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AS 2247.1-1999 (R2013) Eucalyptus oil fractions 1,8-Cineole (Eucalyptol) 现行 发布日期 :  1999-09-05 实施日期 : 

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5.1 The bulk density is an indicator of calcined petroleum coke porosity and packing capability which is an important coke property for anode production in aluminum industry. This procedure will allow an automated measurement of specific sized fractions ranging from 8 mm to 0.25 mm coke particles.5.2 Results from this test method are used in determining coke specifications, classification purposes, and for quality control.1.1 The test method covers the determination of bulk density for a specific size fraction of calcined petroleum coke using an automated pycnometer that compacts coke by applying transaxial pressure under a controlled force.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method describes a physical property of solid waste in processing facilities, a property that characterizes the solid waste streams and hence the operation of resource recovery separators and processors.5.2 The bulk density is an important property for the design of materials handling equipment, separators, and processors.5.3 In this test method, bulk density is not considered an absolute material property as is the density of individual particles of a material. The measured bulk density here depends on the size of the container, the moisture content of the “as tested” material, and how the material is loaded into the container. For example, the bulk density of material placed loosely in a container will be less than that of material tamped into a container. Also, some materials placed loosely in a container will settle with time due to its own weight; thus, its bulk density will increase. As written, the “as tested” waste sample may or may not be dried prior to testing, so that calculated bulk density includes the moisture associated with the “as tested” material.1.1 This test method may be used to determine the bulk density of various fractions from the resource recovery processing of municipal solid waste. It is intended as a means of characterizing such fractions and for providing data useful to designers of solid waste processing plants.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method separates asphalts into four well-defined fractions. Analysis of these fractions can be used to evaluate asphalt composition (1, 2).4 For example, one can compare the ratios of the fractions with other asphalt systems to evaluate processing and aging parameters that relate to performance properties of the asphalt.1.1 This test method covers the separation of four defined fractions from petroleum asphalts. The four fractions are defined as saturates, naphthene aromatics, polar aromatics, and iso-octane insoluble asphaltenes. This method can also be used to isolate saturates, naphthene aromatics, and polar aromatics from distillate products such as vacuum gas oils, lubricating oils, and cycle stocks. These distillate products usually do not contain asphaltenes.1.2 The values stated in SI units are to be regarded as standard.1.3 Since a precision estimate for this standard has not been developed, this test method is to be used for research or informational purposes only. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 For the middle distillates whose boiling range is between 170 °C and 400 °C by such distillation methods like Test Method D2887, Procedure A can separate and determine the content of total aromatics and total nonaromatics by SPE and GC analysis of the resulting fractions. The determination of the total content of saturates and aromatics in petroleum middle distillates is useful to investigate the effects of petroleum processes on production of various finished fuels.5.2 The total aromatics content and polycyclic aromatics content are important to characterize the quality of diesel fuels. This test method is demonstrated to be time-saving and eco-friendly by reducing the amount of reagent consumption and avoiding the necessity of solvent evaporation step as required, for example, in such Test Method D2549.5.3 The determination of detailed hydrocarbon composition by mass spectrometry requires a preliminary separation of the sample into representative aromatics and nonaromatics, as in Test Method D2425, where Test Method D2549 is used to separate the distillate fuel. The SPE fractionation procedure described herein may provide a suitable fractionation alternative approach for these mass spectrometric types of methods.5.4 Biodiesel is a blendstock commodity primarily used as a value-added blending component with diesel fuel. Procedure B can provide a separation and determination technique to monitor the FAME content for FAME biodiesel blends.1.1 This test method covers the separation and determination of representative aromatics, nonaromatics, and fatty acid methyl ester (FAME) fractions in middle distillates that boil between 170 °C and 400 °C, including biodiesel blends with up to 20 % by volume of FAME, by solid phase extraction and gas chromatography.1.2 This test method provides two procedures, A and B. Procedure A is applicable to the petroleum-based middle distillates fuel, and Procedure B is applicable to the biodiesel blends with up to 20 % by volume of FAME.1.3 This test method is applicable to middle distillates samples with aromatics content ranging from 5 % to 50 % by mass and biodiesel blends with FAME content in the range of 0.5 % to 20 % by volume. This test method may apply to concentrations outside these ranges, but the precision has not been determined.1.4 For Procedure B, biodiesels in the form of fatty acid ethyl ester (FAEE) can also fully elute into the FAME fraction, and they have the similar FID (flame ionization detector) relative response factors with that of FAME. The determined content of FAME fractions are the sum of concentrations of FAME and FAEE by this test method (see 3.2.5).1.5 From the investigation results obtained for FAME determination, the low concentrations of monoglycerides (usually less than 0.5 % by mass in biodiesel blends) are not detectable under the gas chromatographic (GC) condition of this test method and will not interfere with the determination of FAME by Procedure B. As a result, biodiesel blends, conforming to the requirements of Specification D7467, containing up to 20 % by volume of biodiesel blendstock meeting the requirements in Specification D6751, typically contain concentrations of monoglycerides of less than 0.1 % by mass. The diglycerides and triglycerides, if present, are not detected under the GC condition of this test method due to their higher boiling points.NOTE 1: If a sample is suspected of containing an abnormal FAME biodiesel feedstock than specified in Specification D6751, for example, a sample contaminated with vegetable oil with a high level of total triglycerides, the content of mono-, di-, or tri-glycerides in the isolated FAME fraction may be determined using Test Method D6584. Samples containing biodiesels with a high amount of glycerides than specified in Specification D6751 may contaminate the GC column and not recommended for this test method.1.6 The values stated in acceptable SI units are to be regarded as the standard. No other units of measurement are included in this standard1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.NOTE 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 A knowledge of the hydrocarbon composition of process streams and petroleum products boiling within the range 205 °C to 540 °C (400 °F to 1000 °F) is useful in following the effect of changes in process variables, diagnosing the source of plant upsets, and in evaluating the effect of changes in composition on product performance properties. This method, when used together with Test Method D2786, provides a detailed analysis of the hydrocarbon composition of such materials.1.1 This test method2 covers the determination by high ionizing voltage, low resolution mass spectrometry of 18 aromatic hydrocarbon types and 3 aromatic thiophenotypes in straight run aromatic petroleum fractions boiling within the range from 205 °C to 540 °C (400 °F to 1000 °F) (corrected to atmospheric pressure). Samples must be nonolefinic, must contain not more than 1 % by mass of total sulfur, and must contain not more than 5 % nonaromatic hydrocarbons. Composition data are in volume percent.NOTE 1: Although names are given to 15 of the compound types determined, the presence of other compound types of the same empirical formulae is not excluded. All other compound types in the sample, unidentified by name or empirical formula, are lumped into six groups in accordance with their respective homologous series.1.2 The values stated in acceptable SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 The determination of compound types by mass spectrometry requires, in some instances, a preliminary separation of the petroleum sample into representative aromatics and nonaromatics fractions, as in Test Methods D2425, D2786, and D3239. This test method provides a suitable separation technique for this application.1.1 This test method covers the separation and determination of representative aromatics and nonaromatics fractions from hydrocarbon mixtures that boil between 232 °C and 538 °C (450 °F and 1000 °F). Alternative procedures are provided for the separation of 2 g or 10 g of hydrocarbon mixture.NOTE 1: Some components may not be eluted from the chromatographic column for some types of samples under the conditions used in this method.NOTE 2: Test Method D2007 is an alternative method of separating high-boiling oils into polar compounds, aromatics, and saturates fractions.1.2 An alternative procedure is provided to handle samples boiling below 232 °C (450 °F), but whose 5 % point is above 178 °C (350 °F) as determined by Test Method D2887. This procedure is given in Appendix X1.1.3 The values stated in acceptable SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This guide is intended to provide the conventions adopted by the International Standards Organization (ISO 7708), the Comité Européen de Normalisation (CEN EN 481), and the American Conference of Governmental Industrial Hygienists (ACGIH) (1). The definition of respirable aerosol is the basis for recommended exposure levels (REL) of respirable coal mine dust as promulgated by NIOSH (Criteria for a Recommended Standard, Occupational Exposure to Respirable Coal Mine Dust (15)). The respirable aerosol definition also forms the basis of the NIOSH sampling method for respirable particulates not otherwise regulated (NIOSH Manual of Analytical Methods (16)).4.2 The convention can be used for those who are preparing to evaluate a workplace environment by collecting samples of aerosolized particles, or who wish to obtain an understanding of what information can be obtained by such sampling. The convention to be used is not always straightforward, but generally depends on what part of the respiratory system is affected by the aerosol particles. The conventions are often applied for approximating mass fractions, but they may also be used in the evaluation of total surface area or the number of particles in the collected material.4.3 The conventions constitute a part of the performance characteristics required of aerosol samplers for collecting aerosol according to the relevant health effects. This guide therefore does not specify particular samplers for measuring the aerosol fractions defined here. Detailed guidelines for evaluating any given sampler relative to the conventions are available (CEN EN 13205, six parts). Several advantages over instrument specification can be attributed to the adoption of these performance-associated conventions:4.3.1 The conventions have a recognized relationship to health effects.4.3.2 Performance criteria permit instrument designers to seek practical sampler improvements.4.3.3 Performance criteria promote continued experimental testing of the samplers in use with the result that the significant variables (such as wind speed, particle charge, and so forth) affecting sampler operation become understood.1.1 This guide defines conventions for personal samplers of specific particle-size-dependent fractions of any given non-fibrous airborne aerosol. Such samplers are used for assessing health effects and in the setting of and testing for compliance with permissible exposure limits in the workplace and ambient environment. The conventions have been adopted by the International Standards Organization (ISO 7708), the Comité Européen de Normalisation (CEN EN 481), and the American Conference of Governmental Industrial Hygienists (ACGIH) (1).2 The conventions were developed (2) in part from health-effects studies reviewed (3) by the ACGIH and in part as a compromise between definitions proposed by the ACGIH (3) and by the British Medical Research Council (BMRC) (4). Conventions are given here for inhalable, thoracic, and respirable fractions.1.2 This guide is complementary to Test Method D4532, which describes the performance of respirable dust cyclones and operational procedures for use. The procedures, specifically the optimal flow rate, are still valid although the estimated accuracy differs somewhat from use with previous aerosol fraction definitions. Details on these instruments have been published (5-11).1.3 Limitations: 1.3.1 The definitions given here were adopted by the agencies listed in 1.1 in part on the basis of expected health effects of the different size fractions, but in part allowing for available sampling equipment. The original adoption by CEN was, in fact, for the eventual setting of common standards by the EC countries while permitting the use of a variety of instrumentation. Deviations of the sampling conventions from health-related effects are as follows:1.3.1.1 The inhalable fraction actually depends on the specific air speed and direction, on the breathing rate, and on whether breathing is by nose or mouth. The values given in the inhalable convention are for representative values of breathing rate and represent averages over all wind directions.1.3.1.2 The respirable and thoracic fractions vary from individual to individual and with the breathing pattern. The conventions are approximations to the average case.1.3.1.3 Each convention applies strictly to a fraction penetrating to a region, rather than depositing. Therefore, samples collected according to the conventions may only approximate correlations with biological effects. For example, the respirable convention overestimates the fraction of very small particles deposited in the alveolar region of the respiratory system because some of the particles are actually exhaled without being deposited (12). In many workplaces, these very small particles contribute insignificantly to the sampled mass. Furthermore, the large variability between individuals and the details of clearance may be as important as this type of effect.1.3.1.4 The thoracic convention applies to mouth breathing, for which aerosol collection is greater than during nose breathing.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers the material characteristics of virgin poly(glycolide) and poly(glycolide-co-lactide) resins with mole fractions within the specified range used in surgical implants. This does not cover packaged and sterilized finished implants fabricated from the same materials. Since some characteristics may be altered by processing techniques when used to produces a specific part or device, properties of fabricated forms of the resins should be evaluated independently using appropriate test methods. The identity of the poly(glycolide) homopolymer, poly(glycolide-co-lactide) copolymer, and poly(glycolide-co-lactide) polymer must be confirmed through nuclear magnetic resonance (NMR).1.1 This specification covers both virgin poly(glycolide) homopolymer and poly(glycolide-co-lactide) copolymer resins intended for use in surgical implants. The poly(glycolide-colactide) copolymers covered by this specification possess nominal mole fractions greater than or equal to 70 % glycolide (65.3 % in mass fraction). This specification is also applicable to lactide-co-glycolide copolymers that possess glycolide segments sufficient in size to deliver potential for glycolide-based crystallization, thereby requiring fluorinated solvents for complete dissolution under room temperature conditions.1.2 Since poly(glycolide) is commonly abbreviated as PGA for poly(glycolic acid) and poly(lactide) is commonly abbreviated as PLA for poly(lactic acid), these polymers are commonly referred to as PGA, PLA, and PLA:PGA resins for the hydrolytic byproducts to which they respectively degrade. PLA is a term that carries no stereoisomeric specificity and therefore encompasses both the amorphous atactic/syndiotactic dl-lactide-based polymers and copolymers as well as the isotactic d-PLA and l-PLA moieties, each of which carries potential for crystallization.1.3 This specification is specifically not applicable to amorphous poly(lactide-co-glycolide) or poly(lactide)-based resins able to be fully solvated at 30°C by either methylene chloride (dichloromethane) or chloroform (trichloromethane), which are covered in Specification F2579 and typically possess molar glycolide levels of ~50 % or less. This specification is not applicable to lactide-based polymers or copolymers that possess isotactic polymeric segments sufficient in size to carry potential for lactide-based crystallization, which are covered by Specification F1925 and typically possess nominal mole fractions that equal or exceed 50 % l-lactide.1.4 This specification addresses material characteristics of both virgin poly(glycolide) and poly(>70 % glycolide-co-lactide) resins intended for use in surgical implants and does not apply to packaged and sterilized finished implants fabricated from these materials.1.5 As with any material, some characteristics may be altered by processing techniques (such as molding, extrusion, machining, assembly, sterilization, and so forth) required for the production of a specific part or device. Therefore, properties of fabricated forms of this resin should be evaluated independently using appropriate test methods to assure safety and efficacy.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1018-11(2016) Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

4.1 Knowledge of the hydrogen content of petroleum products, particularly fuels, can be helpful in assessing performance characteristics.4.2 This test method is suitable for most laboratory applications requiring the determination of hydrogen in liquid petroleum lubricants and products.1.1 This test method covers the determination of hydrogen in petroleum fractions that can be burned completely without smoking in a wick lamp.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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