, stress cracking test, corrosion resistance test, heat resistance test shall be performed on the container to meet the requirements prescribed.1.1 This specification establishes nationally recognized performance requirements common to both kerosene and diesel portable containers for reuse by the consumer. Only color and marking are differentiated. The test medium specified for chemical resistance is kerosene due to the more aggressive nature of kerosene on elastomers and other materials of construction.1.2 This specification does not include single-trip pre-packaged containers.1.3 This standard is not a fire risk assessment standard, or a fire test standard, but a specification for portable kerosene containers for consumer use.1.4 The following precautionary caveat pertains only to the test method portion, Section 7, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Additional precautionary information is given in Section 6.

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5.1 This test method evaluates the percent viscosity loss for polymer-containing fluids resulting from polymer degradation in the high shear nozzle device. Thermal or oxidative effects are minimized.5.2 This test method is used for quality control purposes by manufacturers of polymeric lubricant additives and their customers.5.3 This test method is not intended to predict viscosity loss in field service in different field equipment under widely varying operating conditions, which may cause lubricant viscosity to change due to thermal and oxidative changes as well as by the mechanical shearing of polymer. However, when the field service conditions, primarily or exclusively, result in the degradation of polymer by mechanical shearing, there may be a correlation between the results from this test method and results from the field.1.1 This test method covers the evaluation of the shear stability of polymer-containing fluids. The test method measures the percent viscosity loss at 100 °C of polymer-containing fluids when evaluated by a diesel injector apparatus procedure that uses European diesel injector test equipment. The viscosity loss reflects polymer degradation due to shear at the nozzle.NOTE 1: Test Method D2603 has been used for similar evaluation of shear stability; limitations are as indicated in the significance statement. No detailed attempt has been undertaken to correlate the results of this test method with those of the sonic shear test method.NOTE 2: This test method uses test apparatus as defined in CEC L-14-A-93. This test method differs from CEC-L-14-A-93 in the period of time required for calibration.NOTE 3: Test Method D5275 also shears oils in a diesel injector apparatus but may give different results.NOTE 4: This test method has different calibration and operational requirements than withdrawn Test Method D3945.NOTE 5: Test Method D7109 is a similar procedure that measures shear stability at both 30 and 90 injection cycles. This test method uses 30 injection cycles only.1.2 The values stated in SI units are to be regarded as the standard.1.2.1 Exception—Non-SI units are provided in parentheses.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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