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4.1 The test method is useful for determining the water-soluble materials in vegetable-tanned leathers.4.2 The water-soluble matter includes the soluble nontanning components of the tanning materials used, sugars and materials of a similar nature, and inorganic compounds such as Epsom salts, Glauber's salts, borax, and other soluble salts added during curing and tannery processing.1.1 This test method covers the determination of the water-soluble materials in all types of vegetable-tanned leathers. This test method does not apply to wet blue.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This test method covers the procedures for determining soluble sulfate ions present in water or a filtrate using a photometer to measure the turbidity of precipitated barium sulfate. This test method also details a method for standardizing the photometer to be used. The soluble sulfate ions may be removed from clays or clay-water slurries by leaching with water during mixing and then filter pressing. An impractical number of washings would be needed to remove all sulfate ions, therefore, this test method should be considered only as a control test and not a quantitative analysis for sulfate ions. Test apparatus include a balance, high speed mixer, filter press, glass beakers, transfer pipets, spectrophotometer, measuring spoon, and other laboratory equipment. All reagents to be used should be of the required purity and concentration.1.1 This test method covers the determination of soluble sulfate ions present in water or a filtrate by means of a photometer measuring the turbidity of precipitated barium sulfate. A method of standardizing the photometer for this test method is also given.1.2 Soluble sulfate ions may be removed from clays or clay-water slurries by leaching with water during mixing and subsequent filter pressing. To remove all the sulfate ions would require an impractical number of washings; therefore, this test method should be considered a control test and not a quantitative analysis for SO4 ions.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Source water protection calls for a rapid and reliable optical method to identify and quantify the oil spill contamination, such as water-soluble fraction of aromatic compounds from the BTEX family (benzene, toluene, ethylbenzene, and xylenes) and naphthalene from the polycyclic aromatic hydrocarbon (PAH) group.5.2 This test method identifies the presence of contamination and quantifies the target contamination component(s) to provide a threshold-based alert signal.5.3 This test method can be used by drinking water treatment plant operators and decision makers as a first line of defense for both initially detecting petroleum product spills, as well as tracking attenuation over time, in source water to prevent contaminant uptake into the processed water and treatment infrastructure.1.1 This test method covers the (1) detection of trace level (µg/L range) of oil and petroleum (water-soluble fraction) pollutants in surface and ground drinking water sources, (2) identification of the compounds, and (3) alerting analysts with a contaminant concentration prediction. This test method facilitates identification and quantification from 20 to 1000 µg/L of target contaminants, including: water-soluble fraction of aromatic compounds from the BTEX family (benzene, toluene, ethylbenzene, and xylenes) and naphthalene from the polycyclic aromatic hydrocarbon (PAH) group, referred to as BTEXN in this test method, in water samples with up to 15 mg/L of dissolved organic carbon (DOC). The main approach involves analyzing and characterizing key water intake locations before the treatment and developing the contaminant library. The water-soluble (BTEXN) contaminants are associated with, but not limited to petroleum oils and fuels including commercial diesel fuel, gasoline, kerosene, heavy oil, fuel oil and lubricate oil, etc.1.2 The data sets are analyzed using multivariate methods to test contaminant identification and quantification. The multivariate methods include classification and regression algorithms to analyze fluorescence EEM data acquired in the laboratory. The common goal of these algorithms is to reduce multidimensionality and eliminate noise of fluorescence and background signals. Automated identification-quantification methods linked directly to the instrument acquisition-analysis software are commercially available.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method provides a reliable means for the determination of the relative amounts of these salts when comparing different lots of the same pigment grade. Water-soluble salts also affect the water resistance and blister resistance of coatings, especially primers for steel. Conductivity measurements, however, cannot be used as the only method to determine and compare the amount of water soluble salts of pigments with the same chemical composition but produced by different manufacturing processes.1.1 This test method covers the determination of the specific resistance of the aqueous leachate from a pigment as an index of water-soluble salt content. This test method is applicable to white pigments and colored pigments (organic and inorganic). The water-soluble salts content is a function of the specific resistance of the solution formed by extracting the pigment with water.1.2 This test method is based on a water to pigment ratio of 9+1. The leachate yield (minimum 160 mL) sufficient for rinsing the cylinder dip cell and thermometer plus the minimum 80 mL required for the measurement to determine the quantity of pigment to be used.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Asphalt is a material used in the construction of roads and as a roofing material and sealant.5.2 This test method provides a means of evaluating exposure to asphalt fume in the working environment at the presently recommended exposure guidelines (for example, Threshold Limit Values and Biological Exposure Indices, ACGIH).75.3 This procedure has been adapted from NIOSH Method 5023 (withdrawn prior to 4th edition (1994) and replaced in 1998 with NIOSH Method 5042) and OSHA Method 58 to reduce the level of background contamination providing better reproducibility.1.1 This test method covers the determination of asphalt fume particulate matter (as benzene soluble fraction) and total particulate matter weight in workplace atmospheres using a polytetrafluoroethylene (PTFE) filter methodology.1.2 This procedure has been adapted from NIOSH Method 5023 (withdrawn prior to 4th edition (1994) and replaced in 1998 with NIOSH Method 5042) and OSHA Method 58. This adaptation was made to reduce the level of background contamination providing better reproducibility.1.3 This procedure is compatible with high flow rate personal sampling equipment–0.5 to 2.0 L/min. It can be used for personal or area monitoring.1.4 The sampling method develops a time-weighted average (TWA) sample and can be used to determine short-term exposure limit (STEL).1.5 The applicable concentration range for the TWA sample is from 0.2 to 2.0 mg/m3.NOTE 1: A study has suggested candidate solvents for benzene replacement.2 A less toxic solvent for this analysis would be more appropriate, although the substitution with a solvent other than benzene needs further validations with field data.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific precautionary statements, see Section 9.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Where sulfates are suspected, subgrade soils should be tested as an integral part of a geotechnical evaluation because the possibility that sulfate induced heave may occur if calcium containing stabilizers are used to improve the soils and sulfate reactions may also cause deterioration in concrete structures. When planning to treat a soil used in construction with lime, testing the soil for water soluble sulfates prior to treatment becomes very important (Note 2).5.2 When sulfate containing cohesive soils are treated with calcium-based stabilizers for foundation improvements, sulfates and free alumina in natural soils react with calcium and free hydroxide to form crystalline minerals, such as ettringite and thaumasite.4 Thaumasite forms when ettringite undergoes changes in the presence of carbonates at low temperatures.5 The sulfate minerals expand considerably when they are hydrated.NOTE 2: For more information on the effect of treating soils containing water soluble sulfates, refer to the following publication: Little, D.N., Stabilization of Pavement Subgrades and Base Course with Lime, Kendal/Hunt Publishing Co., Dubuque, IA, 1995.NOTE 3: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 These methods determine the water soluble sulfate content of cohesive soils used in construction by using the colorimetric technique. Two methods are presented in this standard. Method A is for use in the field and Method B is for use in the laboratory. The colorimetric technique involves measuring the scattering of a light beam through a solution that contains suspended particulate matter. Measurements of sulfate concentrations in construction soils can be used to guide professionals in the selection of appropriate stabilization methods and to assist in assessment of potential deterioration in concrete structures.NOTE 1: These test methods are partially based on the research conducted by Texas A & M University.1.2 The field method, Method A, is used as a screening test for the presence of sulfates and their concentration. The laboratory method, Method B, provides better resolution than the field method.1.3 Ion chromatography is also an acceptable alternative method that can be used to evaluate results, however, it is outside the scope of this standard.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.1.5.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Abrasive media may contain ionic contamination naturally (for example, beach sand), from manufacturing (quenching with contaminated water), transportation, storage or use (in the case of abrasive that is reused). Ionic contamination on the abrasive may transfer to the surface during abrasive blast cleaning, resulting in potential osmotic blistering, accelerated underfilm corrosion and premature coating failure.4.2 This test method describes a shop/field procedure for assessing the level of conductive species on an abrasive.4.3 Abrasive standards published by SSPC (AB) and ISO 11126 provide tolerance levels for water soluble contaminants of the abrasive.1.1 This test method describes a procedure for assessing blast cleaning abrasives for the presence of conductive-potential, ionic contaminants by determining the total concentration of water soluble conductive species using a conductivity test.1.2 This test method does not identify the ionic species present nor provide quantitative results on each species.1.3 This test method is based on a volume comparison among abrasives of similar sizes. A volume comparison is more closely related to surface area of the abrasives than is a weight comparison.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice is suitable for all types of akalali-soluble resins. The resin manufacturer shall specify the percent ammonium hydroxide to be used (based on the equivalent weight of resin) and the maximum temperature to be used to achieve solution.1.1 This practice is a procedure for preparing solutions of alkali-soluble resins in aqueous ammonia and determining the characteristics of such solutions.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Sediment in insulating oil may deposit on transformer parts and interfere with heat transfer and may choke oil ducts; thus hindering oil circulation and heat dissipation. Inorganic sediment usually indicates contamination of some type and organic sediment indicates either deterioration of the oil or contamination.Soluble sludge indicates deterioration of the oil, presence of contaminants, or both. It serves as a warning that formation of sediment may be imminent.The determination of sediment and soluble sludge in a used insulating oil assists in deciding whether the oil may continue to be used in its existing condition or should be replaced, reclaimed, or reconditioned.1.1 This test method covers the determination of sediment and soluble sludge in service-aged insulating oils of petroleum origin. Also, provision is made for determining organic and inorganic content of the sediment. The method is intended primarily for oils of comparatively low viscosity; for example 5.7 to 13.0 cSt (mm2/s) at 40°C (104°F). Suitability for high viscosity oils have not been determined.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is suitable for determining the quantity of hydrogen peroxide, organic hydroperoxides, and organic peroxides as total active oxygen in various hydrocarbon streams for both quality control and quality assurance of the product.1.1 This test method covers the determination of trace peroxides in various hydrocarbon streams. A list of typical hydrocarbon streams can be found in Appendix X2.1.2 This test method is applicable to the determination of peroxides in petroleum liquids including, but not limited to, 1,3-butadiene, styrene, methylcyclohexane, and alpha olefins in the range of 0.1 mg/kg to 100 mg/kg active oxygen. The limit of detection (LOD) is 0.03 mg/kg for active oxygen and the limit of quantitation (LOQ) is 0.11 mg/kg active oxygen. The upper limit has been determined by the calibration range.NOTE 1: LOD and LOQ were calculated using data obtained during development of the method.1.3 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Sources of particulate and water-soluble gaseous fluorides in the atmosphere include the fertilizers, aluminum reduction plants, phosphate processors, steel mills, coal burning operations, brick and tile manufacturers, and various less significant sources (5). Gaseous fluorides can cause adverse effects when ingested or inhaled by animals or humans, or absorbed by plants. The procedures documented in this test method provide a means of determining of particulate and water soluble gaseous fluoride in atmospheres.5.2 This test method provides a means of separation and collection of particulate and water soluble gaseous fluoride and provides samples that are convenient to analyze.1.1 This test method provides a procedure for separation and collection of particulate and water-soluble gaseous fluorides from the atmosphere on a chemically treated filter and in an impinger. The sampling rate may vary from 30  L/min (1.0 ft3/min) to 15 L/min (0.5 ft3/min) for longer sampling periods depending on the atmospheric fluoride concentration. This test method is not intended to be applied to gaseous fluorine compounds that are not water-soluble.1.2 There are several limitations of the test method:1.2.1 Although the acid-treated, medium retentive, prefilter has been shown to allow passage of HF, it restricts passage of particulate matter only as small as about 1 μm. Thus, smaller particulate matter may pass through the filter and be collected in or pass through the impingers.1.2.2 The maximum sample volume to be taken using this test method prior to changing the acid-treated prefilter is recommended as 12 m3. This recommendation is made to minimize any effects due to particulate matter build-up.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 7.4.3.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 It is expected that this practice will be suitable to identify and quantify contaminants found in systems, system materials, and components used in systems requiring a high level of cleanliness, such as components for oxygen service. Nonmetallic piece parts such as seals and valve seats can be tested as received. Warning—If parts being tested are to be subsequently installed in an oxygen-enriched system, residual extraction solvent remaining in the part due to inadequate drying may increase the susceptibility of the system to ignition. The extraction solvent shall be thoroughly removed from the parts prior to service.5.2 Processing materials such as gloves and wipers, or samples thereof, to be used in the cleaning operation can be evaluated prior to use to ensure that the proposed cleaning solvent does not extract contaminants that may be deposited as residues on the surface to be cleaned.NOTE 1: Test methods that do not require Soxhlet equipment, such as Test Methods E1560 and E1731, may be suitable alternatives for evaluation of processing materials. Test Method G144 with Practice G136 may be suitable for use when the material to be tested is not degraded by sonication. However, results from this test method cannot be directly compared to results from other test methods. Soxhlet extraction may be more aggressive than other extraction methods.5.3 Wipers or other cleaning supplies can be tested before and after use to determine the amount of contaminant removed from a surface. The type of contaminant removed from the surface may also be determined by qualitative analysis of the extracted NVR using analytical methods such as Fourier Transform Infrared (FTIR). This procedure can be used to obtain samples for NVR analysis using contaminated control coupons that were subjected to the cleaning process as controls to validate cleaning operations.5.4 The selection of the solvent requires some knowledge of the contaminant (see Practice G93 for recommendations). If a nonvolatile residue (NVR) analysis is to be performed on the molecular contaminant, the boiling point of the solvent shall be significantly lower than that of the contaminant. For other analytical methods, the tester must know the accuracy of the analytical methods, and the solvent shall be chosen so as not to interfere with the selected analytical method. To identify the composition of the NVR, analytical methods such as infrared spectroscopy or gas chromatography/mass spectroscopy have been used satisfactorily.1.1 This practice describes a procedure for the determination of residual contamination in materials to be used within or in contact with hardware requiring a high level of cleanliness, such as components for oxygen service, by Soxhlet extraction.1.2 This practice may be used for extracting nonvolatile and semivolatile residues from solids such as new and used gloves, new and used wipers, contaminated test specimens or control coupons, small piece parts (metallic or nonmetallic), etc. When used with proposed consumable cleaning materials (wipers, gloves, etc.), this practice may be used to determine the potential of the proposed solvent to extract contaminants (plasticizers, residual detergents, brighteners, etc.) from the cleaning material and deposit them on the surface being cleaned.1.3 This practice is not suitable for the evaluation of particulate contamination.1.4 The values stated in SI units are standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D365-23 Standard Guide for Soluble Nitrocellulose Base Solutions Active 发布日期 :  1970-01-01 实施日期 : 

3.1 Since the desired specifications and compositions of soluble nitrocellulose base solutions vary greatly, these methods are used to establish whether limits that shall be as agreed upon between the producer and the user have been met.1.1 This guide covers the testing of soluble nitrocellulose base solutions that are made by dispersing various kinds and concentrations of soluble nitrocellulose (cellulose nitrate) in various solvent mixtures.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 11.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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