4.1 This practice is intended to help users, particularly power plant operators, maintain effective control over their mineral lubricating oils and lubrication monitoring program. This practice may be used to perform oil changes based on oil condition and test results rather than on the basis of service time or calendar time. It is intended to save operating and maintenance expenses.4.2 This practice is also intended to help users monitor the condition of mineral lubricating oils and guard against excessive component wear, oil degradation, or contamination, thereby minimizing the potential of catastrophic machine problems that are more likely to occur in the absence of such an oil condition monitoring program.4.3 This practice does not necessarily reference all of the current oil testing technologies and is not meant to preclude the use of alternative instrumentation or test methods that provide meaningful or trendable test data, or both. Some oil testing devices and sensors (typically used for screening oils that will be tested according to standard methods) provide trendable indicators that correlate to water, particulates, and other contaminants but do not directly measure these.4.4 This practice is intended for mineral oil products, and not for synthetic type of products, with the exception of phosphate esters fluids typically used in power plant control systems.1.1 This practice covers the requirements for the effective monitoring of mineral oil and phosphate ester fluid lubricating oils in service auxiliary (non-turbine) equipment used for power generation. Auxiliary equipment covered includes gears, hydraulic systems, diesel engines, pumps, compressors, and electrohydraulic control (EHC) systems. It includes sampling and testing schedules and recommended action steps, as well as information on how oils degrade.NOTE 1: Other types of synthetic lubricants are sometimes used but are not addressed in this practice because they represent only a small fraction of the fluids in use. Users of these fluids should consult the manufacturer to determine recommended monitoring practices.1.2 This practice does not cover the monitoring of lubricating oil for steam and gas turbines. Rather, it is intended to complement Practice D4378.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method measures the tendency of automotive manual transmission and final drive lubricants to deteriorate under high-temperature conditions, resulting in thick oil, sludge, carbon and varnish deposits, and the formation of corrosive products. This deterioration can lead to serious equipment performance problems, including, in particular, seal failures due to deposit formation at the shaft-seal interface. This test method is used to screen lubricants for problematic additives and base oils with regard to these tendencies.5.2 This test method is used or referred to in the following documents:5.2.1 American Petroleum Institute (API) Publication 1560-Lubricant Service Designations for Automotive Manual Transmissions, Manual Transaxles, and Axles,75.2.2 STP-512A–Laboratory Performance Tests for Automotive Gear Lubricants Intended for API GL-5 Service,85.2.3 SAE J308-Information Report on Axle and Manual Transmission Lubricants,9 and5.2.4 U.S. Military Specification MIL-L-2105D.1.1 This test method is commonly referred to as the L-60-1 test.2 It covers the oil-thickening, insolubles-formation, and deposit-formation characteristics of automotive manual transmission and final drive axle lubricating oils when subjected to high-temperature oxidizing conditions.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.2.1 Exceptions—The values stated in SI units for catalyst mass loss, oil mass and volume, alternator output, and air flow are to be regarded as standard.1.2.2 SI units are provided for all parameters except where there is no direct equivalent such as the units for screw threads, or where there is a sole source supply equipment specification.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning information is given in Sections 7 and 8 and Annex A7.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This laboratory test method can be used to quickly determine extreme pressure properties of lubricating greases at selected temperatures specified for use in applications where high-speed vibrational or start-stop motions are present with high Hertzian point contact. This test method has found wide application in qualifying lubricating greases used in constant velocity joints of front-wheel-drive automobiles. Users of this test method should determine whether results correlate with field performance or other applications.1.1 This test method covers a procedure for determining extreme pressure properties of lubricating greases under high-frequency linear-oscillation motion using the SRV test machine. This test method can also be used for evaluating extreme pressure properties of lubricating fluid.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The expanded limits of the Adjunct for VCF are defined in a mixture of terms of customary and metric units. Table 1 shows the defining limits and their associated units in bold italics. Also shown in Table 1 are the limits converted to their equivalent units (and, in the case of the densities, other base temperatures).5.2 Note that only the precision levels of the defining values shown in Table 1 are correct. The other values showing converted units have been rounded to the significant digits shown; as rounded values, they may numerically fall just outside of the actual limits established by the defining values.5.3 Table 2 provides a cross-reference between the historical table designations and the corresponding section in the Adjunct for VCF. Note that procedure paragraphs 11.1.6.3 (U.S. customary units) and 11.1.7.3 (metric units) provide methods for correcting on-line density measurements from live conditions to base conditions and then to compute CTPL factors for continuous volume corrections to base conditions.5.4 When a glass hydrometer is used to measure the density of a liquid, special corrections must be made to account for the thermal expansion of the glass when the temperature is different from that at which the hydrometer was calibrated. The 1980 CTL Tables had generalized equations to correct glass hydrometer readings, and these corrections were part of the printed odd-numbered tables. However, detailed procedures to correct a glass hydrometer reading are beyond the scope of the Adjunct for VCF. The user should refer to the appropriate sections of API MPMS Chapter 9 or other appropriate density/hydrometer standards for guidance.5.5 The set of correlations given in the Adjunct for VCF is intended for use with petroleum fluids comprising either crude oils, refined products, or lubricating oils that are single-phase liquids under normal operating conditions. The liquid classifications listed here are typical terms used in the industry, but local nomenclature may vary. The list is illustrative and is not meant to be all-inclusive.5.6 Crude Oils—A crude oil is considered to conform to the commodity group Generalized Crude Oils if its density falls in the range between approximately –10°API to 100°API. Crude oils that have been stabilized for transportation or storage purposes and whose API gravities lie within that range are considered to be part of the Crude Oil group. Also, aviation Jet B (JP-4) is best represented by the Crude Oil correlation.5.7 Refined Products—A refined product is considered to conform to the commodity group of Generalized Refined Products if the fluid falls within one of the refined product groups. Note the product descriptors are generalizations. The commercial specification ranges of some products may place their densities partly within an adjacent class (for example, a low-density diesel may lie in the jet fuel class). In such cases, the product should be allocated to the class appropriate to its density, not its descriptor. The groups are defined as follows:5.7.1 Gasoline—Motor gasoline and unfinished gasoline blending stock with a base density range between approximately 50°API and 85°API. This group includes substances with the commercial identification of: premium gasoline, unleaded gasoline, motor spirit, clear gasoline, low-lead gas, motor gasoline, catalyst gas, alkylate, catalytic cracked gasoline, naphtha, reformulated gasoline, and aviation gasoline.5.7.2 Jet Fuels—Jet fuels, kerosene, and Stoddard solvents with a base density range between approximately 37°API and 50°API. This group includes substances with the commercial identification of: aviation kerosene K1 and K2, aviation Jet A and A-1, kerosene, Stoddard solvent, JP-5, and JP-8.5.7.3 Fuel Oils—Diesel oils, heating oils, and fuel oils with a base density range between approximately –10°API and 37°API. This group includes substances with the commercial identification of: No. 6 fuel oil, fuel oil PA, low-sulfur fuel oil, LT (low temperature) fuel oil, fuel oil, fuel oils LLS (light low sulfur), No. 2 furnace oil, furnace oil, auto diesel, gas oil, No. 2 burner fuel, diesel fuel, heating oil, and premium diesel.5.8 Lubricating Oils—A lubricating oil is considered to conform to the commodity group Generalized Lubricating Oils if it is a base stock derived from crude oil fractions by distillation or asphalt precipitation. For the purpose of the Adjunct for VCF, lubricating oils have initial boiling points greater than 700 °F (370 °C) and densities in the range between approximately –10°API to 45°API.5.9 Special Applications—Liquids that are assigned the special applications category are generally relatively pure products or homogeneous mixtures with stable (unchanging) chemical composition that are derived from petroleum (or are petroleum-based with minor proportions of other constituents) and have been tested to establish a specific thermal expansion factor for the particular fluid. These tables should be considered for use when:5.9.1 The generalized commodity groups' parameters are suspected of not adequately representing the thermal expansion properties of the liquid.5.9.2 A precise thermal expansion coefficient can be determined by experiment. A minimum of ten temperature/density data points is recommended to use this method. See 11.1.5.2 of the Adjunct for VCF for the procedure to calculate the thermal expansion coefficient from measured density data.5.9.3 Buyer and seller agree that, for their purpose, a greater degree of equity can be obtained using factors specifically measured for the liquid involved in the transaction.5.10 Refer to paragraphs 11.1.2.4 and 11.1.2.5 in the Adjunct for VCF for a complete description of the suitability of the implementation procedures for specific hydrocarbon liquids.1.1 This guide provides information related to the algorithm and implementation procedure but does not contain the full set of algorithms. The algorithms, instructions, procedures, and examples are located in the associated supplementary adjuncts. The Adjunct for Volume Correction Factors (VCF) for temperature and pressure volume correction factors for generalized crude oils, refined products, and lubricating oils provides the algorithm and implementation procedure for the correction of temperature and pressure effects on density and volume of liquid hydrocarbons. Natural gas liquids (NGLs) and liquefied petroleum gases (LPGs) are excluded from consideration in this standard but may be found in API MPMS Chapter 11.2.4/GPA 8217 Temperature Correction for NGL and LPG. As this Adjunct for VCF will be applied to a variety of applications, the output parameters of CTL, Fp, CPL, and CTPL may be used as specified in other standards.1.2 Including the pressure correction in the Adjunct for VCF represents an important change from the “temperature only” correction factors given in the 1980 Petroleum Measurement Tables. However, if the pressure is one atmosphere (the standard pressure), then there is no pressure correction and the standard/adjunct(s) will give CTL values consistent with the 1980 Petroleum Measurement Tables.1.3 The Adjunct for VCF covers general procedures for the conversion of input data to generate CTL, Fp, CPL, and CTPL values at the user-specified base temperature and pressure (Tb, Pb). Two sets of procedures are included for computing volume correction factor: one set for data expressed in customary units (temperature in °F, pressure in psig); the other for the metric system of units (temperature in °C, pressure in kPa or bar).NOTE 1: In contrast to the 1980 Petroleum Measurement Tables, the metric procedures require the procedure for customary units be used first to compute density at 60 °F. This value is then further corrected to give the metric output. The metric procedures now incorporate the base temperature of 20 °C in addition to 15 °C.1.4 The procedures in the Adjunct for VCF recognize three distinct commodity groups: crude oil, refined products, and lubricating oils. A procedure is also provided for determining volume correction for special applications where the generalized commodity groups’ parameters may not adequately represent the thermal expansion properties of the liquid and a precise thermal expansion coefficient has been determined by experiment. Procedures for determining Volume Correction Factors (VCF) for Denatured Ethanol can be found in API MPMS Chapter 11.3.3, Miscellaneous Hydrocarbon Properties—Denatured Ethanol Density and Volume Correction Factors, 3rd edition. Procedures for determining Volume Correction Factors (VCF) for Gasoline and Denatured Ethanol Blends can be found in API MPMS Chapter 11.3.4, Miscellaneous Hydrocarbon Properties—Denatured Ethanol and Gasoline Component Blend Densities and Volume Correction Factors, 1st edition.1.5 The values stated in either SI units or inch‐pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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6.1 The quantitative determination of remaining antioxidants for in-service industrial oils by measuring the amount of these additives that have been added to the oil as protection against oxidation. Industrial lubricants, such as turbine oils, compressor oils, gear oils, hydraulic oils, bearing lubricants and greases can be formulated with a wide variety of antioxidants types such as phenols and amines (as primary antioxidants), which are working synergistically and therefore all important to be monitored individually. For in-service oils, the LSV determines and compares the amount of original primary antioxidants remaining after oxidation have reduced its initial concentration.6.2 This guide covers procedures for primary antioxidants such as amines and phenols, as described by Test Method D6971 and D6810.6.3 LSV is not designed or intended to detect all of the antioxidant intermediates formed during the thermal and oxidative stressing of the oils, which are recognized as having some contribution to the remaining useful life of the used or in-service oil. In order to measure the overall stability of an oil (including contribution of intermediates present), and before making final judgment on the remaining useful life of the used oil (which might result in the replacement of the oil reservoir), it is advised to perform additional analytical techniques (in accordance with Practice D4378 and Practice D6224).6.4 This guide is applicable to a wide range of industrial oils, both mineral or synthetic based, which can contain rust and oxidation inhibitors, antiwear additives such as zinc dialkyl dithiophosphates on gear oils, circulating oils, transmission oils and other industrial lubricating oils.6.5 The test is also suitable for manufacturing control and specification acceptance.6.6 When a voltammetric analysis is obtained for a industrial lubricant inhibited with at least one type of antioxidant, there is an increase in the current of the produced voltammogram between 5 s to 8 s (or 0.5 V to 0.8 V applied voltage) (see Note 1) for the zinc dialkyl dithiophosphate type of antioxidant (Fig. 1), an increase in the current of the produced voltammogram between 8 s to 12 s (or 0.8 V to 1.2 V applied voltage) (Fig. 2) (see Note 1) for the aromatic amines, and increase in the current of the produced voltammogram between 13 s and 16 s (or 1.3 V to 1.6 V applied voltage) (see Note 1) for the hindered phenols or carbamates in the neutral acetone solution (Fig. 2: x-axis 1 s = 0.1 V), or both. Hindered phenol antioxidants detected by voltammetric analysis include, but are not limited to, 2,6-di-tert -butyl-4-methylphenol; 2,6-di-tert-butylphenol and 4,4’-Methylenebis(2,6-di-tert-butylphenol). Aromatic amine antioxidants detected by voltammetric analysis include, but are not limited to, phenyl alpha naphthylamines, and alkylated diphenylamines.FIG. 2 Aromatic Amine and Hindered Phenol Voltammetric Response in the Neutral Test Solution with Blank Response ZeroedNOTE 1: Voltages listed with respect to reference electrode. The voltammograms shown in Figs. 1-6 were obtained with a platinum reference electrode and a voltage scan rate of 0.1 V/s.FIG. 3 Hindered Phenol Voltammetric Response in Basic Test Solution with Blank Response ZeroedFIG. 4 Voltammetric Reading for an In-service Oil Sample Comparing Aromatic Amines (additive #1) and Hindered Phenols (additive #2) Peaks (in the Neutral Test Solution)—Standard (top line) and Sample In-Service Oil (lower line)FIG. 5 a Filming Problems Due to Oil SolubilityFIG. 5 b Filming Due to Additive Concentration (continued)FIG. 5 c Filming Problems Due to Oil Solubility (continued)FIG. 6 Shifting of Antioxidant Peaks Due to Oil Solubility6.7 For industrial lubricants containing zinc dialkyl dithiophosphate type of antioxidants, there is an increase in the current of the produced voltammogram between 5 s to 8 s (or 0.5 V to 0.8 V applied voltage) (see Note 1) by using the neutral acetone test solution (see Fig. 1). There is no corresponding ASTM International standard describing the test method procedures for measuring zinc dialkyl dithiophosphates type of antioxidants in industrial lubricants.6.8 For industrial lubricants containing only aromatic amines as antioxidants, there is an increase in the current of the produced voltammogram between 8 s to 12 s (or 0.8 V to 1.2 V applied voltage) (see Note 1) for the aromatic amines, by using the neutral acetone test solution (first peak in Fig. 2) as described in Test Method D6971.6.9 For industrial lubricants containing only hindered phenolic antioxidants, it is preferable to use a basic alcohol solution rather than the neutral acetone solutions, to achieve an increase in the current of the produced voltammogram between 3 s to 6 s (or 0.3 V to 0.6 V applied voltage) (see Note 1) in basic alcohol solution (Fig. 3: x-axis 1 s = 0.1 V) as described in Test Method D6810.1.1 This guide covers the voltammetric analysis for qualitative measurements of primary antioxidants in new or in-service type industrial lubricants detectable in concentrations as low as 0.0075 % by mass up to concentrations found in new oils by measuring the amount of current flow at a specified voltage in the produced voltammogram.1.2 This guide can be used as a resource for a condition monitoring program to track the oxidative health of a range of industrial lubricants which contain primary antioxidants. In order to avoid excessive degradation of the base-oil, these primary antioxidants play a major role to protect the lubricants against thermal-oxidative degradation. This guide can help users with interpretation and troubleshooting results obtained using linear sweep voltammetry (LSV).1.3 When used as part of oil condition monitoring practices, it is important to apply trend analysis to monitor the antioxidant depletion rate relative to a baseline sample rather than use voltammetry for an absolute measurement of the antioxidant concentration. The trending pattern provides a proactive means to identify the level of oil degradation or abnormal changes in the condition of the in-service lubricant.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method usually requires several minutes per sample. This test method covers eight elements and thus provides more elemental composition data than Test Method D4628 or Test Methods D4927. In addition, this test method provides more accurate results than Test Method D5185, which is intended for used lubricating oils and base oils.4.2 Additive packages are blends of individual additives, which can act as detergents, antioxidants, antiwear agents, and so forth. Many additives contain one or more elements covered by this test method. Additive package specifications are based, in part, on elemental composition. Lubricating oils are typically blends of additive packages, and their specifications are also determined, in part, by elemental composition. This test method can be used to determine if additive packages and unused lubricating oils meet specifications with respect to elemental composition.4.3 Several additive elements and their compounds are added to the lubricating oils to give beneficial performance (Table 1).1.1 This test method covers the quantitative determination of barium, boron, calcium, copper, magnesium, molybdenum, phosphorus, sulfur, and zinc in unused lubricating oils and additive packages.1.2 The precision statements are valid for dilutions in which the mass % sample in solvent is held constant in the range of 1 % to 5 % by mass of oil.1.3 The precision tables define the concentration ranges covered in the interlaboratory study. However, both lower and higher concentrations can be determined by this test method. The low concentration limits are dependent on the sensitivity of the ICP instrument and the dilution factor. The high concentration limits are determined by the product of the maximum concentration defined by the linear calibration curve and the sample dilution factor.1.4 Sulfur can be determined if the instrument can operate at a wavelength of 180 nm.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method can be used to determine anti-wear properties and coefficient of friction of greases in order to prevent “fretting” wear under linear oscillation with associated low strokes and high Hertzian contact pressures at selected temperatures and loads specified for use in applications in which induced, high-speed vibrational motions are present for extended periods of time. It has found application as a screening test for grease lubricants used in ball and roller bearings, roller or ball screw (spindle) drives or side shaft systems (Tripode or Rzeppa type) for example, so-called constant velocity (CV) joints. Users of this test method should determine whether results correlate with field performance or other applications.1.1 This test method covers a procedure for determining the lubricating action of greases in order to prevent “fretting” wear under linear oscillation with associated low strokes and high Hertzian contact pressures under high-frequency linear-oscillation motion using the SRV test machine. By performing additional, nonmandatory extreme-pressure tests in accordance with Test Method D5706, the test grease should be shown to be able to withstand a Hertzian contact pressure of at least 2200 MPa without adhesive failure.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Coagulated pentane insolubles can include oil-insoluble materials, some oil-insoluble resinous matter originating from oil or additive degradation, soot from incomplete diesel fuel combustion, or a combination of all three.5.2 A significant change in coagulated pentane insolubles indicates a change in oil, and this could lead to lubrication system problems.5.3 Coagulated pentane insolubles measurements can also assist in evaluating the performance characteristics of a used oil or in determining the cause of equipment failure.5.4 High values of coagulated pentane insolubles have been associated with plugged oil filters, leading to opening of the bypass valve and circulation of unfiltered oil in the engine. This can lead to increased piston deposits, increased bearing wear, and premature engine failure.1.1 This test method covers the determination of coagulated pentane insolubles in used lubricating oils by a paper filtration method.1.2 This test method was originally developed by the Fuels, Lubricants, and Environmental Committee (FL&E) of the Locomotive Maintenance Officer’s Association (LMOA).21.3 This test method is used primary for testing used diesel engine oils from railroad locomotive service. It may be applied to other samples types but precision, bias, and significance have not been determined for samples other than used railroad locomotive diesel engine oils.1.4 This test method, in general, does not correlate with Test Method D893 on Insolubles in Lubricating Oils, since it uses separation by centrifugation and a more concentrated solution of anti-coagulant.1.5 The correlation between this test method and Appendix A4 (Enhanced Thermal Gravimetric Analysis (TGA) Procedure) in Test Method D5967 has not been investigated.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.2, 7.3, and 7.4.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method estimates the resistance of greases to water washout from ball bearings under conditions of the test. No correlation with field service has been established.1.1 This test method covers the evaluation of the resistance of a lubricating grease to washout by water from a bearing, when tested at 38 °C and 79 °C (100 °F and 175 °F) under the prescribed laboratory conditions. It is not to be considered the equivalent of service evaluation tests. Precision and bias was determined using grease ranging from NLGI 3 to 0 grades in the research report (see Section 10).1.2 This test method may not be suitable for some greases containing highly volatile components. This test method does not attempt to account for sample evaporation. It is the user's responsibility to determine if evaporation of the sample is a significant contributor to mass loss at the required drying temperature.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 6.3.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The vapor pressure of a substance as determined by measurement of evaporation reflects a property of the bulk sample. Little weight is given by the procedure to the presence of low concentrations of volatile impurities.5.2 Vapor pressure, per se, is a thermodynamic property that is dependent only upon composition and temperature for stable systems. In the present method, composition changes occur during the course of the test so that the contribution of minor amounts of volatile impurities is minimized.1.1 This test method covers a calculation procedure for converting data obtained by Test Method D972 to apparent vapor pressures and molecular weights. It has been demonstrated to be applicable to petroleum-based and synthetic ester lubricating oils,2 at temperatures of 395 K to 535 K (250 °F to 500 °F). However, its applicability to lubricating greases has not been established.NOTE 1: Most lubricants boil over a fairly wide temperature range, a fact recognized in discussion of their vapor pressures. For example, the apparent vapor pressure over the range 0 % to 0.1 % evaporated may be as much as 100 times that over the range 4.9 % to 5.0 % evaporated.1.2 The values stated in SI units are to be regarded as the standard. In cases in which materials, products, or equipment are available in inch-pound units only, SI units are omitted.1.3 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability or regulatory limitations prior to use. For specific warning statements, see 6.2, 7.1, 8.2, and Annex A2.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The concentration of nitrogen is a measure of the presence of nitrogen-containing additives. Knowledge of its concentration can be used to predict performance.1.1 This test method covers the determination of nitrogen in lubricating oils when present in the concentration from 0.03 % to 0.10 % by mass, and for the determination of nitrogen in fuel oils when present in the concentration from 0.015 % to 2.0 % by mass. This test method is also applicable to the analysis of additive concentrates and additive packages.NOTE 1: This test method may not be applicable to certain materials containing N–O or N–N linkage. However, the samples used in the cooperative program to establish the precision of the test method were compounded with currently available ashless additives containing nitrogen. Complete recovery of the nitrogen present in these additives was obtained.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.6, 7.9, and 9.8.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method can be used to determine wear properties and coefficient of friction of lubricating greases at selected temperatures and loads specified for use in applications where high-speed vibrational or start-stop motions are present for extended periods of time under initial high Hertzian point contact pressures. This test method has found application in qualifying lubricating greases used in constant velocity joints of front-wheel-drive automobiles and for lubricating greases used in roller bearings. Users of this test method should determine whether results correlate with field performance or other applications.1.1 This test method covers a procedure for determining a lubricating grease's coefficient of friction and its ability to protect against wear when subjected to high-frequency, linear-oscillation motion using an SRV test machine at a test load of 200 N, frequency of 50 Hz, stroke amplitude of 1.00 mm, duration of 2 h, and temperature within the range of the test machine, specifically, ambient to 280 °C. Other test loads (10 N to 1200 N for SRVI-model, 10 N to 1400 N for SRVII-model, and 10 N to 2000 N for SRVIII-model), frequencies (5 Hz to 500 Hz) and stroke amplitudes (0.1 mm up to 4.0 mm) can be used, if specified. The precision of this test method is based on the stated parameters and test temperatures of 50 °C and 80 °C. Average wear scar dimensions on ball and coefficient of friction are determined and reported.NOTE 1: Optimol Instruments supplies an upgrade kit to allow SRVI/II-machines to operate with 1600 N, if needed.1.2 This test method can also be used for determining a fluid lubricant's ability to protect against wear and its coefficient of friction under similar test conditions.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Fluid analysis is one of the pillars in determining fluid and equipment conditions. The results of fluid analysis are used for planning corrective maintenance activities, if required.5.2 The objective of a proper fluid sampling process is to obtain a representative fluid sample from critical location(s) that can provide information on both the equipment and the condition of the lubricant or hydraulic fluid.5.3 The additional objective is to reduce the probability of outside contamination of the system and the fluid sample during the sampling process.5.4 The intent of this guide is to help users in obtaining representative and repeatable fluid samples in a safe manner while preventing system and fluid sample contamination.1.1 This guide is applicable for collecting representative fluid samples for the effective condition monitoring of steam and gas turbine lubrication and generator cooling gas sealing systems in the power generation industry. In addition, this guide is also applicable for collecting representative samples from power generation auxiliary equipment including hydraulic systems.1.2 The fluid may be used for lubrication of turbine-generator bearings and gears, for sealing generator cooling gas as well as a hydraulic fluid for the control system. The fluid is typically supplied by dedicated pumps to different points in the system from a common or separate reservoirs. Some large steam turbine lubrication systems may also have a separate high pressure pump to allow generation of a hydrostatic fluid film for the most heavily loaded bearings prior to rotation. For some components, the lubricating fluid may be provided in the form of splashing formed by the system components moving through fluid surfaces at atmospheric pressure.1.3 Turbine lubrication and hydraulic systems are primarily lubricated with petroleum based fluids but occasionally also use synthetic fluids.1.4 For large lubrication and hydraulic turbine systems, it may be beneficial to extract multiple samples from different locations for determining the condition of a specific component.1.5 The values stated in SI units are regarded as standard.1.5.1 The values given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method covers the rapid determination of 22 elements in used and unused lubricating oils and base oils, and it provides rapid screening of used oils for indications of wear. Test times approximate a few minutes per test specimen, and detectability for most elements is in the low mg/kg range. In addition, this test method covers a wide variety of metals in virgin and re-refined base oils. Twenty-two elements can be determined rapidly, with test times approximating several minutes per test specimen.5.2 When the predominant source of additive elements in used lubricating oils is the additive package, significant differences between the concentrations of the additive elements and their respective specifications can indicate that the incorrect oil is being used. The concentrations of wear metals can be indicative of abnormal wear if there are baseline concentration data for comparison. A marked increase in boron, sodium, or potassium levels can be indicative of contamination as a result of coolant leakage in the equipment. This test method can be used to monitor equipment condition and define when corrective actions are needed.5.2.1 The significance of metal analysis in used lubricating oils is tabulated in Table 4.5.3 The concentrations of metals in re-refined base oils can be indicative of the efficiency of the re-refining process. This test method can be used to determine if the base oil meets specifications with respect to metal content.1.1 This test method covers the determination of additive elements, wear metals, and contaminants in used and unused lubricating oils and base oils by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in Table 1.(A) These wavelengths are only suggested and do not represent all possible choices.1.2 This test method covers the determination of selected elements, listed in Table 1, in re-refined and virgin base oils.1.3 For analysis of any element using wavelengths below 190 nm, a vacuum or inert-gas optical path is required. The determination of sodium and potassium is not possible on some instruments having a limited spectral range.1.4 This test method uses oil-soluble metals for calibration and does not purport to quantitatively determine insoluble particulates. Analytical results are particle size dependent, and low results are obtained for particles larger than a few micrometers.21.5 Elements present at concentrations above the upper limit of the calibration curves can be determined with additional, appropriate dilutions and with no degradation of precision.1.6 For elements other than calcium, sulfur, and zinc, the low limits listed in Table 2 and Table 3 were estimated to be ten times the repeatability standard deviation. For calcium, sulfur, and zinc, the low limits represent the lowest concentrations tested in the interlaboratory study.(A) where: X = mean concentration, μg/g.(A) where: X = mean concentration, μg/g.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 6.1, 8.2, and 8.4.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Lubricating greases are used in almost all bearings used in any machinery. Lubricating grease is composed of ~90 % additized oil and soap or other thickening agent. There are over a dozen metallic elements present in greases, either blended as additives for performance enhancements or as thickeners, or in used greases present as contaminants and wear metals. Determining their concentrations can be an important aspect of grease manufacture. The metal content can also indicate the amount of thickeners in the grease. Additionally, a reliable analysis technique can also assist in the process of trouble shooting problems with new and used grease in the field.5.2 Although widely used in other sectors of the oil industry for metal analysis, ICP-AES based Test Methods D4951 or D5185 cannot be used for analyzing greases because of their insolubility in organic solvents used in these test methods. Hence, grease samples need to be brought into aqueous solution by acid decomposition before ICP-AES measurements.5.3 Test Method D3340 has been used to determine lithium and sodium content of lubricating greases using flame photometry. This technique is no longer widely used. This new test method provides a test method for multi-element analysis of grease samples. This is the first D02 standard available for simultaneous multi-element analysis of lubricating greases.1.1 This test method covers the determination of a number of metals such as aluminum, antimony, barium, calcium, iron, lithium, magnesium, molybdenum, phosphorus, silicon, sodium, sulfur, and zinc in unused lubricating greases by inductively coupled plasma atomic emission spectrometry (ICP-AES) technique.1.1.1 The range of applicability for this test method, based on the interlaboratory study conducted in 2005,2 is aluminum (10 to 600), antimony (10 to 2300), barium (50 to 800), calcium (20 to 50 000), iron (10 to 360), lithium (300 to 3200), magnesium (30 to 10 000), molybdenum (50 to 22 000), phosphorus (50 to 2000), silicon (10 to 15 000), sodium (30 to 1500), sulfur (1600 to 28 000), and zinc (300 to 2200), all in mg/kg. Lower levels of elements may be determined by using larger sample weights, and higher levels of elements may be determined by using smaller amounts of sample or by using a larger dilution factor after sample dissolution. However, the test precision in such cases has not been determined, and may be different than the ones given in Table 3.1.1.2 It may also be possible to determine additional metals such as bismuth, boron, cadmium, chromium, copper, lead, manganese, potassium, titanium, etc. by this technique. However, not enough data is available to specify the precision for these latter determinations. These metals may originate into greases through contamination or as additive elements.1.1.3 During sample preparation, the grease samples are decomposed with a variety of acid mixture(s). It is beyond the scope of this test method to specify appropriate acid mixtures for all possible combination of metals present in the sample. But if the ash dissolution results in any visible insoluble material, the test method may not be applicable for the type of grease being analyzed, assuming the insoluble material contains some of the analytes of interest.1.2 Elements present at concentrations above the upper limit of the calibration curves can be determined with additional appropriate dilutions of dissolved samples and with no degradation of precision.1.3 The development of the technique behind this test method is documented by Fox.31.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Sections 8 and 10.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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