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4.1 pH is, within the limits described in 1.1, an accurate measurement of the hydrogen ion concentration and thus is widely used for the characterization of aqueous solutions.4.2 pH measurement is one of the main process control variables in the chemical industry and has a prominent place in pollution control.1.1 This test method specifies the apparatus and procedures for the electrometric measurement of pH values of aqueous solutions with the glass electrode. It does not deal with the manner in which the solutions are prepared. pH measurements of good precision can be made in aqueous solutions containing high concentrations of electrolytes or water-soluble organic compounds, or both. It should be understood, however, that pH measurements in such solutions are only a semiquantitative indication of hydrogen ion concentration or activity. The measured pH will yield an accurate result for these quantities only when the composition of the medium matches approximately that of the standard reference solutions. In general, this test method will not give an accurate measure of hydrogen ion activity unless the pH lies between 2 and 12 and the concentration of neither electrolytes nor nonelectrolytes exceeds 0.1 mol/L (M).1.2 The values stated in SI units are to be regarded as standard. The values in parentheses are for information only.1.3 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Coefficients of linear thermal expansion are used for design and quality control purposes and to determine dimensional changes of parts and components (such as carbon anodes, cathodes, and so forth) when subjected to varying temperatures.1.1 This test method covers the determination of the coefficient of linear thermal expansion (CTE) for carbon anodes and cathodes used in the aluminum industry, in baked form, by use of a vitreous silica dilatometer.1.2 The applicable temperature range for this test method for research purposes is ambient to 1000 °C. The recommended maximum use temperature for product evaluation is 500 °C.1.3 This test method and procedure is based on Test Method E228, which is a generic all-encompassing method. Specifics dictated by the nature of electrode carbons and the purposes for which they are used are addressed by this procedure.1.4 Electrode carbons in the baked form will only exhibit primarily reversible dimensional changes when heated.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method permits measurement of the fluorine content of coal and coke for the evaluation of potential fluorine emission from coal combustion or conversion processes. When coal samples are combusted in accordance with this test method, the fluorine is quantitatively released from the coal and retained in the pyrohydrolysate so that it is representative of the total fluorine concentration in coal.1.1 This test method covers the analysis of total fluorine in coal and coke.1.2 This analysis was successfully tested on coals containing 37 % ash or less (see AS 1038.10.4 and Conrad2).1.3 The values stated in SI units shall be regarded as standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Note 4.1.5 All accountability and quality control aspects of Guide D4621 apply to this test method.

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5.1 This test method is used to ascertain whether or not materials meet specifications for plutonium concentration or plutonium mass fraction.5.1.1 The materials (nuclear grade plutonium nitrate solutions, plutonium metal, plutonium oxide powder, and mixed oxide and carbide powders and pellets) to which this test method applies are subject to nuclear safeguards regulations governing their possession and use. However, adherence to this test method does not automatically guarantee regulatory acceptance of the resulting safeguards measurements. It remains the sole responsibility of the user of this test method to ensure that its application to safeguards has the approval of the proper regulatory authorities.5.1.2 When used in conjunction with appropriate certified reference materials (CRMs), this test method can demonstrate traceability to the international measurements system (SI).5.2 Fitness for Purpose of Safeguards and Nuclear Safety Application—Methods intended for use in safeguards and nuclear safety applications shall meet the requirements specified by Guide C1068 for use in such applications.5.3 A chemical calibration of the coulometer is necessary for accurate results.FIG. 1 Example of a Cell Design Used at Los Alamos National Laboratory (LANL)1.1 This test method covers the determination of milligram quantities of plutonium in unirradiated uranium-plutonium mixed oxide having a U/Pu ratio range of 0.1 to 10. This test method is also applicable to plutonium metal, plutonium oxide, uranium-plutonium mixed carbide, various plutonium compounds including fluoride and chloride salts, and plutonium solutions.1.2 The recommended amount of plutonium for each aliquant in the coulometric analysis is 5 mg to 10 mg. Precision worsens for lower amounts of plutonium, and elapsed time of electrolysis becomes impractical for higher amounts of plutonium.1.3 The quantity values stated in SI units are to be regarded as standard. The quantity values with non-SI units are given in parentheses for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The critical level of hydrogen in steels is that hydrogen which can build up to high concentrations at points of high triaxial stress causing embrittlement of the steel which can lead to catastrophic damage. This hydrogen can enter by various means, such as during pickling and electroplating. Means of reducing this hydrogen during processing are given in Specification B766 and Practices B183 and B242. It is still necessary, however, to know how effective these methods are. Though the ultimate reason for measuring this hydrogen is to relate it to embrittlement, this is not within the scope of this test method. As susceptibility to hydrogen embrittlement is a function of alloy type, heat treatment, intended use,and so forth, the tolerance for hydrogen must be determined by the user according to Method F519.4.2 Though the actual hydrogen concentration is not determined in this test method, the current densities have been shown to be useful as an indication of relative hydrogen concentrations (1-3),3 and therefore the degree of hydrogen embrittlement (1,2). Thus, measurements can be compared to one another (see 4.1 and 7.1).4.3 This test method is applicable as a quality control tool for processing (such as to monitor plating and baking) or to measure hydrogen uptake caused by corrosion.4.4 This test method is nondestructive; however, if there is a coating, it must be removed by a method which has been demonstrated to neither damage the steel nor introduce hydrogen to make the measurement.4.5 This test method is also applicable to situations producing continuous hydrogen permeation, such as high pressure hydrogen cylinders or corrosion processes. The results, however, would require a different treatment and interpretation (4).4.6 This test method is also applicable to small parts, such as fasteners. The technique, procedure, and interpretation would, however, have to be altered.4.7 Use of this test method on austenitic stainless steels and other face centered cubic (FCC) alloys would require different measurement times and interpretation of results because of differing kinetics.4.8 This test method can be used on slightly curved surfaces as long as the gasket defines a reproducible area. The area calculation must, however, be changed.1.1 This test method covers the procedure for measuring diffusible hydrogen in steels by an electrochemical method.1.2 This test method is limited to carbon or alloy steels, excluding austenitic stainless steels.1.3 This test method is limited to flat specimens to which the cell can be attached (see 4.6 and 4.8).1.4 This test method describes testing on bare or plated steel after the plate has been removed (see 4.4).1.5 This test method is limited to measurements at room temperature, 20 to 25°C (68 to 77°F).1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers drawn, soft annealed round copper electrode wire used in welding machines for the purpose of seam welding of cans. It does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this specification to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.1 This specification covers the requirements for drawn, soft annealed round copper electrode wire used in welding machines for the purpose of seam welding of cans.1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The purpose of this test method is to measure the total chlorine content of coal. The chlorine content of coals may be useful in the evaluation of slagging problems, corrosion in engineering processes, and in the total analysis of coal and coke. When coal samples are combusted in accordance with this method, the chlorine is quantitatively retained and is representative of the total chlorine content of the whole coal.1.1 This test method covers the analysis of total chlorine in coal.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Electrical equipment has the potential to fail as a result of electrical tracking of insulating material that is exposed to various contaminating environments and surface conditions. A number of ASTM and other tests have been designed to quantify behavior of materials, especially at relatively high voltages. This method is an accelerated test which, at relatively low test voltages, provides a comparison of the performance of insulating materials under wet and contaminated conditions. The Tracking Index-Copper Electrodes test is not related directly to the suitable operating voltage in service.5.2 When organic electrical insulating materials are subjected to conduction currents between electrodes on their surfaces, many minute tree-like carbonaceous paths or tracks are developed near the electrodes. These tracks are oriented randomly, but generally propagate between the electrodes under the influence of the applied potential difference. Eventually a series of tracks spans the electrode gap, and failure occurs by shorting of the electrodes.5.3 As in other tracking test methods, for example, IEC 60112 and Test Method D3638, this test method specifies test procedures that are intended to promote the formation of surface discharges which will produce carbon tracks in a reproducible manner. Since these conditions rarely reproduce the actual conditions encountered in service, the results of tracking tests cannot be used to infer either direct or relative service behavior of a material in a specific design application. Tracking tests can be used for screening purposes only. Suitability is verified through testing of the material in actual end use or under conditions that closely simulate actual end use.5.4 The use of copper electrodes in this type of test was developed at the University of Cincinnati, NEMA laboratory. It is felt by the members of the Industrial Laminates Section of NEMA that using copper electrodes gives a more realistic value for a tracking index, related to the resin system used to reinforce the substrate of a laminate. In general, tracking tests made with copper electrodes tend to give lower values than platinum electrodes in the same type of test. It is a fact that copper is more widely used than platinum for electrical conductors.51.1 This test method was developed using copper electrodes to evaluate the low-voltage (up to 600 V) tracking resistance of materials in the presence of aqueous contaminants.2NOTE 1: At this time, only industrial laminates have been examined using this method, which was developed at the National Manufacturers Electrical Association (NEMA) laboratory located at the University of Cincinnati. It was found that a closer end point (less scatter) was obtained than with platinum electrodes, and materials tested tended to be ranked by resin system.1.1.1 It is acceptable to consider other electrode materials for use with this test method depending upon the application of the insulating material.1.2 This test method is similar to Test Method D3638, which determines the comparative tracking index of materials using platinum electrodes to produce the tracking on the specimen surface.1.3 The values stated in metric (SI) units are the standard. The inch-pound equivalents of the metric units are approximate.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Used Lubricating Oil—The determination of debris in used oil is a key diagnostic method practiced in machine condition monitoring programs. The presence or increase in concentration of specific wear metals can be indicative of the early stages of wear if there are baseline concentration data for comparison. A marked increase in contaminant elements can be indicative of foreign materials in the lubricants, such as antifreeze or sand, which may lead to wear or lubricant degradation. The test method identifies the metals and their concentration so that trends relative to time or distance can be established and corrective action can be taken prior to more serious or catastrophic failure.1.1 This test method covers the determination of wear metals and contaminants in used lubricating oils and used hydraulic fluids by rotating disc electrode atomic emission spectroscopy (RDE-AES).1.2 This test method provides a quick indication for abnormal wear and the presence of contamination in new or used lubricants and hydraulic fluids.1.3 This test method uses oil-soluble metals for calibration and does not purport to relate quantitatively the values determined as insoluble particles to the dissolved metals. Analytical results are particle size dependent and low results may be obtained for those elements present in used oil samples as large particles.1.4 The test method is capable of detecting and quantifying elements resulting from wear and contamination ranging from dissolved materials to particles approximately 10 μm in size.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5.1 The preferred units are mg/kg (ppm by mass).1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This PDF includes GI #2. 1. Scope This Standard applies to (a) electrode receptacles and fittings for mounting gas tubes intended for indoor and outdoor applications operating at voltages of 15 000 V and less but not exceeding 7 500 V to ground for

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5.1 A major factor affecting the life of insulating materials is thermal degradation. Other factors, such as moisture and vibration, are able to cause failures after the material has been weakened by thermal degradation.5.2 Electrical insulation is effective in electrical equipment only as long as it retains its physical and electrical integrity. Thermal degradation is able to be characterized by weight change, porosity, crazing, and generally a reduction in flexibility, and is usually accompanied by an ultimate reduction in dielectric breakdown voltage.1.1 This test method provides a procedure for evaluating thermal endurance of flexible sheet materials by determining dielectric breakdown voltage at room temperature after aging in air at selected elevated temperatures. Thermal endurance is expressed in terms of a temperature index.1.2 This test method is applicable to such solid electrical insulating materials as coated fabrics, dielectric films, composite laminates, and other materials where retention of flexibility after heat aging is of major importance (see Note 4).1.3 This test method is not intended for the evaluation of rigid laminate materials nor for the determination of thermal endurance of those materials which are not expected or required to retain flexibility in actual service.1.4 The values stated in acceptable metric units are to be regarded as the standard. The values in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see 10.1.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The ER of a battery separator is a standard measurement used by separator and battery manufacturers for quality control purposes and separator selection.5.2 Separator ER and the separator's interaction with the electrolyte, that is resistance to wetting or flow, will contribute to the internal resistance of the battery and this has the potential to limit the electrical output of a battery. The ER determination is a tool for battery manufacturers to use in design, material selection, and performance specifications.5.3 The change in the bath electrical resistance imparted by a separator is affected by the porosity, thickness, and tortuousity of the pore structure of the separator, the wettability of the separator to the electrolyte, and the temperature and concentration of the electrolyte.5.4 Incomplete wetting or saturation of the pore structure limits the lowest ER value obtainable from a separator structure. Separators are pretreated to assure that the specimen being tested has been adequately wetted out. A separator that is not fully wetted out (saturated) will give a higher ER.5.5 This test method is intended to give a rapid and repeatable measurement that approximates the change in ER that could happen when the separator is used in a battery.1.1 This test method covers the pretreatment, test conditions, apparatus, and procedure to determine the ionic resistivity, commonly referred to in the battery industry as electrical resistance (ER) of an alkaline battery separator immersed in an electrolyte of 40 % potassium hydroxide (KOH).1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Selection of corrosion inhibitor for oil field and refinery applications involves qualification of corrosion inhibitors in the laboratory (see Guide G170). Field conditions should be simulated in the laboratory in a fast and cost-effective manner (1).35.2 Oil field corrosion inhibitors should provide protection over a range of flow conditions from stagnant to that found during typical production conditions. Not all inhibitors are equally effective over this range of conditions so that is important for a proper evaluation of inhibitors to test the inhibitors using a range of flow conditions.5.3 The RCE is a compact and relatively inexpensive approach to obtaining varying hydrodynamic conditions in a laboratory apparatus. It allows electrochemical methods of estimating corrosion rates on the specimen and produces a uniform hydrodynamic state across the metal test surface. (2-21)5.4 In this practice, a general procedure is presented to obtain reproducible results using RCE to simulate the effects of different types of coupon materials, inhibitor concentrations, oil, gas and brine compositions, temperature, pressure, and flow. Oil field fluids may often contain sand. This practice does not cover erosive effects that occur when sand is present.1.1 This practice covers a generally accepted procedure to use the rotating cylinder electrode (RCE) for evaluating corrosion inhibitors for oil field and refinery applications in defined flow conditions.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The resistivity of the surrounding soil environment is a factor in the corrosion of underground structures. High resistivity soils are generally not as corrosive as low resistivity soils. The resistivity of the soil is one of many factors that influence the service life of a buried structure. Soil resistivity may affect the material selection and the location of a structure.55.2 Soil resistivity is of particular importance and interest in the corrosion process because it is basic in the analysis of corrosion problems and the design of corrective measures.5.3 The test method is focused to provide an accurate, expeditious measurement of soil resistivity to assist in the determination of a soil’s corrosive nature. Test Method G57 emphasizes an in situ measurement commonly utilized in the design of a buried structures’ corrosion control (cathodic protection systems’ ground bed design, and so forth), but also includes information and procedures on a four-pin soil box method. The two-electrode soil box method is an accurate and more expeditious method than the four-pin soil box and often complements the four-pin, in situ soil resistivity method.5.4 The saturated soil resistivity determined by this test method does not necessarily indicate the minimum soil resistivity.1.1 This test method covers the equipment and procedures for the measurement of soil resistivity, for soil samples removed from the ground, for use in the assessment and control of corrosion of buried structures.1.2 Procedures allow for this test method to be used in the field or in the laboratory.1.3 The test method procedures are for the resistivity measurement of soil samples in the saturated condition and in the as-received condition.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. Soil resistivity values are reported in ohm-centimeter.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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