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This specification covers standard dimensional requirements for glass distillation flasks. It includes general purpose flasks and flasks designed for specific tests especially in the petroleum testing area. Distillation flasks shall be of the following types: Type I and Type II. Type II distilling flasks shall be of the following classes: Class 1; Class 2; Class 3; Class 4; and Class 5.1.1 This specification covers standard dimensional requirements for glass distillation flasks. It includes general purpose flasks and flasks designed for specific tests especially in the petroleum testing area.NOTE 1: For packaging standards, choose among Specifications E920, E1157, and E1133.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Cyanide and hydrogen cyanide are highly toxic. Regulations have been established to require the monitoring of cyanide in industrial and domestic wastes and surface waters.35.2 This test method is applicable for natural waters, industrial wastewaters and effluents.1.1 This test method is used to determine the concentration of total cyanide in an aqueous wastewater or effluent. This test method detects the cyanides that are free (HCN and CN–) and strong-metal-cyanide complexes that dissociate and release free cyanide when refluxed under strongly acidic conditions.1.2 This test method may not be applicable to process solutions from precious metals mining operations.1.3 This procedure is applicable over a range of approximately 2 to 500 μg/L (parts per billion) total cyanide. Higher concentrations can be measured with sample dilution or lower injection volume.1.4 The determinative step of this test method utilizes flow injection with amperometric detection based on Test Method D6888. Prior to analysis, samples must be distilled with a micro-distillation apparatus described in this test method or with a suitable cyanide distillation apparatus specified in Test Methods D2036.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 8.6 and Section 9.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Some fuel dilution of the engine oil may take place during normal operation. However, excessive fuel dilution is of concern in terms of possible performance problems.1.1 This test method covers determination of the amount of dilution in crankcase oils of engines when gasoline has been used as the fuel.NOTE 1: There may be cases in dispute, therefore, the user of this test method is advised to establish whether this method will be accepted. There may be cases where Test Method D3525 results will be set as the referee value.1.2 The values stated in acceptable SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statement, see 6.4, 7.1, and 9.3.

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1.1 This test method covers a procedure for the distillation of creosote and creosote-coal tar solution. Test Methods D38 covers the sampling of wood preservatives prior to testing. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Test Method D2462 for testing for moisture in wool is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable.5.1.1 In case of a dispute arising from differences in reported test results when using Test Method D2462 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative testing to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of the bias. As a minimum, the two parties should take a group of test specimens that are as homogenous as possible and that are from a lot of the type material in question. The test specimens should be assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-Test for unpaired data and an acceptance probability level chosen by the two parties before the test is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in light of the known bias.5.2 This test method is the preferred method for all suitable samples of wool where it is important to obtain a result free from the possible biases, introduced by the conditions discussed in 5.3 and 5.4.5.3 This test method is free from the interferences caused by different conditions of ambient atmosphere such as might affect the results of oven-drying. A slight amount of residual moisture may be retained in a specimen subjected to oven-drying because of the relative humidity of the ambient air; however, the amount of moisture retained may be estimated from published data.35.4 This test method is free from the interference caused by nonaqueous volatile material. Such material, when present, is erroneously measured as moisture by oven-drying methods, the extent of the error depending upon the amount and characteristics of any added oils or finishes.5.5 This test method is relatively cumbersome, time consuming, and costly compared to oven-drying, and is not recommended for routine process control, in-plant evaluations, or for other purposes where a high degree of accuracy is not necessary. The cost of operation can be reduced somewhat by redistilling the used toluene, which is then suitable for reuse without further treatment.5.6 Unlike an oven-drying method, any moisture gained or lost by a specimen after its mass has been determined will appear as a direct error in the final result. Since one of the principal uses of the method is to determine the average moisture present in large lots of wool or wool products exposed to variable atmospheric conditions, numerous laboratory samples and test specimens are common. To avoid errors of the type mentioned above, this procedure includes provisions for stabilizing the sample(s) in the laboratory atmosphere so that, during the time necessary for selecting, weighing, and transferring the specimens to flasks, gain or loss of moisture which cannot be accounted for will be minimized. A further advantage of the stabilizing process is realized in cases where the interest is solely in the average moisture content of the sample, and the actual moisture content within the sample is highly variable. By stabilizing the sample before selecting the specimens, equal precision can be achieved with fewer specimens.1.1 This test method covers the determination of the amount of moisture present in grease wool, scoured wool, carded wool, garnetted wool, wool top and intermediate wool products, and rovings, by distillation with toluene.1.2 Equations are given for calculating the amount of water present as moisture content (as-received basis) and moisture regain (dry fiber) basis. The term that corresponds to the basis used in the calculation and report must always be stated.1.3 This test method is not applicable to material known to contain any steam-distillable, water-soluble matter. If it is suspected that such matter is present, the method should be used with caution.1.4 Xylene or other solvents should not be substituted for toluene as no other solvents have been evaluated for use in this standard.NOTE 1: The determination of moisture in wool by oven-drying is covered in Test Method D1576 and for textile materials in general in Test Methods D2654. A method for sampling wool for the determination of moisture in wool is covered in Practice D2525.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.For specific safety hazard statements, see Section 8.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work on industrial aromatic hydrocarbons and related materials.5.2 This test method gives a broad indication of general purity and can also indicate presence of excessive moisture. It will not differentiate between products of similar boiling range.1.1 This test method covers the distillation of industrial aromatic hydrocarbons and related materials of relatively narrow boiling ranges from 30 to 250°C. Warning—This test method is not applicable for styrene which will exothermically polymerize during the distillation process.1.2 The following applies to all specified limits in this test method: for the purposes of determining conformance to this test method, an observed or calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 6.5.2, 6.6.1, and Section 7.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 Organic chlorides do not occur naturally in crude oil. When present, they result from contamination in some manner, such as disposal of chlorinated solvent used in many dewaxing pipeline or other equipment operations.5.1.1 Uncontaminated crude oil will contain no detectable organic chloride, and most refineries can handle very small amounts without deleterious effects.5.1.1.1 Most trade contracts specify that no organic chloride is present in the crude oil.5.1.2 Several pipelines have set specification limits less than 1 μg/g organic chlorides in the whole crude, and less than 5 μg/g in the light naphtha, based on the yield of naphtha being 20 % of the original sample.5.1.2.1 To ensure less than 1 μg/g organic chloride in the crude oil, the amount measured in the naphtha fraction shall be less than 1/f (where f is the naphtha fraction calculated with Eq 1). For example, a crude oil sample with 1 μg/g of organic chloride but a 10 % yield of naphtha would create a naphtha containing 10 μg/g organic chloride. Further, a crude containing 1 μg/g of organic chloride but a 40 % yield of naphtha would create a naphtha containing 2.5 μg/g organic chloride. Due to the difference in naphtha yields, the impact on refining operations can be significantly different.5.1.2.2 Since crude oil deposits worldwide exhibit different yields of naphtha, the working range of detection for this method shall cover a broad range, possibly as high as 50 μg/g in a naphtha fraction.5.1.3 Organic chloride present in the crude oil (for example, methylene chloride, perchloroethylene, etc.) is usually distilled into the naphtha fraction. Some compounds break down during fractionation and produce hydrochloric acid, which has a corrosive effect. Some compounds survive fractionation and are destroyed during hydro-treating (desulfurization of the naphtha).5.2 Other halides can also be used for dewaxing crude oil; in such cases, any organic halides will have similar impact on the refining operations as the organic chlorides.5.3 Organic chloride species are potentially damaging to refinery processes. Hydrochloric acid can be produced in hydro- treating or reforming reactors and the acid accumulates in condensing regions of the refinery. Unexpected concentrations of organic chlorides cannot be effectively neutralized and damage can result. Organic chlorides are not known to be naturally present in crude oils and usually result from cleaning operations at producing sites, pipelines, or tanks. It is important for the oil industry to have common methods available for the determination of organic chlorides in crude oil, particularly when transfer of custody is involved.1.1 This test method covers the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using distillation and combustion ion chromatography.1.2 This test method involves the distillation of crude oil test specimens to obtain a naphtha fraction prior to chloride determination. The chloride content of the naphtha fraction of the whole crude oil can thereby be obtained. See Section 6 regarding potential interferences.1.3 The test procedure covers the determination of organic chloride in the washed naphtha fraction of crude oil by combustion ion chromatography. Other halides can be determined but are not included in the precision statement of the test method.1.4 The values stated in SI units are to be regarded as standard. The preferred concentration units are micrograms of chloride per gram of sample.1.4.1 Exception—The values given in parentheses are for information only.1.5 Warning—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 590元 / 折扣价： 502 元 加购物车

5.1 This test method is one of a number of tests conducted on a crude oil to determine its value. It provides an estimate of the yields of fractions of various boiling ranges and is therefore valuable in technical discussions of a commercial nature.5.2 This test method corresponds to the standard laboratory distillation efficiency referred to as 15/5. The fractions produced can be analyzed as produced or combined to produce samples for analytical studies, engineering, and product quality evaluations. The preparation and evaluation of such blends is not part of this test method.5.3 This test method can be used as an analytical tool for examination of other petroleum mixtures with the exception of LPG, very light naphthas, and mixtures with initial boiling points above 400 °C.1.1 This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method employs a fractionating column having an efficiency of 14 to 18 theoretical plates operated at a reflux ratio of 5:1. Performance criteria for the necessary equipment is specified. Some typical examples of acceptable apparatus are presented in schematic form. This test method offers a compromise between efficiency and time in order to facilitate the comparison of distillation data between laboratories.NOTE 1: Defined as having a Reid vapor pressure less than 82.7 kPa (12 psi).1.2 This test method details procedures for the production of a liquefied gas, distillate fractions, and residuum of standardized quality on which analytical data can be obtained, and the determination of yields of the above fractions by both mass and volume. From the preceding information, a graph of temperature versus mass % distilled can be produced. This distillation curve corresponds to a laboratory technique, which is defined at 15/5 (15 theoretical plate column, 5:1 reflux ratio) or TBP (true boiling point).1.3 This test method can also be applied to any petroleum mixture except liquefied petroleum gases, very light naphthas, and fractions having initial boiling points above 400 °C.1.4 This test method contains the following annexes and appendixes:1.4.1 Annex A1—Test Method for the Determination of the Efficiency of a Distillation Column,1.4.2 Annex A2—Test Method for the Determination of the Dynamic Holdup of a Distillation Column,1.4.3 Annex A3—Test Method for the Determination of the Heat Loss in a Distillation Column (Static Conditions),1.4.4 Annex A4—Test Method for the Verification of Temperature Sensor Location,1.4.5 Annex A5—Test Method for Determination of the Temperature Response Time,1.4.6 Annex A6—Practice for the Calibration of Sensors,1.4.7 Annex A7—Test Method for the Verification of Reflux Dividing Valves,1.4.8 Annex A8—Practice for Conversion of Observed Vapor Temperature to Atmospheric Equivalent Temperature (AET),1.4.9 Appendix X1—Test Method for Dehydration of a Sample of Wet Crude Oil, and1.4.10 Appendix X2—Practice for Performance Check.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.6 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 10.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is one of a number of tests conducted on heavy hydrocarbon mixtures to characterize these materials for a refiner or a purchaser. It provides an estimate of the yields of fractions of various boiling ranges.5.2 The fractions made by this test method can be used alone or in combination with other fractions to produce samples for analytical studies and quality evaluations.5.3 Residues to be used in the manufacture of asphalt can also be made but may not always be suitable. The long heat soaking that occurs in this test method may alter some of the properties.NOTE 1: While the practice of reblending distillates with residue can be done to produce a lighter residue, it is not recommended because it produces blends with irregular properties.5.4 Details of cutpoints must be mutually agreed upon before the test begins.5.5 This is a complex procedure involving many interacting variables. It is most important that at the time of first use of a new apparatus, its components be checked as detailed in Annex A1 and Annex A2 and that the location of the vapor temperature sensor be verified as detailed in 6.5.3 and Fig. 1.1.1 This test method covers the procedure for distillation of heavy hydrocarbon mixtures having initial boiling points greater than 150 °C (300 °F), such as heavy crude oils, petroleum distillates, residues, and synthetic mixtures. It employs a potstill with a low pressure drop entrainment separator operated under total takeoff conditions. Distillation conditions and equipment performance criteria are specified and typical apparatus is illustrated.1.2 This test method details the procedures for the production of distillate fractions of standardized quality in the gas oil and lubricating oil range as well as the production of standard residue. In addition, it provides for the determination of standard distillation curves to the highest atmospheric equivalent temperature possible by conventional distillation.1.3 The maximum achievable atmospheric equivalent temperature (AET) is dependent upon the heat tolerance of the charge. For most samples, a temperature up to 565 °C (1050 °F) can be attained. This maximum will be significantly lower for heat sensitive samples (for example, heavy residues) and might be somewhat higher for nonheat sensitive samples.1.4 The recommended distillation method for crude oils up to cutpoint 400 °C (752 °F) AET is Test Method D2892. This test method can be used for heavy crude oils with initial boiling points greater than 150 °C (302 °F). However, distillation curves and fraction qualities obtained by these methods are not comparable.1.5 This test method contains the following annexes:1.5.1 Annex A1—Test Method for Determination of Temperature Response Time,1.5.2 Annex A2—Practice for Calibration of Sensors,1.5.3 Annex A3—Test Method for Dehydration of a Wet Sample of Oil,1.5.4 Annex A4—Practice for Conversion of Observed Vapor Temperature to Atmospheric Equivalent Temperature (AET), and1.5.5 Annex A5—Test Method for Determination of Wettage.1.6 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warnings, see 6.5.4.2, 6.5.6.3, 6.9.3, 9.5, 9.7, and A2.3.1.3.1.8 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The distillation (volatility) characteristics of hydrocarbons and other liquids have an important effect on their safety and performance, especially in the case of fuels and solvents. The boiling range gives information on the composition, the properties, and the behavior of the fuel during storage and use. Volatility is the major determinant of the tendency of a hydrocarbon mixture to produce potentially explosive vapors.5.2 The distillation characteristics are equally important for both automotive and aviation gasolines, affecting starting, warm-up, and tendency to vapor lock at high operating temperatures or high altitude, or both. The presence of high boiling point components in these and other fuels can significantly affect the degree of formation of solid combustion deposits.5.3 Volatility, as it affects the rate of evaporation, is an important factor in the application of many solvents, particularly those used in paints.5.4 Distillation limits are often included in petroleum product specifications, in commercial contract agreements, process refinery/control applications, and for compliance to regulatory rules.5.5 This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work on hydrocarbon solvents.5.5.1 This test method gives a broad indication of general purity and can also indicate presence of excessive moisture. It will not differentiate between products of similar boiling range.1.1 This test method covers the procedure for the determination of the distillation characteristics of petroleum products and liquid fuels in the range of 20 °C to 400 °C (68 °F to 752 °F) using miniaturized automatic distillation apparatus.1.2 This test method is applicable to such products as: light and middle distillates, automotive spark-ignition engine fuels, automotive spark-ignition engine fuels containing up to 10 % ethanol, aviation gasolines, aviation turbine fuels, all grades of No. 1 and No. 2 diesel fuels (as described in Specification D975), biodiesel (B100), biodiesel blends up to 30 % biodiesel, special petroleum spirits, pure petrochemical compounds, naphthas, white spirits, kerosenes, furnace fuel oils, and distillate marine fuels.NOTE 1: The up to 10 % by volume ethanol limit in spark ignition engine fuels (E10) was the range used in the supporting interlaboratory studies. Spark ignition engine fuels containing > 10 % by volume ethanol and up to 20 % by volume ethanol (E20) may be analyzed, however the stated precision and bias does not apply.1.3 This test method is designed for the analysis of distillate products; it is not applicable to products containing appreciable quantities of residual material.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The distillation (volatility) characteristics of hydrocarbons and other liquids have an important effect on their safety and performance, especially in the case of fuels and solvents. The boiling range gives information on the composition, the properties, and the behavior of the fuel during storage and use. Volatility is the major determinant of the tendency of a hydrocarbon mixture to produce potentially explosive vapors.5.2 The distillation characteristics are critically important for both automotive and aviation gasolines, affecting starting, warm-up, and tendency to vapor lock at high operating temperature or at high altitude, or both. The presence of high boiling point components in these and other fuels can significantly affect the degree of formation of solid combustion deposits.5.3 Distillation limits are often included in petroleum product specifications, in commercial contract agreements, process refinery/control applications, and for compliance to regulatory rules.5.4 This test method can be applied to contaminated products or hydrocarbon mixtures. This is valuable for fast product quality screening, refining process monitoring, fuel adulteration control, or other purposes including use as a portable apparatus for field testing.5.5 This test method uses an automatic micro distillation apparatus, provides fast results using small sample volume, and eliminates much of the operator time and subjectivity in comparison to Test Method D86.1.1 This test method covers a procedure for determination of the distillation characteristics of petroleum products and liquid fuels having boiling range between 20 °C to 400 °C at atmospheric pressure using an automatic micro distillation apparatus.1.2 This test method is applicable to such products as; light and middle distillates, automotive spark-ignition engine fuels, automotive spark-ignition engine fuels containing up to 20 % ethanol, aviation gasolines, aviation turbine fuels, regular and low sulfur diesel fuels, biodiesel (B100), biodiesel blends up to 20 % biodiesel, special petroleum spirits, naphthas, white spirits, kerosines, burner fuels, and marine fuels.1.3 The test method is also applicable to hydrocarbons with a narrow boiling range, like organic solvents or oxygenated compounds.1.4 The test method is designed for the analysis of distillate products; it is not applicable to products containing appreciable quantities of residual material.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价： 843元 / 折扣价： 717 元 加购物车

This practice covers the vacuum distillation process used to separate solvents from the nonvolatile portions of paints for analysis. The procedure entails adding tricresyl phosphate to a sample of the whole paint and heating the mixture using a silicon oil bath. The distillation is then allowed to proceed for a time before vacuum is applied and then dry air is made to pass through the system to facilitate the removal of any high-boiling solvents present. The apparatus needed for this practice include a custom made apparatus, a vacuum punp, a septum sample vial, and a safety shield. Methylene chloride or acetone, silicone oil, and tricresyl phosphate are used as reagents.1.1 This practice covers a vacuum distillation procedure that separates the solvents from the nonvolatile portion of paints so they may be analyzed.1.2 An alternative procedure for the analysis of solvents in paints is described in Practice D 3271.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

定价： 0元 / 折扣价： 0 元

1.1 This is a general method for the separation by steam distillation and the recovery of solvent and base from bituminous mixtures.1.2 The following safety hazards caveat pertains only to the test methods described in this specification. This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.>

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5.1 The basic test method of determining the boiling range of a petroleum product by performing a simple batch distillation has been in use as long as the petroleum industry has existed. It is one of the oldest test methods under the jurisdiction of ASTM Committee D02, dating from the time when it was still referred to as the Engler distillation. Since the test method has been in use for such an extended period, a tremendous number of historical data bases exist for estimating end-use sensitivity on products and processes.5.2 The distillation (volatility) characteristics of hydrocarbons have an important effect on their safety and performance, especially in the case of fuels and solvents. The boiling range gives information on the composition, the properties, and the behavior of the fuel during storage and use. Volatility is the major determinant of the tendency of a hydrocarbon mixture to produce potentially explosive vapors.5.3 The distillation characteristics are critically important for both automotive and aviation gasolines, affecting starting, warm-up, and tendency to vapor lock at high operating temperature or at high altitude, or both. The presence of high boiling point components in these and other fuels can significantly affect the degree of formation of solid combustion deposits.5.4 Volatility, as it affects rate of evaporation, is an important factor in the application of many solvents, particularly those used in paints.5.5 Distillation limits are often included in petroleum product specifications, in commercial contract agreements, process refinery/control applications, and for compliance to regulatory rules.1.1 This test method covers the atmospheric distillation of petroleum products and liquid fuels using a laboratory batch distillation unit to determine quantitatively the boiling range characteristics of such products as light and middle distillates, automotive spark-ignition engine fuels with or without oxygenates (see Note 1), aviation gasolines, aviation turbine fuels, diesel fuels, biodiesel blends up to 30 % volume, marine fuels, special petroleum spirits, naphthas, white spirits, kerosines, and Grades 1 and 2 burner fuels.NOTE 1: An interlaboratory study was conducted in 2008 involving 11 different laboratories submitting 15 data sets and 15 different samples of ethanol-fuel blends containing 25 % volume, 50 % volume, and 75 % volume ethanol. The results indicate that the repeatability limits of these samples are comparable or within the published repeatability of the method (with the exception of FBP of 75 % ethanol-fuel blends). On this basis, it can be concluded that Test Method D86 is applicable to ethanol-fuel blends such as Ed75 and Ed85 (Specification D5798) or other ethanol-fuel blends with greater than 10 % volume ethanol. See ASTM RR:D02-1694 for supporting data.21.2 The test method is designed for the analysis of distillate fuels; it is not applicable to products containing appreciable quantities of residual material.1.3 This test method covers both manual and automated instruments.1.4 Unless otherwise noted, the values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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