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AS 1896-1976 Method of test for ignition temperature of gases and vapours 现行 发布日期 :  1976-07-01 实施日期 : 

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5.1 Knowledge of the individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons can be determined through the use of this test method.5.2 This test method is adopted from earlier development and enhancement.4,5,6,7 The chromatographic operating conditions and column tuning process, included in this test method, were developed to provide and enhance the separation and subsequent determination of many individual components not obtained with previous single-column analyses. The column temperature program profile is selected to afford the maximum resolution of possible co-eluting components, especially where these are of two different compound types (for example, a paraffin and a naphthene).5.3 Although a majority of the individual hydrocarbons present in petroleum distillates are determined, some co-elution of compounds is encountered. If this test method is utilized to determine bulk hydrocarbon group-type composition (PONA), the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of olefinic or naphthenic, or both, constituents above octane may reflect significant errors in PONA-type groupings.5.4 If water is or is suspected of being present, its concentration is determined by the use of Test Method D1744. Other compounds containing oxygen, sulfur, nitrogen, and so forth may also be present, and may co-elute with the hydrocarbons. When known co-elution exists, these are noted in the test method data tables. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Method D4815 and D5599 for oxygenates, Test Method D5580 for aromatics, and Test Method D5623 for sulfur compounds.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels and their mixtures containing oxygenate blends (MTBE, ETBE, ethanol, and so forth) with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels.1.2 Based on the cooperative study results, individual component concentrations and precision are determined in the range from 0.01 % to approximately 30 % by mass. The test method may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the test method is used for components with concentrations outside the specified ranges.1.3 This test method also determines methanol, ethanol, t-butanol, methyl t-butyl ether (MTBE), ethyl t-butyl ether (ETBE), and t-amyl methyl ether (TAME) in spark ignition engine fuels in the concentration range from 1 % to 30 % by mass. However, the cooperative study data provided insufficient statistical data for obtaining a precision statement for these compounds.1.4 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this test method is utilized to estimate bulk hydrocarbon group-type composition (PONA), the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of naphthenic (for example, virgin naphthas) constituents above n-octane may reflect significant errors in PONA-type groupings. Based on the gasoline samples in the interlaboratory cooperative study, this test method is applicable to samples containing less than 25 % by mass of olefins. However, some interfering co-elution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Annex A1 of this test method compares results of the test method with other test methods for selected components, including olefins, and several group types for several interlaboratory cooperative study samples. Although benzene, toulene, and several oxygenates are determined, when doubtful as to the analytical results of these components, confirmatory analyses can be obtained by using the specific test methods listed in the reference section.1.4.1 Total olefins in the samples may be obtained or confirmed, or both, if necessary, by Test Method D1319 (percent by volume) or other test methods, such as those based on multidimentional PONA-type of instruments.1.5 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744 or equivalent. Other compounds containing oxygen, sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Methods D4815 and D5599 for oxygenates, and Test Method D5623 for sulfur compounds, or equivalent.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Most organic liquids and solids will ignite in a pressurized oxidizing gas atmosphere if heated to a sufficiently high temperature and pressure. This procedure provides a numerical value for the temperature at the onset of ignition under carefully controlled conditions. Means for extrapolation from this idealized situation to the description, appraisal, or regulation of fire and explosion hazards in specific field situations, are not established. Ranking of the ignition temperatures of several materials in the standard apparatus is generally in conformity with field experience.4.2 The temperature at which material will ignite spontaneously (AIT) will vary greatly with the geometry of the test system and the rate of heating. To achieve good interlaboratory agreement of ignition temperatures, it is necessary to use equipment of approximately the dimensions described in the test method. It is also necessary to follow the described procedure as closely as possible.4.3 The decomposition and oxidation of some fully fluorinated materials releases so little energy that there is no clear-cut indication of ignition. Nor will there be a clear indication of ignition if a sample volatilizes, distilling to another part of the reaction vessel, before reaching ignition temperature.1.1 This test method covers the determination of the temperature at which liquids and solids will spontaneously ignite. These materials must ignite without application of spark or flame in a high-pressure oxygen-enriched environment.1.2 This test method is intended for use at pressures of 2.1 MPa to 20.7 MPa [300 psi to 3000 psi]. The pressure used in the description of the method is 10.3 MPa [1500 psi], and is intended for applicability to high pressure conditions. The test method, as described, is for liquids or solids with ignition temperature in the range from 60 °C to 500 °C [140 °F to 932 °F].NOTE 1: Test Method G72/G72M normally utilizes samples of approximately 0.20 ± 0.03-g mass, a starting pressure of 10.3 MPa [1500 psi] and a temperature ramp rate of 5 °C/min. However, Autogenous Ignition Temperatures (AIT) can also be obtained under other test conditions. Testing experience has shown that AIT testing of volatile liquids can be influenced by the sample pre-conditioning and the sample mass. This will be addressed in the standard as Special Case 1 in subsection 8.2.2. Testing experience has also shown that AIT testing of solid or non-volatile liquid materials at low pressures (that is, < 2.1 MPa) can be significantly influenced by the sample mass and the temperature ramp rate. This will be addressed in the standard as Special Case 2, in subsection 8.2.3. Since the AIT of a material is dependent on the sample mass/configuration and test conditions, any departure from the standard conditions normally used for Test Method G72/G72M testing should be clearly indicated in the test report.1.3 This test method is for high-pressure pure oxygen. The test method may be used in atmospheres from 0.5 % to 100 % oxygen.1.4 An apparatus suitable for these requirements is described. This test method could be applied to higher pressures and materials of higher ignition temperature. If more severe requirements or other oxidizers than those described are desired, care must be taken in selecting an alternative safe apparatus capable of withstanding the conditions.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test standard describes how to evaluate the relative sensitivity of materials and components to dynamic pressure impacts by various gaseous fluid media (can include gas mixtures).4.2 Changes or variations in test specimen configurations, thickness, preparation, and cleanliness can cause a significant change in their impact ignition sensitivity/reaction. For material tests, the test specimen configuration shall be specified on the test report.4.3 Changes or variation in the test system configuration from that specified herein may cause a significant change in the severity produced by a dynamic pressure surge of the gaseous media.4.4 A reaction is indicated by an abrupt increase in test specimen temperature, by obvious changes in odor, color, or material appearance, or a combination thereof, as observed during post-test examinations. Odor alone is not considered positive evidence that a reaction has occurred. When an increase in test specimen temperature is observed, a test specimen reaction must be confirmed by visual inspection. To aid with visual inspection, magnification less than 10× can be used.4.5 When testing components, the test article must be disassembled and the nonmetallic materials examined for evidence of ignition after completion of the specified pressure surge cycles.4.6 Ignition or precursors to ignition for any test sample shall be considered a failure and are indicated by burning, material loss, scorching, or melting of a test material detected through direct visual means. Ignition is often indicated by consumption of the non-metallic material under test, whether as an individual material or within a component. Partial ignition can also occur, as shown in Fig. 3a, b, and c, and shall also be considered an ignition (failure) for the purpose of this test standard.FIG. 3 a Untested PCTFE (10X Magnification) (Polychlorotrifluoroethylene) Sample.FIG. 3 b Untested Nylon (PA, polyamide) Valve Seat (10X magnification) (continued)FIG. 3 c Untested Pin-Index Sealing Washer (10X magnification) (continued)NOTE 1: For the purpose of this standard, test samples that visually appear in these conditions, or similar, are considered to be representative of ignition.FIG. 3 Photographs Representing Partial Reactions Including Scorching, Discoloration, Melting and Material Loss or Material Consumption. For the purpose of this standard, test samples that visually appear in these conditions, or similar, are considered to be representative of ignition.NOTE 2: A representative (exemplar) material or component may be requested by the test laboratory personnel for visual comparison with the post-test condition of the test samples.4.7 For material testing, the prescribed procedure is conducted on multiple samples until a statistically significant number of ignitions or no-ignitions, or both, are achieved at various test pressures. The data is then analyzed by a procedure that calculates the median failure pressure (i.e., the 50 % reaction pressure) or the functional form of the ignition probability versus pressure by logistic regression analysis. Materials tested in a similar configuration can be ranked against each other by either of these two criteria. The initial test gas temperature may be varied as required depending on the requirements of the test.4.8 For component testing, a specified number of pressure surge cycles are conducted at a defined test pressure, usually specified by a particular industry test standard. Usually, this pressure is 1.2 times the maximum allowable working pressure of the component. The initial test gas temperature may be varied depending on the requirements of the test; however, most commonly the initial test gas temperature is 60 ± 3 °C.1.1 This test method describes a method to determine the relative sensitivity of nonmetallic materials (including plastics, elastomers, coatings, etc.) and components (including valves, regulators flexible hoses, etc.) to dynamic pressure impacts by gases such as oxygen, air, or blends of gases containing oxygen.1.2 This test method describes the test apparatus and test procedures employed in the evaluation of materials and components for use in gases under dynamic pressure operating conditions up to gauge pressures of 69 MPa and at elevated temperatures.1.3 This test method is primarily a test method for ranking of materials and qualifying components for use in gaseous oxygen. The material test method is not necessarily valid for determination of the sensitivity of the materials in an “as-used” configuration since the material sensitivity can be altered because of changes in material configuration, usage, and service conditions/interactions. However, the component testing method outlined herein can be valid for determination of the sensitivity of components under service conditions. The current provisions of this method were based on the testing of components having an inlet diameter (ID bore) less than or equal to 14 mm (see Note 1).1.4 A 5 mm Gaseous Fluid Impact Sensitivity (GFIS) test system and a 14 mm GFIS test system are described in this standard. The 5 mm GFIS system is utilized for materials and components that are directly attached to a high-pressure source and have minimal volume between the material/component and the pressure source. The 14 mm GFIS system is utilized for materials and components that are attached to a high pressure source through a manifold or other higher volume or larger sized connection. Other sizes than these may be utilized but no attempt has been made to characterize the thermal profiles of other volumes and geometries (see Note 1).NOTE 1: The energy delivered by this test method is dependent on the gas volume being rapidly compressed at the inlet to the test specimen or test article. Therefore the geometry of the upstream volume (diameter and length) is crucial to the test and crucial to the application of the results to actual service conditions. It is therefore recommended that caution be exercised in applying the results of this testing to rapid pressurization of volumes larger than those standardized by this test method. This energy delivered by this standard is based on the rapid compression of the volume in either a 5 mm ID by 1000 mm long impact tube or a 14 mm ID by 750 mm long impact tube. These two upstream volumes are specified in this standard based on historic application within the industry.1.5 This test method can be utilized to provide batch-to-batch comparison screening of materials when the data is analyzed according to the methods described herein. Acceptability of any material by this test method may be based on its 50 % reaction pressure or its probability of ignition based on a logistic regression analysis of the data (described herein).1.6 Many ASTM, CGA, and ISO test standards require ignition testing of materials and components by gaseous fluid impact, also referred to as adiabatic compression testing. This test method provides the test system requirements consistent with the requirements of these other various standards. The pass/fail acceptance criteria may be provided within other standards and users should refer to those standards. Pass/fail guidance is provided in this standard such as that noted in section 4.6. This test method is designed to ensure that consistent gaseous fluid impact tests are conducted in different laboratories.1.7 The criteria used for the acceptance, retest, and rejection, or any combination thereof of materials and components for any given application shall be determined by the user and are not fixed by this method. However, it is recommended that at a minimum the 95 % confidence interval be established for all test results since ignition by this method is inherently probabilistic and should be treated by appropriate statistical methods.1.8 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautions see Section 7.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Knowledge of the individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons may be determined through the use of this test method.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as, blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels. The tables in Annex A1 enumerate the components reported. Component concentrations are determined in the range from 0.10 % to 15 % by mass. The procedure may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the procedures are used for components with concentrations outside the specified ranges.1.2 This test method is applicable also to spark-ignition engine fuel blends containing oxygenated components. However, in this case, the oxygenate content must be determined by Test Methods D5599 or D4815.1.3 Benzene co-elutes with 1-methylcyclopentene. Benzene content must be determined by Test Method D3606 or D5580.1.4 Toluene co-elutes with 2,3,3-trimethylpentane. Toluene content must be determined by Test Method D3606 or D5580.1.5 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this procedure is utilized to estimate bulk hydrocarbon group-type composition (PONA) the user of such data should be cautioned that error may be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of naphthenic (for example, virgin naphthas) constituents above n-octane may reflect significant errors in PONA type groupings. Based on the interlaboratory cooperative study, this procedure is applicable to samples having concentrations of olefins less than 20 % by mass. However, significant interfering coelution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Many of the olefins in spark ignition fuels are at a concentration below 0.10 %; they are not reported by this test method and may bias the total olefin results low.1.5.1 Total olefins in the samples may be obtained or confirmed, or both, by Test Method D1319 (volume %) or other test methods, such as those based on multidimensional PONA type of instruments.1.6 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744. Other compounds containing sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Method D5623 for sulfur compounds.1.7 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The residue on ignition, which consists essentially of SiO2, is related to the silicon content of the silane and may be used to verify the composition of the silane.1.1 This test method covers the determination of the residue on ignition of silanes of the type bis-(triethoxysilylpropyl)sul- fane, or of admixtures of these silanes and solid carriers, such as carbon black, waxes, or organic polymers.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1. Scope Section A - Transformers for Luminous-Tube Signs A1.1 This section applies to transformers for luminous-tube signs of portable and stationary types, for potentials up to and includ ing 600 volts low-potential, and l5,000 volts open-circuit

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5.1 This test method was developed to evaluate automotive engine oils for protection against oil thickening and engine wear during moderately high-speed, high-temperature service.5.2 The increase in oil viscosity obtained in this test indicates the tendency of an oil to thicken because of oxidation. In automotive service, such thickening can cause oil pump starvation and resultant catastrophic engine failures.5.3 The deposit ratings for an oil indicate the tendency for the formation of deposits throughout the engine, including those that can cause sticking of the piston rings in their grooves. This can be involved in the loss of compression pressures in the engine.5.4 The camshaft and lifter wear values obtained in this test provide a measure of the anti-wear quality of an oil under conditions of high unit pressure mechanical contact.5.5 The test method was developed to correlate with oils of known good and poor protection against oil thickening and engine wear. Specially formulated oils that produce less than desirable results with unleaded fuels were also used during the development of this test.5.6 The Sequence IIIG engine oil test has replaced the Sequence IIIF test and can be used in specifications and classifications of engine lubricating oils, such as the following:5.6.1 Specification D4485,5.6.2 Military Specification MIL-PRF-2104, and5.6.3 SAE Classification J183.1.1 This test method covers an engine test procedure for evaluating automotive engine oils for certain high-temperature performance characteristics, including oil thickening, varnish deposition, oil consumption, as well as engine wear. Such oils include both single viscosity grade and multiviscosity grade oils that are used in both spark-ignition, gasoline-fueled engines, as well as in diesel engines.1.1.1 Additionally, with nonmandatory supplemental requirements, a IIIGA Test (Mini Rotary Viscometer and Cold Cranking Simulator measurements), a IIIGVS Test (EOT viscosity increase measurement), or a IIIGB Test (phosphorous retention measurement) can be conducted. These supplemental test procedures are contained in Appendix X1, Appendix X2, and Appendix X3, respectively.NOTE 1: Companion test methods used to evaluate engine oil performance for specification requirements are discussed in SAE J304.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exception—Where there is no direct SI equivalent such as screw threads, national pipe threads/diameters, and tubing size.1.3 This test method is arranged as follows:  SectionIntroduction   1Referenced Documents 2Terminology 3Summary of Test Methods 4 5Apparatus 6 Laboratory 6.1 Drawings 6.2 Specified Equipment 6.3 Test Engine 6.4  Engine Parts 6.4.1 Engine Speed and Load Control 6.5 Fluid Conditioning Module 6.6  Engine Cooling System 6.6.1 Flushing Tank 6.7 Coolant Mixing Tank 6.8 Condenser Cooling Systems 6.9 Engine Oil-Cooling System 6.10 Fuel System 6.11 Induction Air Supply Humidity, Temperature, and Pressure 6.12 Temperature Measurement 6.13  Thermocouple Location 6.13.1 Air-to-Fuel Ratio Determination 6.14  Injector Flow Testing 6.14.1 Exhaust and Exhaust Back Pressure Systems 6.15 Blowby Flow Rate Measurement 6.16 Pressure Measurement and Pressure Sensor Location 6.17Reagents and Materials 7 Test Fuel 7.1 Engine and Condenser Coolant 7.2 Coolant Additive 7.3 Coolant Preparation 7.4 Pre-Test Cleaning Materials 7.5 Sealing and Anti-seize Compounds 7.6Test Oil Sample Requirements 8Preparation of Apparatus 9 Condenser Cleaning 9.1 Intake Manifold Cleaning 9.2 Cleaning of Engine Parts (other than the block and heads) 9.3 Connecting Rod Cleaning 9.4 Engine Block Cleaning 9.5 Cylinder Head Cleaning 9.6 Engine Build-up Procedure 9.7  General Information 9.7.1  Special Parts 9.7.2  Hardware Information 9.7.3  Fastener Torque Specifications and Torquing Procedures 9.7.4   Main Bearing Cap Bolts 9.7.4.1   Cylinder Head Bolts 9.7.4.2   Torques for Miscellaneous Bolts, Studs, and Nuts 9.7.4.3 Parts Replacement 9.8 Engine Block Preparation 9.9 Piston Fitting and Numbering 9.10  Piston Ring Fitting 9.10.1 Pre-Test Camshaft and Lifter Measurements 9.11 Camshaft Bearing Installation 9.12 Camshaft Installation 9.13 Main Bearings 9.14  Crankshaft Installation 9.14.1  Main Bearing Cap Installation 9.14.2 Crankshaft Sprocket 9.15 Camshaft Sprocket, and Timing Chain 9.16 Crankshaft End Play 9.17 Piston Pin Installation 9.18  Piston Installation 9.18.1 Harmonic Balancer 9.19 Connecting Rod Bearings 9.20 Engine Front Cover 9.21 Coolant Inlet Adapter 9.22 Oil Dipstick Hole 9.23 Oil Pan 9.24 Cylinder Head Assembly 9.25 Adjustment of Valve Spring Loads 9.26 Cylinder Head Installation 9.27 Hydraulic Valve Lifters 9.28 Pushrods 9.29 Valve Train Loading 9.30 Intake Manifold 9.31 Rocker Covers 9.32 Water Inlet Adapter 9.33 Condenser 9.34 Coolant Outlet Adapter 9.35 External Oil Cooling System 9.36 Oil Sample Valve 9.37 Ignition System 9.38 Throttle Body 9.39 Accessory Drive Units 9.40 Exhaust Manifolds, Water-Cooled 9.41 Engine Flywheel 9.42 Pressure Checking of Engine Coolant System 9.43 Lifting of Assembled Engines 9.44 Mounting the Engine on the Test Stand 9.45 External Cooling System Cleaning 9.46 Engine Coolant Jacket Cleaning (Flushing) 9.47 Coolant Charging 9.48 Test Oil Charging 9.49 Engine Oil Pump Priming 9.50Calibration 10 Laboratory and Engine Test Stand Calibration 10.1 Testing of Reference Oils 10.2 Reference Oil Test Frequency 10.3 Evaluation of Reference Oil Test Results 10.4 Status of Non-Reference Oil Tests Relative to Reference  Oil Test 10.5 Status of Test Stands Used for Non-Standard Tests 10.6 Data Acquisition and Control 10.7  Sample Rate 10.7.1  Measurement Accuracy 10.7.2  Temperature 10.7.3  Pressure 10.7.4  Flow 10.7.5  Speed 10.7.6  Load 10.7.7  Measurement Resolution 10.7.8  System Time Response 10.7.9  Quality Index 10.7.10Engine Operating Procedure 11 Dipstick and Hole Plug 11.1 Dipstick Hole O-ring 11.2 Engine Start-up and Shutdown Procedures 11.3 Start-up 11.4 Scheduled Shutdown 11.5 Non-Scheduled Shutdowns 11.6 Oil Sampling 11.7 Oil Leveling 11.8 Air-to-Fuel-Ratio Measurement and Control 11.9 Air-to-Fuel Ratio Verification 11.10 Blowby Flow Rate Measurement 11.11 NOx Determinations 11.12 Data Recording 11.13 Initial run (10 min) 11.14 Engine Oil Quality Testing (100 h) 11.15 Test Termination 11.16Determination of Test Results 12 Engine Disassembly 12.2 Preparation of Parts for Rating of Sticking, Deposits,  and Plugging 12.3 Piston Deposit Rating 12.4 Post-Test Camshaft and Lifter Wear Measurements 12.5 Viscosity Test 12.6 Testing Oil Samples for Wear Metals 12.7 Blowby Flow Rate Measurements 12.8 Oil Consumption Computation 12.9 Photographs of Test Parts 12.10 Retention of Representative Test Parts 12.11 Severity Adjustments 12.12 Determination of Operational Validity 12.13Report 13 Report Forms 13.1 Precision of Reported Units 13.4Precision and Bias 14Keywords 15ASTM Test Monitoring Center: Organization Annex A1ASTM Test Monitoring Center: Calibration Procedures Annex A2ASTM Test Monitoring Center: Maintenance Activities Annex A3ASTM Test Monitoring Center: Related Information Annex A4Sequence IIIG Test Parts Replacement Guidelines Annex A5Sequence IIIG Determination Volume of Engine Oil in Pan Annex A6Sequence IIIG Test Fuel Analysis Annex A7Sequence IIIG Test Report Forms and Data Dictionary Annex A8Sequence IIIG Test Air-to-Fuel Ratio Control Flow Chart Annex A9Sequence IIIG Test Set Points and Control States Annex A10Sequence IIIG Quality Index Upper and Lower Values Annex A11Sequence IIIG Engine Oil Level Worksheet Annex A12Blowby Flow Rate Determination Annex A13Safety Hazards Annex A14Sequence IIIG Blueprint Listing Annex A15Fluid Condition Module Components Annex A16Engine Build Worksheets Annex A17Engine Oil Cooling System Schematic Annex A18Guidelines For Hardware Subject To First-In/First-Out Criteria Annex A19Sequence IIIGA Test Procedure Appendix X1Sequence IIIGVIS Test Procedure Appendix X2Sequence IIIGB Test Procedure Appendix X31.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are provided in 6.14.1.1 and 7.1.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers the material, manufacturing, and specialized property requirements for producing special-purpose aviation distillate test fuels that are intended only for engineering and certification testing of aircraft, engines, and aircraft equipment. It deals with special-purpose test fuels that may be used to evaluate the operability, performance and durability of aviation compression-ignition engines when operating with fuels of marginal performance. Aviation distillate fuel, except as otherwise specified in this specification, shall consist predominantly of refined hydrocarbons derived from conventional sources such as crude oil, natural gas liquid condensates, heavy oil, shale oil, and oil sands. The use of middle distillate fuel blends containing components from other sources is permitted. This specification also lists acceptable additives for aviation distillate special-purpose test fuels. Use of this specification for engineering and certification testing of aircraft is not mandatory. It is directed at civil applications, and maintained as such, but may be adopted for military, government, or other specialized uses.1.1 This specification is intended to support purchasing agencies when formulating specifications for purchases of aviation distillate fuel under contract.1.2 This specification defines specialized property requirements to produce special-purpose aviation distillate test fuels that are intended only for engineering and certification testing of aircraft, engines, and aircraft equipment. Use of this specification for engineering and certification testing of aircraft is not mandatory. Its use is at the discretion of the aircraft manufacturer, engine manufacturer, or certification authorities when determining criteria for validation of aircraft equipment design.1.3 This specification defines special-purpose test fuels that may be used to evaluate the operability, performance and durability of aviation compression-ignition engines when operating with fuels of marginal performance. The aviation distillate test fuels defined in this specification are not intended for general purpose use in aircraft. This specification also lists acceptable additives for aviation distillate special-purpose test fuels.1.4 Specification D8147 is directed at civil applications, and maintained as such, but may be adopted for military, government, or other specialized uses.1.5 This specification can be used as a standard in describing the quality of aviation distillate fuel from production to the aircraft. However, this specification does not define the quality assurance testing and procedures necessary to ensure that fuel continues to comply with this specification after batch certification.1.6 This specification does not include all fuels satisfactory for aviation compression-ignition (CI) engines.1.7 The values stated in SI units are to be regarded as standard.1.7.1 Exception—Other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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This specification covers requirements for fuel grade methyl tertiary-butyl ether utilized in commerce, terminal blending, or downstream blending with fuels for spark-ignition engines. The following test methods shall be conducted to meet the specified requirements: appearance; sulfur; solvent-washed gum content; MTBE mass percentage; methanol mass percentage; API gravity; density; copper strip corrosion; water content; vapor pressure; and color.1.1 This specification covers requirements for fuel grade methyl tertiary-butyl ether utilized in blending with gasolines at 1 % to 15 % by volume (equivalent to 2.7 % by weight oxygen) for use as automotive spark-ignition engine fuel covered by Specification D4814 as well as other automotive fuel applications involving MTBE. Other MTBE grades may be available for blending that are not covered by this specification.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 515元 / 折扣价: 438 加购物车

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