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ASTM D4127-18a Standard Terminology Used with Ion-Selective Electrodes Active 发布日期 :  1970-01-01 实施日期 : 

1.1 This terminology covers those terms recommended by the International Union of Pure and Applied Chemistry (IUPAC),2 and is intended to provide guidance in the use of ion-selective electrodes for analytical measurement of species in water, wastewater, and brines.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The capability of this test method to collect and quantitate both particulate and gaseous fluorides over the ranges normally encountered in industrial atmospheres makes it applicable for industrial hygiene evaluation and control purposes. The recommended range of this test method is from 0.005 to 5 mg F−/m3 air.1.1 This test method covers the simultaneous collection and separate measurements of gaseous fluoride (for example, hydrogen fluoride) and particulate fluoride found in certain industrial workplaces. The gaseous fluorides and particulate fluorides collected are reported in terms of fluoride. The method covers sample collection, preparation, and fluoride measurement.1.2 The procedure is not applicable to the collection or analysis of gaseous fluoro compounds (for example, fluorocarbon or fluorosulfur compounds).1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 The dielectric breakdown voltage is a measure of the ability of an insulating liquid to withstand electrical stress. The power-frequency breakdown voltage of a liquid is reduced by the presence of contaminants such as cellulosic fibers, conducting particles, dirt, and water. A low result in this test method indicates the presence of significant concentrations of one or more of these contaminants in the liquid tested. See Appendix X1.3.2 A high breakdown voltage measured in this test method does not necessarily indicate that the amount of the contaminants present in a liquid from which the sample was taken is sufficiently low for the sampled liquid to be acceptable in all electrical equipment. Test Method D877 is not sensitive to low levels of these contaminants. Breakdown in this test method is dominated by events occurring at the electrode edges. The voltage stress distribution between the parallel disk electrodes used in this test method are quasi-uniform and there is substantial stress concentration at the sharp edges of the flat disk faces.3.3 This test method may be used for evaluation of insulating liquids in equipment that is designed to be filled with unprocessed liquids as delivered by a vendor.3.4 This test method is not recommended for evaluation of the breakdown voltage of liquids used in equipment that requires the application of vacuum and filtering of the oil before being placed into service. Test Method D1816 should be used to determine the breakdown voltage of filtered and degassed liquids.3.5 This test method is used in laboratory or field tests. For field breakdown results to be comparable to laboratory results, all criteria including room temperature (20 to 30 °C) must be met.1.1 This test method describes two procedures, A and B, for determining the electrical breakdown voltage of insulating liquid specimens. The breakdown test uses ac voltage in the power-frequency range from 45 to 65 Hz.1.2 This test method is used to determine the electrical discharge voltage of in-use electrical liquids. It is no longer applicable to new insulating liquids upon receipt, in which case Test Method D1816 shall be used.NOTE 1: It is understood that long-term histories for this test method exist, but this test method is no longer considered applicable as numerous deficits exist that affect its usefulness. It is recommended to move all new and in-service electrical discharge voltage testing of electrical insulating liquids to Test Method D1816.1.3 Limitations of the Procedures: 1.3.1 The sensitivity of this test method to the general population of contaminants present in a liquid sample decreases as applied test voltages used in this test method become greater than approximately 25 kV rms.1.3.2 If the concentration of water in the sample at room temperature is less than 60 % of saturation, the sensitivity of this test method to the presence of water is decreased. For further information refer to RR:D27-1006.21.3.3 The suitability for this test method has not been determined for a liquid's viscosity higher than 900 cSt at 40 °C.1.4 Procedure Applications 1.4.1 Procedure A: 1.4.1.1 Procedure A is used to determine the breakdown voltage of liquids in which any insoluble breakdown products easily settle during the interval between the required repeated breakdown tests. These liquids include petroleum oils, hydrocarbons, natural and synthetic esters, and askarels (PCB) used as insulating and cooling liquids in transformers, cables, and similar apparatus.1.4.1.2 Procedure A may be used to obtain the dielectric breakdown of silicone fluid as specified in Test Methods D2225, provided the discharge energy into the sample is less than 20 mJ (milli joule) per breakdown for five consecutive breakdowns.1.4.2 Procedure B: 1.4.2.1 This procedure is used to determine the breakdown voltage of liquids in which any insoluble breakdown products do not completely settle from the space between the disks during the 1-min interval required in Procedure A. Procedure B, modified in accordance with Section 17 of Test Methods D2225, is acceptable for testing silicone dielectric liquids if the requirements of 1.4.1.2 can not be achieved.1.4.2.2 Procedure B should also be applied for the determination of the breakdown voltage of liquid samples containing insoluble materials that settle from the specimen during testing. These may include samples taken from circuit breakers, load tap changers, and other liquids heavily contaminated with insoluble particulate material. These examples represent samples that may have large differences between replicate tests. The use of Procedure B will result in a more accurate value of breakdown voltage when testing such liquids.1.4.2.3 Use Procedure B to establish the breakdown voltage of an insulating liquid where an ASTM specification does not exist or when developing a value for an ASTM guide or standard. Procedure A may be used once the single operator precision of 13.1 has been demonstrated.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 The dielectric breakdown voltage of an insulating liquid is of importance as a measure of the liquid's ability to withstand electric stress without failure. The dielectric breakdown voltage serves to indicate the presence of contaminating agents such as water, dirt, cellulosic fibers, or conducting particles in the liquid, one or more of which may be present in significant concentrations when low breakdown voltages are obtained. However, a high dielectric breakdown voltage does not necessarily indicate the absence of all contaminants; it may merely indicate that the concentrations of contaminants that are present in the liquid between the electrodes are not large enough to deleteriously affect the average breakdown voltage of the liquid when tested by this test method (see Appendix X1.)3.2 This test method is used in laboratory or field tests. For field breakdown results to be comparable to laboratory results, all criteria including room temperature (20 to 30 °C) must be met.1.1 This test method covers the determination of the dielectric breakdown voltage of insulating liquids (oils of petroleum origin, silicone fluids, high fire-point mineral electrical insulating oils, synthetic ester fluids and natural ester fluids). This test method is applicable to insulating liquids commonly used in cables, transformers, oil circuit breakers, and similar apparatus as an insulating and cooling medium. Refer to Terminology D2864 for definitions used in this test method.1.2 This test method is sensitive to the deleterious effects of moisture in solution especially when cellulosic fibers are present in the liquid. It has been found to be especially useful in diagnostic and laboratory investigations of the dielectric breakdown strength of insulating liquid in insulating systems.21.3 This test method is used to judge if the VDE electrode breakdown voltage requirements are met for insulating liquids. This test method should be used as recommended by professional organization standards such as IEEE C57.106.1.4 This test method may be used to obtain the dielectric breakdown of silicone fluid as specified in Test Method D2225, Specification D4652, or Specification D6871, provided that the discharge energy into the sample is less than 20 mJ (milli joule) per breakdown for five consecutive breakdowns.1.5 Both the metric and the alternative inch-pound units are acceptable.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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CSA Preface This is the first edition of CAN/CSA-ISO 14341, Welding consumables - Wire electrodes and deposits for gas shielded metal arc welding of non alloy and fine grain steels - Classification, which is an adoption without modification of the iden

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