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5.1 The metallurgical properties of materials used to manufacture absorbable metallic implants can influence biological reactions and mechanical interaction with soft and hard tissue in the body. This standard guide describes a suggested material characterization scheme for absorbable metallic materials to ensure reproducibility of properties prior to their manufacture into medical implants.1.1 This guidance document provides metallurgical characterization information that may be beneficial in the evaluation of absorbable metallic materials intended for medical implant applications. This guide is primarily intended for absorbable metallic materials that undergo further processing into a fabricated final device. Therefore, this standard does not require assessments that are more appropriately conducted on the final device, such as biological evaluation. However, a few relevant standards for finished implant devices are included for information purposes.1.2 The purpose of this guide is to identify appropriate test methods and relevant medical product standards that can be used to develop future standards for new or modified absorbable metallic materials.1.3 This guide is not intended to cover other major classes of absorbable materials such as polymers, ceramics, composites, and tissue-engineered materials.1.4 This standard guide is focused on the chemical, physical, microstructural, and mechanical properties plus inspection guidelines for metallic materials that are used for medical implants designed to be absorbed in the body over a period of time. This guide focuses on material characterizations and does not address device specific mechanical testing that may be necessary to determine safety and functionality of the implant.1.5 Compliance with materials specifications developed in accordance with this standard may not necessarily result in a material suitable for its intended purpose. Additional testing specific to the intended use may be required.1.6 Since surface modifications of medical implants are generally applied in the latter stages of manufacturing, this standard guide does not cover the characterization of either absorbable or non-absorbable surface coatings that are metallic in origin such as oxides or from the addition of other materials such as ceramics or polymers. However, this standard does apply to absorbable metallic materials, regardless of the presence or absence of a coating.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This guide defines a procedure for testing components being considered for installation into a high-purity gas distribution system. Application of this guide is expected to yield comparable data among components tested for purposes of qualification for this installation.4.2 This guide establishes a procedure for determining the elemental composition and metallurgical characteristics of metal used to fabricate components for high purity gas distribution systems in the semiconductor industry. The composition and metallurgy of stainless steel may be expected to affect properties of importance to this application, including surface roughness, incidence of surface defects, passivation, corrosion resistance, and welding.1.1 This guide covers corrosion resistant metallic alloys of the general class stainless steel, containing chromium, nickel, manganese, and silicon as major alloying additions and possibly molybdenum, that are qualified or specified for the materials of components used in high-purity gas supply systems for the semiconductor industry. This guide is primarily intended for testing to determine conformance to applicable composition and metallurgical specifications as stated in supplier product specifications or customer purchase specifications, or both.1.2 Elements analyzed and reported in this guide are as follows:1.2.1 The alloying additions chromium, nickel, and molybdenum (if specified in alloy, as in type 316L),1.2.2 The minor elements and residuals manganese, silicon, copper, cobalt, and stabilizers such as titanium and columbium (niobium), if present,1.2.3 Carbon, sulfur and phosphorus,1.2.4 Nitrogen and oxygen gases,1.2.5 Any additional minor element additions that may be made as part of the melting and casting practice, such as aluminum and calcium,1.2.6 Available standard analytical and reporting techniques are described for these elements.1.3 Metallurgical characteristics to be analyzed and reported are inclusion contents, grain structure, mechanical properties, and intergranular corrosion susceptibility.1.4 Limitations: 1.4.1 This guide is limited to corrosion resistant metal alloys of the general class stated in the .1.4.2 The test methods cited in this guide are not intended to preclude the use of other generally accepted techniques of demonstrated equivalent or superior precision and bias.1.4.3 Inclusion of testing and analysis procedures for any given element or metallurgical characteristic in this guide is not to be construed as being a requirement for incorporation of that element or metallurgical characteristic into any specifications.1.5 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is primarily to be used to dry samples for determination of total mercury. It should not be used for determination of sample moisture content. Most sample preparation methods prescribe drying samples at 105 °C, until a constant mass is obtained. The moisture content is determined as the percent mass loss on drying. Because mercury and some of its compounds are volatile at 105 °C, samples for mercury determination shall be dried at 60 °C (see Practice E877, ISO 9599, ISO 12743, and ISO 10251).5.2 It is assumed that all who use this practice will be trained analysts capable of performing skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.1.1 This practice covers the sample drying step for the determination of mercury in ores, concentrates, and related metallurgical materials.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice is intended as a rapid means for obtaining an extract of solid waste. The extract may be used to estimate the release of constituents of the solid waste under the laboratory conditions described in this procedure.4.1.1 This practice is not intended to be used as a kinetic test to simulate weathering of ore, metal mining, and metallurgical processing wastes. For kinetic testing of ore, metal mining, and metallurgical processing wastes, refer to Test Method D5744 to determine release rates for constituents of interest. For static testing of metal mining ore and metal mining or metallurgical processing waste materials, refer to Test Methods E1915 and D6234. If the conditions of this practice are not suitable for the test material, Test Method E2242 may be used, if applicable to the ore or waste.4.2 This practice is not intended to provide an extract that is representative of the actual leachate produced from a solid waste in the field, or to produce extracts to be used as the sole basis of engineering design.4.3 This practice is not intended to simulate site-specific leaching conditions. It has not been demonstrated to simulate actual disposal site leaching conditions.4.4 The intent of this practice is that the final pH of the extract reflects the interaction of the extractant with the buffering capacity of the solid waste.4.5 The intent of this practice is that the water extraction simulates conditions where the solid waste is the dominant factor in determining the pH of the extract.4.6 The practice produces an extract that is amenable to the determination of both major and minor constituents. When minor constituents are being determined, it is especially important that precautions are taken in sample storage and handling to avoid possible contamination of the samples.4.6.1 This practice has been tested to determine its applicability to certain inorganic components in metal mining and metallurgical processing wastes.4.7 The practice has not been tested for applicability to organic substances and volatile matter.1.1 This practice covers a procedure for leaching of solid waste to obtain an aqueous solution to be used to determine the constituents leached under the specified testing conditions.1.1.1 This practice includes a procedure for the shake leaching of metal mining ore, waste rock, or metallurgical processing waste containing at least 80 % dry solids (≤20 % moisture) in order to generate a solution to be used to determine the inorganic constituents leached under the specified testing conditions and for regulatory jurisdictions requiring a water leach practice.1.2 This practice provides for the shaking of a known mass of waste with water of specified composition and the separation of the aqueous phase for analysis.1.2.1 This practice is intended to describe the procedure for performing single-batch extractions only. It does not describe all types of sampling, sample preservation, and analytical requirements that may be associated with its application.1.3 The values stated in SI units are to be regarded as standard. Values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 These methods are primarily intended to be used for the determination of silver correction in the fire assay silver determination. Silver assays are determined by fire assay for the purpose of metallurgical exchange between seller and buyer.5.2 It is assumed that all who use this method will be trained analysts capable of performing skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.1.1 This practice covers the determination of silver corrections for fire assay of metal bearing ores, concentrates, and related metallurgical materials using the spent slags and cupels from the fire assay process, by gravimetry and atomic absorption spectrophotometry.1.2 The test methods appear in the following order:  SectionsGravimetric Method 10–11Atomic Absorption Method 12–131.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (See Practices E50 and ISO Guide 35:1989.)1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These practices are primarily intended to test materials for compliance with compositional specifications and for monitoring. Partial extraction of ores and related metallurgical materials can provide information on the availability of elements to leaching, water quality changes, or other site conditions.4.2 It is assumed that the users of these practices will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices such as those described in Guide E882 shall be followed.1.1 These practices cover the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of acid-extractable contents of certain elements by such solution analytical techniques as atomic absorption spectrometry (AAS), inductively coupled plasma atomic emission spectrometry (ICP-AES) (see Test Method D1976), and inductively coupled plasma mass spectrometry (ICP-MS) (see Test Method D5673).1.1.1 Contents of aluminum, antimony, arsenic, barium, beryllium, bismuth, boron, cadmium, calcium, chromium, cobalt, copper, gallium, iron, lead, lithium, magnesium, manganese, mercury, molybdenum, nickel, phosphorus, potassium, scandium, selenium, silver, sodium, strontium, thallium, tin, titanium, vanadium and zinc can be extracted from ores and related metallurgical materials for determination by analytical methods for elements in solution. Other elements may be determined from extracts produced using this practice.1.1.2 Actual element quantification in digested solutions can be accomplished by following the various test methods under other appropriate ASTM standards for element(s) of interest in solution.1.1.3 The detection limit and linear content range for each element is dependent on the atomic absorption, mass spectrometry or emission spectrometric technique employed and may be found in the manual accompanying the instrument used or ASTM standard method for analysis of the solutions. Consider the dilution factor in content calculations due to digestion and dilution of solid samples.1.1.4 The extent of extraction of elements from ores and related metallurgical materials by these practices is dependent upon the physical and mineralogical characteristics of the prepared sample and the digestion practice used.1.2 The digestion practices appear in the following order:  SectionsNitric Acid Microwave Digestion 7 to 14Four-Acid Total Digestion 15 to 211.3 The values stated SI units are to be regarded as the standard. No other units of measurements are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 11 and 20.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is primarily intended to be used for the correction of silver loss in the fire assay process. Silver contents are determined by fire assay for the purpose of metallurgical exchange between buyer and seller. It is assumed that all who use this practice will be trained analysts capable of performing skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.1.1 This practice covers the silver loss correction, utilizing slag recycling and cupellation of proof silver during the fire assay of metal bearing ores, concentrates, and related metallurgical materials.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (See Practices E50 and ISO 35:2006.)1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The determination of the volume percent of the textural components in coke is useful to characterize the optical properties of coke as it relates to utilization. Specifically, the technique has been used as an aid in determining coal blend proportions, and recognition of features present in the coke that can be responsible for coke quality or production problems such as reduced coke strength or difficulty in removing coke from commercial coke ovens, or both. The study of coke textures is also useful in promoting a better understanding of coke reactivity, and the relationship between coal petrography and its conversion to coke.55.2 This test method is used in scientific and industrial research, but not for compliance or referee tests.1.1 This test method covers the equipment and procedures used for determining the types and amounts of coke carbon forms and associated recognizable coal- and process-derived textural components in metallurgical coke in terms of volume percent. This test method does not include coke structural components such as coke pores, coke wall dimensions, or other structural associations.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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