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This specification covers blended uranium oxides with a 235U content of less than 5% for direct hydrogen reduction to nuclear grade uranium dioxide. For commercial-grade uranium oxide with an isotopic content of 235U between that of natural uranium and 5%, the isotopic limits shall apply. Physical and chemical requirements include: uranium content, oxygen-to-uranium ratio, impurity content, equivalent boron content, bulk density, moisture content, ability to flow, particle size, and reduction and sinterability. Maximum concentration limit is specified for impurity elements such as: aluminum, barium, beryllium, bismuth, calcium+magnesium, carbon, chlorine, chromium, cobalt, copper, fluorine, iron, lead, manganese, molybdenum, nickel, phosphorus, silicon, sodium, tantalum, thorium, tin, titanium, tungsten, vanadium, and zinc. The identity of a lot shall be retained throughout.1.1 This specification covers blended uranium trioxide (UO3), U3O8, or mixtures of the two, powders that are intended for conversion into a sinterable uranium dioxide (UO2) powder by means of a direct reduction process. The UO2 powder product of the reduction process must meet the requirements of Specification C 753 and be suitable for subsequent UO2 pellet fabrication by pressing and sintering methods. This specification applies to uranium oxides with a 235U enrichment less than 5 %.1.2 This specification includes chemical, physical, and test method requirements for uranium oxide powders as they relate to the suitability of the powder for storage, transportation, and direct reduction to UO2 powder. This specification is applicable to uranium oxide powders for such use from any source.1.3 The scope of this specification does not comprehensively cover all provisions for preventing criticality accidents, for health and safety, or for shipping. Observance of this specification does not relieve the user of the obligation to conform to all international, national, state, and local regulations for processing, shipping, or any other way of using uranium oxide powders (see 2.2 and 2.3).1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 The following safety hazards caveat pertains only to the test methods portion of the annexes in this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Liquefied petroleum gases and their products of combustion must not be unduly corrosive to the materials with which they come in contact. The potential personnel exposure hazards of H2S also make the detection and measurement of hydrogen sulfide important, even in low concentrations. In addition, in some cases the odor of the gases shall not be objectionable. (See Specification D1835 and GPA 2140.)1.1 This test method2 covers the detection of hydrogen sulfide in liquefied petroleum (LP) gases. The sensitivity of the test is about 4 mg/m3 (0.15 to 0.2 grain of hydrogen sulfide per 100 ft3) of gas.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 These test methods determine whether copper products will be resistant to embrittlement when exposed to elevated temperatures in a reducing atmosphere.5.1.1 It is assumed that all who use these test methods will be trained personnel capable of performing these procedures skillfully and safely. It is expected that work will be performed in a properly equipped facility.1.1 These test methods describe procedures for determining the presence of cuprous oxide (Cu2O) in products made from deoxidized and oxygen-free copper.1.2 The test methods appear in the following order:  Sections   Microscopical Examination without Thermal Treatment 9 – 11Microscopical Examination after Thermal Treatment 13 – 15Closed Bend Test after Thermal Treatment 17 – 19Reverse Bend Test after Thermal Treatment 21 – 231.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Low operating temperature fuel cells such as proton exchange membrane (PEM) fuel cells require high purity hydrogen for maximum material performance and lifetime. Analysis to part-per-billion (ppb) concentration of individual cation contaminants such as potassium, sodium and ammonium in hydrogen and related fuel cell supply gases is necessary for assuring a feed gas of sufficient purity to satisfy fuel cell system needs. More specifically, cations such as ammonium causes irreversible performance degradation of proton exchange membranes used in low temperature fuel cells by reacting with protons in the membrane to form ammonium ions.Although not intended for application to gases other than hydrogen and related fuel cell supply gases, techniques within this test method can be applied to other gaseous samples requiring cation analysis.1.1 This test method describes a procedure for the determination of cations in hydrogen and other fuel cell feed gases. It has been successfully applied to other types of gaseous samples including air, engine exhaust, and landfill samples. An ion chromatograph/conductivity detector (IC/CD) system is used to determine cations. Sensitivity from low part per billion (ppb, μg/l, μg/kg) up to part per million (ppm, mg/l, mg/kg) concentration are achievable dependant on the amount of hydrogen or other fuel cell gas sampled. This test method can be applied to other gaseous samples requiring analysis of trace constituents provided an assessment of potential interferences has been accomplished.1.2 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 General—Hydrogen sulfide is nearly ubiquitous. It occurs naturally in volcanic gases, in sulfur springs and fumaroles, in decaying of plant and animal protein, and in intestines as a result of bacterial action. Hydrogen sulfide is a serious hazard to the health of workers employed in energy production from hydrocarbon or geothermal sources, in the production of fibers and sheets from viscose syrup, in the production of deuterium oxide (heavy water), in tanneries, sewers, sewage treatment and animal waste disposal, in work below ground, on fishing boats, and in chemical operations, including the gas and oil industry.5.2 In 29 CFR 1910.1000, the Federal Occupational Safety and Health Administration designates that worker exposure to certain gases and vapors must not be exceeded in workplace atmospheres at concentrations above specific values, averaged over a certain time span. Hydrogen sulfide is included in this list. Refer also to NIOSH Criteria for a Recommended Standard, Occupational Exposure to Hydrogen Sulfide.5.3 This practice will provide means for the determination of airborne concentrations of hydrogen sulfide.5.4 This practice provides means for either personal or area sampling and for short-term or time-weighted average (TWA) measurements. Refer to Threshold Limit Values for Chemical Substances in the Work Environment.1.1 This practice covers the detection of hydrogen sulfide gas by visual chemical detectors. Included under visual chemical detectors are: short-term detector tubes (1),2 long-term detector tubes (2), and length-of-stain dosimeters (3). Diffusion tubes are not included under this practice because they are not direct reading, and spot tests are not included because of their poor accuracy. The sample results are immediately available by visual observation, thus no analytical equipment is needed.1.2 This practice reflects the current state-of-the-art for commercially available visual length-of-stain detectors for hydrogen sulfide. Any mention of a specific manufacturer in the text or references does not constitute an endorsement by ASTM.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 These test methods cover the determination of total carbon and hydrogen in samples of coal or coke. Both the carbon and hydrogen are determined in one operation. These test methods yield the total percentages of carbon and hydrogen in the coal as analyzed and the results include not only the carbon and hydrogen in the organic matter, but also the carbon present in mineral carbonates and the hydrogen present in the free moisture accompanying the sample as well as hydrogen present as water of hydration of silicates.Note 1—It is recognized that certain technical applications of the data derived from this test procedure may justify additional corrections. These corrections could involve compensation for the carbon present as carbonates, the hydrogen of free moisture accompanying the sample, and the calculated hydrogen present as water of hydration of silicates.1.2 When data are converted and reported on the "dry" basis, the hydrogen value is corrected for the hydrogen present in the free moisture accompanying the sample.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 The values stated in SI units are to be regarded as the standard.

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5.1 Residual fuel oils can contain H2S in the liquid phase and this can result in hazardous vapor phase levels of H2S in storage tank headspaces. The vapor phase levels can vary significantly according to the headspace volume, fuel temperature and agitation. Measurement of H2S levels in the liquid phase provides a useful indication of the residual fuel oil’s propensity to form high vapor phase levels, and lower levels in the residual fuel oil will directly reduce risk of H2S exposure. It is critical, however, that anyone involved in handling fuel oil, such as vessel owners and operators, continue to maintain appropriate safety practices designed to protect the crew, tank farm operators and others who can be exposed to H2S.5.1.1 The measurement of H2S in the liquid phase is appropriate for product quality control, while the measurement of H2S in the vapor phase is appropriate for health and safety purposes.5.2 This test method was developed to provide refineries, fuel terminals and independent testing laboratories, which do not have access to analytical instruments such as a gas chromatograph, with a simple and consistent field test method for the rapid determination of H2S in the vapor phase above residual fuel oils.NOTE 1: D5705 is one of three test methods for quantitatively measuring H2S in residual fuels:1) Test Method D6021 is an analytical test method to determine H2S levels in the liquid phase.2) Test Method D7621 is a rapid test method to determine H2S levels in the liquid phase.NOTE 2: Because of the reactivity, absorptivity and volatility of H2S, any measurement method only provides an H2S concentration at a given moment in time.5.3 This test method does not necessarily simulate the vapor phase H2S concentration in a fuel storage tank. It does, however, provide a level of consistency so that the test result is only a function of the residual fuel oil sample and not the test method, operator, or location. No general correlation can be established between this field test and actual vapor phase concentrations of H2S in residual fuel oil storage or transports. However, a facility that produces fuel oil from the same crude source under essentially constant conditions might be able to develop a correlation for its individual case.1.1 This test method covers the field determination of hydrogen sulfide (H2S) in the vapor phase (equilibrium headspace) of a residual fuel oil sample.1.2 The test method is applicable to liquids with a viscosity range of 5.5 mm2/s at 40 °C to 50 mm2/s at 100 °C. The test method is applicable to fuels conforming to Specification D396 Grade Nos. 4, 5 (Heavy), and 6.1.3 The applicable range is from 5 μmol/mol to 4000 μmol/mol (micromoles per mole) (5 ppm v/v to 4000 ppm v/v (parts per million by volume)).1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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