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5.1 Ultrasonic extraction using dilute nitric acid is a simpler and easier method for extracting lead from environmental samples than are traditional digestion methods that employ hot plate or microwave digestion with concentrated acids (3), (5), (7), (8). Hence, ultrasonic extraction may be used in lieu of the more rigorous strong acid/high temperature digestion methods (for example, see Ref (3) and Test Method E1613), provided that the performance is demonstrated using accepted criteria as delineated in Guide E1775.5.2 In contrast with hot plate or microwave digestion techniques, ultrasonic extraction is field-portable, which allows for on-site sample analysis.1.1 This practice covers an ultrasonic extraction procedure for the extraction of lead from environmental samples of interest in lead abatement and renovation (or related) work, for analytical purposes.1.2 Environmental matrices of concern include dry paint films, settled dusts, soils, and air particulates.1.3 Samples subjected to ultrasonic extraction are prepared for subsequent determination of lead by laboratory analytical methods.1.4 This practice includes, where applicable, descriptions of procedures for sample homogenization and weighing prior to ultrasonic extraction.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice may be used to collect dust from carpeted or bare floor surfaces for gravimetric or chemical analysis. The collected sample is substantially unmodified by the sampling procedure.5.2 This practice provides for a reproducible dust removal rate from level loop and plush carpets, as well as bare floors. It has the ability to achieve relatively constant removal efficiency at different loadings of floor dust.5.3 This practice also provides for the efficient capture of semivolatile organic chemicals associated with the dust. The test system can be fitted with special canisters downstream of the cyclone for the capture of specific semivolatile organic chemicals that may volatilize from the dust particles during collection.5.4 This practice does not describe procedures for evaluation of the safety of floor surfaces or the potential human exposure to floor dust. It is the user's responsibility to evaluate the data collected by this practice and make such determinations in the light of other available information.5.5 This practice provides per-event dust chemical concentration and chemical loading. Advantages and trade-offs of different sampling approaches have been discussed (7).5.6 This practice uses a removable, cleanable dropout jar that facilitates per-event sampling. Other per-event vacuum attachments are commercially available. These are not directly comparable with composite sampling done using whole vacuum cleaner bags.1.1 This practice covers a procedure for the collection of a sample of dust from carpets and bare floors that can be analyzed for inorganic metals such as lead and organic compounds such as pesticides and other semi-volatile organic compounds (SVOCs).1.2 This practice is applicable to a variety of carpeted and bare floor surfaces. It has been tested for level loop and plush pile carpets and bare wood floors, specifically. This practice is not applicable to elevated, non-floor surfaces.1.3 This practice is not intended for the collection and evaluation of dust for the presence of asbestos fibers.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This practice describes use of a sampling device, the High-Volume Small Surface Sampler (HVS3). Other event-based sampling devices that use commercially available vacuum attachments are not in scope. Composite sampling using whole vacuum cleaner bags is not in scope. Other approaches for floor or non-floor surface sampling (Practices D6966, D6661, D7144) are not within the scope.1.6 This practice only applies to the HVS3. Other dust sampling methods may or may not be directly comparable. Method evaluation for other dust sampling approaches is encouraged. This could be done by comparison with methods outlined in this standard practice for HVS3 or through independent evaluation using field spikes and certified reference materials.1.7 This practice provides information on dust loading, chemical dust concentration, and chemical dust loading. Information on the type of floor, the floor surface area sampled, and amount of dust collected is required (see Fig. 2). Cleaning the vacuum attachments in between sampling events is also required (see Section 13).1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The test is designed to quantify the amount of dust control material added to calcined coke. The dust control material is applied to calcined coke to help maintain a dust-free environment. It generally serves no other useful purpose. It adds mass to the coke and can have a negative effect on the quality of carbon and graphite artifacts made from the treated coke. For these reasons the coke customer wants to know the amount of dust control material on the coke and can specify a maximum level.1.1 This test method covers the determination of the amount of material applied to calcined coke to control dust associated with coke handling and transportation.1.2 This test method is limited to those materials that are soluble in a solvent that can be used in a Soxhlet extraction type of apparatus such as methylene chloride (dichloro-methane).NOTE 1: Methylene chloride is the most popular solvent for removing dust control oil at the time this procedure is being written. Toluene and methyl chloroform, however, have been used with equal results on all cokes tested which have included only those sprayed with aromatic or waxy materials.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended for the collection of settled dust samples for the subsequent measurement of beryllium and compounds. The practice is meant for use in the collection of settled dust samples that are of interest in clearance, hazard evaluation, risk assessment, and other purposes.5.2 This practice is intended solely for the collection of settled dust samples from hard, relatively smooth nonporous surfaces that may be compromised by water or other wetting agents and that are therefore not suitable for wet wipe sampling using Practice D6966 or micro-vacuum sampling using Practice D7144. Use of this practice for any purpose other than the intended purpose is discouraged due to the limited collection efficiency and high variability of dry wipe sampling as compared to wetted wipe or micro-vacuum sampling.35.3 This practice is less effective for collecting settled dust samples from surfaces with substantial texture such as rough concrete, brickwork, textured ceilings, and soft fibrous surfaces such as upholstery and carpeting. Micro-vacuum sampling using Practice D7144 may be more suitable for these surfaces.1.1 This practice covers the collection of settled dust containing beryllium and beryllium compounds on surfaces using the dry wipe sampling method, or both. These samples are collected in a manner that will permit subsequent extraction and determination of beryllium and compounds in the wipes using laboratory analysis techniques such as atomic spectrometry or fluorescence detection.1.2 This practice is limited in its scope to applications where wetted wipe sampling (using Practice D6966) or vacuum sampling (using Practice D7144) is not physically feasible (for example, if the surface to be wiped would be compromised by use of wetted wipes).1.3 This practice does not address the sampling design criteria (that is, sampling plan which includes the number and location of samples) that are used for clearance, hazard evaluation, risk assessment, and other purposes. To provide for valid conclusions, sufficient numbers of samples should be obtained as directed by a sampling plan. Additional guidance is provided in Guide D7659.1.4 This practice contains notes that are explanatory and are not part of the mandatory requirements of this practice.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Ingression protection classifications are widely used by manufacturers for specifying the level of protection offered by enclosures.5.2 An example of such a classification scheme is IEC 60529. Membrane switch manufacturers are often asked to meet these standards, however the test methods specified within these standards do not address considerations specific to membrane switches.5.3 The MSIP classification system considers the membrane switch separately from the testing and IP codes used for classifying the enclosure when subject to similar test conditions.5.4 Ingression testing can be useful to identify design deficiencies.1.1 This guide establishes a classification system and references test methods for verifying the degrees of:1.1.1 The ingress of dust into the internal layers of a membrane switch.1.1.2 Ingress of water into the internal layers of a membrane switch.1.1.3 Where external test methods are referenced, this guide specifies the special conditions that shall be considered in applying these tests to membrane switches and how the results are interpreted.1.2 This guide references test methods that can be used to establish the ingress classification of a membrane switch.1.3 This guide utilizes the test methods and reporting structure of IEC 60529 – (Degrees of Protection Provided by Enclosures) modified for membrane switches.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended for the collection of settled dust samples in and around buildings and related structures for the subsequent determination of lead content in a manner consistent with that described in the HUD Guidelines and 40 CFR 745.63. The practice is meant for use in the collection of settled dust samples that are of interest in clearance, hazard assessment, risk assessment, and other purposes.5.2 Use of different pressures applied to the sampled surface along with the use of different wiping patterns contribute to collection variability. Thus, the sampling result can vary between operators performing collection from identical surfaces as a result of collection variables. Collection for any group of sampling locations at a given sampling site is best when limited to a single operator.5.3 This practice is recommended for the collection of settled dust samples from hard, relatively smooth, nonporous surfaces. This practice is less effective for collecting settled dust samples from surfaces with substantial texture such as rough concrete, brickwork, textured ceilings, and soft fibrous surfaces such as upholstery and carpeting.1.1 This practice covers the collection of settled lead-containing dust on surfaces using the wipe sampling method. These samples are collected in a manner that will permit subsequent extraction (see Practices E1644 and E1979) and determination of lead using laboratory analysis techniques such as atomic spectrometry (see Test Methods E3193/E3193M and E3203) or electroanalysis (see Practice E2051). For collection of settled dust samples for determination of lead and other metals, use Practice D6966.1.2 This practice does not address the sampling design criteria (that is, sampling plan which includes the number and location of samples) that are used for clearance (see Practices E2271/E2271M and E3074/E3074M), lead hazard evaluation, or risk assessment (see Guide E2115), and other purposes. To provide for valid conclusions, sufficient numbers of samples should be obtained as directed by a sampling plan.1.3 This practice contains notes that are explanatory and are not part of the mandatory requirements of this practice.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D520-00(2019) Standard Specification for Zinc Dust Pigment Active 发布日期 :  1970-01-01 实施日期 : 

This specification covers three types of zinc dust, for use as a pigment in paints. The pigments shall consist substantially of metallic zinc and shall conform to the requirements for composition prescribed. The total and metallic zinc shall be shall be tested to meet the requirements prescribed. Lead, cadmium, and iron shall be tested to meet the requirements prescribed. Oily or fatty matter, or both shall, and the coarse particle shall be tested to meet the requirements prescribed.1.1 This specification covers three types of zinc dust, for use as a pigment in paints.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods compile procedures which can be used to check the composition of purity of metallic zinc powder. This information is useful to both the formulator and users.1.1 These test methods cover procedures for the chemical analysis of metallic zinc powder in the form commercially known as zinc dust for use as a pigment in paints.1.2 The analytical procedures appear in the following order:  SectionsMoisture and Other Volatile Matter 7Coarse Particles 8Matter Soluble in Hexane 9 and 10Total Zinc 11 and 12Metallic Zinc 13 and 14Zinc Oxide 15Calcium 16 and 17Lead 18Iron 19Cadmium 20Chlorine 21 and 22Sulfur 23 and 241.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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