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Preservatives of the metallic series and oil soluble preservatives are not readily apparent in a cross section of wood either due to similar color to the species of wood or lack of color of the preservative itself. Chemical staining of a treated specimen of wood reveals the presence of the preservative. The sapwood and heartwood of Douglas-Fir and the pine species can be differentiated by a chemical stain.1.1 These test methods cover procedures for determining penetration of preservatives in wood in cases where demarcation between the treated and untreated wood is not readily visible. Included are test methods for differentiating the heartwood and the sapwood of wood samples for specific species, and a test method for differentiating the heartwoods between the red oaks and the white oaks. 1.2 The procedures appear in the following order: Procedure Sections Penetration of Arsenic-Containing Preservatives 6 to 8 Penetration of Copper-Containing Preservatives 9 to 11 Penetration of Fluoride-Containing Preservatives 12 to 15 Penetration of Pentachlorophenol Using 4,4[prime]-bis-Dimethylamino-Triphenylmethane (DMTM) 16 to 20 Penetration of Pentachlorophenol Using a Silver-Copper Complex Known as "Penta-Check" 21 to 24 Penetration of Solvent Used With Oil-Soluble Preservatives 25 to 28 Penetration of Zinc-Containing Preservatives 29 to 32 Differentiating between Sapwood and Heartwood in Pine Species (Pinus sp.) 33 to 36 Differentiating between Sapwood and Heartwood in Douglas Fir (Pseudotsuga menziesii) 37 to 40 Differentiating between Sapwood and Heartwood in White Fir (Abies concolor) 41 to 44 Differentiating Between Woods of the Red Oak and the White Oak Species 45 to 48 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is normally used to evaluate the barrier effectiveness against penetration of liquids through materials, seams, closures, or other planar assemblies used in protective clothing and specimens from finished items of protective clothing.5.1.1 Finished items of protective clothing include gloves, arm protectors, aprons, coveralls, suits, hoods, boots, and similar items.5.1.2 The phrase “specimens from finished items” is permitted to include continuous regions of protective clothing items as well as seamed or other discontinuous regions of protective clothing.5.1.3 The types of specimens are limited to those that are relatively flat (planar) that are capable of being sealed in the test cell specified in this test method without peripheral leakage.5.2 A substitute challenge liquid (for example, water or isopropanol) is appropriate in some cases to generalize material penetration resistance to liquids. However, it is possible that differences in chemical and molecular properties (for example, surface tension) may lead to different results.5.3 In addition to the failure mode where a liquid finds a pathway for penetration through a void, imperfection, or defect in material or clothing subassembly, some selected chemicals cause degradation of barrier material, film, or coating, leading to penetration over extended periods of contact.75.4 Five different procedures for how the specimen is exposed to the liquid are provided in Table 1. In this test method, all procedures involve liquid exposure that is continuous over the duration of the test. These procedures entail different hydrostatic pressures and durations of liquid exposure.5.4.1 Procedures A, B, and C apply a set pressure (6.9 or 13.8 kPa [1 or 2 psig]) for a specified period of time (1 or 10 min) over a 15- or 60-min liquid exposure time.5.4.2 Procedures A and B represent the originally established methods of liquid contact developed by the National Institute for Occupational Safety and Health, where Procedure A involves the application of a test pressure (13.8 kPa [2 psig]) that has been found to discriminate the liquid barrier performance of materials, while a lower pressure (6.9 kPa [1 psig]) is used for Procedure B to accommodate materials that exhibit ballooning or extension when the 13.8 kPa (2 psig) pressure is applied.8,9 Both procedures entail exposure of the specimen for 5 min at ambient pressure followed by 10 min of exposure of the specimen to the test pressure.5.4.3 Procedure C was developed to account for potentially longer exposures where failure may also occur as the result of material or assembly degradation. Procedure C uses a 13.8 kPa (2 psig) test pressure for a portion of the test where the specimen is first exposed to the liquid at ambient pressure for 5 min, followed by 1 min at 13.8 kPa (2 psig), and continuing for 54 additional minutes at ambient pressure.5.4.4 Procedure D involves the sequential increase of pressure from ambient (0 kPa [0 psig]) to 68.9 kPa (10 psig) in increments of 3.5 kPa (0.5 psig) in 1-min intervals until liquid penetration is observed at a specific test pressure. The time interval between changes in pressure is set at 1 min to coincide with the time of applied pressure in Procedure C.5.4.5 Procedure E permits the test method user to specify the pressures and duration of the specimen’s exposure to the liquid.5.5 Different results are reported by the different procedures.5.5.1 Procedures A, B, and C results are reported as “pass” or “fail” for each replicate. Passing results indicate that no liquid penetration was observed over the duration of the test exposure.5.5.2 Procedure D results are reported as the test pressure at which liquid penetration was observed for each replicate.5.6 The choice of pressure/time sequence and type of test result are dependent on the objectives of the testing.5.6.1 Procedure C is specified in several different National Fire Protection Association standards for establishing the minimum barrier performance of protective clothing materials, seams, and closures of first responder protective clothing.5.6.2 Procedure D may be used when the pressure where penetration occurs is sought without a set pressure pass/fail criterion. Procedure D also has utility for assessing the robustness of protective clothing materials and assemblies as part of quality systems. It is also possible to use Procedure D to supplement the pass/fail results provided by Procedures A, B, and C.5.6.3 Procedure E permits setting a specific sequence of pressure/time exposures based on the specific needs for the testing.5.6.4 In this test method, a hydrostatic pressure is applied but does not necessarily correlate with a mechanical pressure against a semi-rigid or rigid surface.5.6.5 It is recommended that a human factors investigation, hazard/risk exposure assessment, or similar study be conducted to determine the most suitable procedure for relating the choice of a specific procedure for measuring protective clothing material liquid penetration resistance to the intended protective performance of the clothing material.5.7 This test method permits the use of a retaining screen for preventing the overextension of a specimen as pressure is applied. However, it is important that the selected retaining screen does not interfere with the observation of liquid penetration or affect the sealing of the specimen in the test cell.5.8 A critical feature of the test is how the specimen is sealed in the test cell. Inadequate sealing of the specimen can lead to a false result (observed liquid penetration that is due to the method of sealing rather than penetration through the specimen). It is recommended that any special means used to seal specimens in the test cell be validated for providing sufficient integrity of the specimen in the test cell, not contribute to specimen damage, and not interfere with the observation of liquid penetration. Special means used to seal specimens in the test cell should be documented in the report.5.9 A minimum number of three test specimens is established for this test method. However, it is also appropriate to establish sampling plans based on a specific acceptable quality limit using a larger number of specimens, depending on the application of the test method. Potential sampling plans for this approach are found in MIL-STD-105E, ANSI/ASQC Z1.4, and ISO 2859-1.5.10 This test method does not address the liquid penetration of full protective clothing or ensembles. Use Test Method F1359 to provide a complete evaluation of the liquid integrity of protective clothing or ensembles, particularly areas of the clothing or ensembles that cannot be directly assessed by this test method, such as interface areas between different items of clothing and equipment.1.1 This test method is used to test specimens of protective clothing materials, assemblies such as seams and closures, or interfaces used in the construction of protective clothing. The resistance to visible penetration of the test liquid is determined with the liquid in continuous contact with the normally outside (exterior) surface of the test specimen.1.2 This test method includes different procedures for maintaining the liquid in contact with the test specimen in terms of the length of exposure and the pressure applied. Suggestions are provided for how to select an appropriate procedure for liquid contact.1.3 In some cases, significant amounts of hazardous materials will permeate specimens that pass the penetration tests. For more sensitive analyses, use either Test Method F739 or F1383 to determine permeation.1.4 This test method does not address penetration of vapors through protective clothing materials.1.5 This test method is not applicable to non-planar protective clothing materials, interfaces, or assemblies such as the fingertips or crotch areas of gloves, which are possible failure points.1.6 This test method does not address the liquid penetration resistance of full protective clothing items or ensembles. Use Test Method F1359 for this purpose.1.7 The values as stated in inch-pound units are to be regarded as the standard. The values in parentheses are for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards are given in Section 7.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Advanced composite systems are used in a number of applications as shields to prevent penetration by projectiles. In general, the use of composites is more effective for blunt, rather than sharp, projectiles or in hybrid systems in which an additional shield can be used to blunt a sharp projectile. Knowledge of the penetration impact resistance of different material systems or the effects of environmental or in-service load exposure to the penetration resistance of given materials is useful for product development and material selection.5.2 An impact test used to measure the penetration resistance of a material can serve the following purposes:5.2.1 To quantify the effect of fiber architecture, stacking sequence, fiber and matrix material selection, and processing parameters on the penetration resistance of different composite materials;5.2.2 To measure the effects of environmental or in-service load exposure on the penetration impact resistance of a given material system; and5.2.3 As a tool for quality assurance requirements for materials designed for penetration resistance applications.5.3 The penetration resistance values obtained with this test method are most commonly used in material specification and selection and research and development activities. The data are not intended for use in establishing design allowables, as the results are specific to the geometry and physical conditions tested and are not generally scalable to other configurations.5.4 The reporting section requires items that tend to influence the penetration resistance of material systems. These include the following: fiber and matrix materials, fiber architecture, layup sequence, methods of material fabrication, environmental exposure parameters, specimen geometry and overall thickness, void content, specimen conditioning, testing environment and exposure time, specimen fixture and alignment, projectile mass and geometry, and projectile orientation at impact. Additional reporting requirements include size and description of damage, results of any pre- and post-test nondestructive inspection, impact velocity, accuracy of the velocity measurement apparatus, and whether or not the projectile penetrated the panel. Residual velocity is a desirable, but not a necessary, value to be reported.5.5 The reporting section shall also include the parameters of a statistical function that gives the probability of penetration as a function of impact kinetic energy (see 14.4).5.6 The relevant measurements that result from the impact test are the kinetic energy and impact velocity of the projectile and whether or not the projectile penetrated the specimen. An optional item to be measured is the loss in kinetic energy of the projectile as a function of impact velocity if measurements of the residual velocity are recorded.1.1 This test method measures the resistance of flat composite panels in one specific clamping configuration to penetration by a blunt projectile in free flight. In this test method, the term “penetration” is defined as the case in which the projectile travels completely through the composite panel and fully exits the back side. The composite materials may be continuous fiber angle-ply, woven or braided fiber-reinforced polymer matrix composites, or chopped fiber-reinforced composites. The resistance to penetration is quantified by a statistical function that defines the probability of penetration for a given kinetic energy.1.2 This test method is intended for composite test panels in which the thickness dimension is small compared with the test panel width and length (span to thickness on the order of 40 or greater).1.3 This test method is intended for applications such as jet engine fan containment, open rotor engine blade containment, or other applications in which protection is needed for projectiles at velocities typically lower than seen in ballistic armor applications. The typical impact velocity that this test is intended for is in the range of 100 to 500 m/s [300 to 1500 ft/s], as opposed to higher velocities associated with armor penetration.1.4 A flat composite panel is fixed between a circular-shaped clamping fixture and a large base fixture each with a large coaxial hole defining a region of the panel that is subjected to impact in the direction normal to the plane of the flat panel by a blunt projectile. Clamping pressure is provided by 28 through bolts that pass through the front clamp, the test specimen, and the back plate. The mass, geometry, desired impact kinetic energy, and impact orientation of the projectile with respect to the panel are specified before the test. Equipment and procedures are required for measuring the actual impact velocity and orientation during the test. The impact penetration resistance can be quantified by either the velocity or kinetic energy required for the projectile to penetrate the test panel fully. A number of tests are required to obtain a statistical probability of penetration for given impact conditions.1.5 This test method measures the penetration resistance for a specific projectile and test configuration and can be used to screen materials for impact penetration resistance, compare the impact penetration resistance of different composite materials under the same test geometry conditions, or assess the effects of in-service or environmental exposure on the impact penetration resistance of materials.1.6 The impact penetration resistance is highly dependent on the test panel materials and architecture, projectile geometry and mass, and panel boundary conditions. Results are not generally scalable to other configurations but, for the same test configurations, may be used to assess the relative impact penetration resistance of different materials and fiber architectures.1.7 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Within the text, the inch-pound units are shown in brackets.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 U.S. Department of Defense and U.S. Department of Justice standards and specifications require assessing the penetration resistance and backface deformation of ballistic-resistant body armor.5.2 This test method may be used by private-sector and government laboratories, manufacturers, research and development organizations, and others assessing the ballistic resistance of body armor or performing research and development of new materials.5.3 It is intended that this test method be referenced by other standards, specifications, or test methods.1.1 This test method addresses resistance to ballistic penetration and to backface deformation (BFD) for ballistic-resistant torso body armor and shoot packs.1.2 This test method is intended for testing of soft body armor, hard armor plates, in conjunction with armor, and shoot packs mounted on a clay block as the backing assembly.NOTE 1: This test method does not apply to ballistic helmets, inserts, trauma packs, trauma plates, or accessories.1.3 The test method does not specify performance criteria or usage of the test results.1.4 This test method does not address conditioning of test items.1.5 It is anticipated that this test method will be referenced by certifiers, purchasers, or other users in order to meet their specific needs.1.5.1 Purchasers and other users will specify the ballistic test threats to be used. Within this test method, the reference defining the ballistic test threats is called the “test threats document.”1.5.2 In this test method, “other standards and specifications” and “unless specified elsewhere” refer to documents (for example, military standards, purchase specifications) that require the use of this test method. Purchasers and other users are responsible for the “other standards and specifications” and for specifying any requirements that supersede those of this test method.1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6.1 The user of this standard will identify the system of units to be used, and it is critical to ensure that any cross-referenced standards maintain consistency of units between standards.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is a standard procedure for determining the resistance to water penetration under uniform or cyclic static air pressure differences of installed exterior windows, skylights, curtain walls, and doors. The air-pressure differences acting across a building envelope vary greatly. These factors should be considered fully prior to specifying the test pressure difference to be used.NOTE 1: In applying the results of tests by this test method, note that the performance of a wall or its components, or both, may be a function of proper installation and adjustment. In service, the performance will also depend on the rigidity of supporting construction and on the resistance of components to deterioration by various causes, vibration, thermal expansion and contraction, and so forth. It is difficult to simulate the identical complex wetting conditions that can be encountered in service, with large wind-blown water drops, increasing water drop impact pressures with increasing wind velocity, and lateral or upward moving air and water. Some designs are more sensitive than others to this upward moving water.NOTE 2: This test method does not identify unobservable liquid water which may penetrate into the test specimen.5.2 Laboratory tests are designed to give an indication of the performance of an assembly. Field performance may vary from laboratory performance since the supporting structure for the test specimen, methods of mounting, and sealing in the laboratory can only simulate the actual conditions that will exist in the building. Shipping, handling, installation, acts of subsequent trades, aging, and other environmental conditions all may have an adverse effect upon the performance of the installed product. This field test procedure provides a means for determining the performance of a product once installed in the building.5.3 The field test may be made at the time the window, skylight, curtain-wall, or door assemblies are initially installed and before the interior of the building is finished. At this time, it is generally easier to check the interior surfaces of the assemblies for water penetration and to identify the points of penetration. The major advantage of testing when assemblies are initially installed is that errors in fabrication or installation can be readily discovered and corrections made before the entire wall with its component assemblies is completed at which time the expense of corrective work may be increased many times.5.4 The field test may also be made after the building is completed and in service to determine whether or not reported leakage problems are due to the failure of the installed assemblies to resist water penetration at the specified static air pressure difference. Generally it is possible to conduct tests on window, skylight, and door assemblies without too much difficulty, and to identify sources of leakage. A curtain-wall assembly, on the other hand, may not be accessible from the inside without the removal of interior finished walls and ceilings. Even with removal of interior walls and ceilings, it may not be possible to observe curtain-wall surfaces behind spandrel beams. The feasibility of conducting a meaningful static air pressure difference water penetration test on an in-service building must be carefully evaluated before being specified.5.5 Weather conditions can affect the static air pressure difference measurements. If wind gusting causes pressure fluctuation to exceed ±10 % from the specified test pressure, the test should not be conducted.5.6 Generally it is more convenient to use an interior mounted pressure chamber from which air is exhausted to obtain a lower pressure on the interior surface of the specimen. A calibrated rack of nozzles is then used to spray water at the proper rate on the exterior surface. Under circumstances where it is desirable to use an exterior-mounted pressure chamber, the spray rack must be located in the pressure chamber and air supplied to maintain a higher pressure on the exterior surface. Exterior chambers are difficult to attach readily and seal to exterior surfaces.5.7 Even though the equipment requirements are similar, this procedure is not intended to measure air infiltration because of the difficulty of isolating the component air leakage from the extraneous leakage through weep holes, mullion joints, trim, or other surrounding materials.1.1 This test method covers the determination of the resistance of installed exterior windows, curtain walls, skylights, and doors to water penetration when water is applied to the outdoor face and exposed edges simultaneously with a static air pressure at the outdoor face higher than the pressure at the indoor face.1.2 This test method is applicable to any curtain-wall area or to windows, skylights, or doors alone. It is intended primarily for determining the resistance to water penetration through such assemblies for compliance with specified performance criteria, but it may also be used to determine the resistance to penetration through the joints between the assemblies and the adjacent construction. Other procedures may be appropriate to identify sources of leakage.1.3 This test method addresses water penetration through a manufactured assembly. Water that penetrates the assembly, but does not result in a failure as defined herein, may have adverse effects on the performance of contained materials such as sealants and insulating or laminated glass. This test method does not address these issues.1.4 The proper use of this test method requires a knowledge of the principles of pressure measurement.1.5 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 7.1.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D243/D243M-22 Standard Test Method for Residue of Specified Penetration Active 发布日期 :  1970-01-01 实施日期 : 

5.1 This test method is used to determine the percentage of residue having a specified penetration at 100 g/5 s at 25 °C [77 °F]. This test method provides a residue for quality control or for use in other tests as desired.NOTE 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method is used to thermally reduce cutback asphalt, a road oil or a semisolid asphalt, having a penetration greater than 100, to a residue of specified penetration. It is primarily used with slow-curing cutback asphalt as specified in Specification D2026/D2026M.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, into your state may be prohibited by state law.1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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