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AS 1019-2000 Internal combustion engines - Spark emission control devices 现行 发布日期 :  2000-08-01 实施日期 : 

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5.1 Knowledge of the specified individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons may be determined through the use of this test method.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels and their mixtures containing oxygenate blends (MTBE, ETBE, ethanol, and so forth) with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels.1.2 Based on the cooperative study results, individual component concentrations and precision are determined in the range of 0.01 % mass to approximately 30 % mass. The procedure may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the procedure is used for components with concentrations outside the specified ranges.1.3 The test method also determines methanol, ethanol, t-butanol, methyl t-butyl ether (MTBE), ethyl t-butyl ether (ETBE), t-amyl methyl ether (TAME) in spark ignition engine fuels in the concentration range of 1 % mass to 30 % mass. However, the cooperative study data provided sufficient statistical data for MTBE only.1.4 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this test method is utilized to estimate bulk hydrocarbon group-type composition (PONA) the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of olefinic or naphthenic (for example, virgin naphthas), or both, constituents above n-octane may reflect significant errors in PONA type groupings. Based on the gasoline samples in the interlaboratory cooperative study, this procedure is applicable to samples containing less than 25 % mass of olefins. However, some interfering coelution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Caution should also be exercised when analyzing olefin-free samples using this test method as some of the paraffins may be reported as olefins since analysis is based purely on retention times of the eluting components.1.4.1 Total olefins in the samples may be obtained or confirmed, or both, if necessary, by Test Method D1319 (percent volume) or other test methods, such as those based on multidimensional PONA type of instruments (Test Method D6839).1.5 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744, or equivalent. Other compounds containing oxygen, sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Methods D4815 and D5599 for oxygenates, and D5623 for sulfur compounds, or equivalent.1.6 Annex A1 of this test method compares results of the test procedure with other test methods for selected components, including olefins, and several group types for several interlaboratory cooperative study samples. Although benzene, toluene, and several oxygenates are determined, when doubtful as to the analytical results of these components, confirmatory analyses can be obtained by using specific test methods.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Knowledge of the individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons can be determined through the use of this test method.5.2 This test method is adopted from earlier development and enhancement.4,5,6,7 The chromatographic operating conditions and column tuning process, included in this test method, were developed to provide and enhance the separation and subsequent determination of many individual components not obtained with previous single-column analyses. The column temperature program profile is selected to afford the maximum resolution of possible co-eluting components, especially where these are of two different compound types (for example, a paraffin and a naphthene).5.3 Although a majority of the individual hydrocarbons present in petroleum distillates are determined, some co-elution of compounds is encountered. If this test method is utilized to determine bulk hydrocarbon group-type composition (PONA), the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of olefinic or naphthenic, or both, constituents above octane may reflect significant errors in PONA-type groupings.5.4 If water is or is suspected of being present, its concentration is determined by the use of Test Method D1744. Other compounds containing oxygen, sulfur, nitrogen, and so forth may also be present, and may co-elute with the hydrocarbons. When known co-elution exists, these are noted in the test method data tables. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Method D4815 and D5599 for oxygenates, Test Method D5580 for aromatics, and Test Method D5623 for sulfur compounds.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels and their mixtures containing oxygenate blends (MTBE, ETBE, ethanol, and so forth) with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels.1.2 Based on the cooperative study results, individual component concentrations and precision are determined in the range from 0.01 % to approximately 30 % by mass. The test method may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the test method is used for components with concentrations outside the specified ranges.1.3 This test method also determines methanol, ethanol, t-butanol, methyl t-butyl ether (MTBE), ethyl t-butyl ether (ETBE), and t-amyl methyl ether (TAME) in spark ignition engine fuels in the concentration range from 1 % to 30 % by mass. However, the cooperative study data provided insufficient statistical data for obtaining a precision statement for these compounds.1.4 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this test method is utilized to estimate bulk hydrocarbon group-type composition (PONA), the user of such data should be cautioned that some error will be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of naphthenic (for example, virgin naphthas) constituents above n-octane may reflect significant errors in PONA-type groupings. Based on the gasoline samples in the interlaboratory cooperative study, this test method is applicable to samples containing less than 25 % by mass of olefins. However, some interfering co-elution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Annex A1 of this test method compares results of the test method with other test methods for selected components, including olefins, and several group types for several interlaboratory cooperative study samples. Although benzene, toulene, and several oxygenates are determined, when doubtful as to the analytical results of these components, confirmatory analyses can be obtained by using the specific test methods listed in the reference section.1.4.1 Total olefins in the samples may be obtained or confirmed, or both, if necessary, by Test Method D1319 (percent by volume) or other test methods, such as those based on multidimentional PONA-type of instruments.1.5 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744 or equivalent. Other compounds containing oxygen, sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Methods D4815 and D5599 for oxygenates, and Test Method D5623 for sulfur compounds, or equivalent.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Knowledge of the individual component composition (speciation) of gasoline fuels and blending stocks is useful for refinery quality control and product specification. Process control and product specification compliance for many individual hydrocarbons may be determined through the use of this test method.1.1 This test method covers the determination of individual hydrocarbon components of spark-ignition engine fuels with boiling ranges up to 225 °C. Other light liquid hydrocarbon mixtures typically encountered in petroleum refining operations, such as, blending stocks (naphthas, reformates, alkylates, and so forth) may also be analyzed; however, statistical data was obtained only with blended spark-ignition engine fuels. The tables in Annex A1 enumerate the components reported. Component concentrations are determined in the range from 0.10 % to 15 % by mass. The procedure may be applicable to higher and lower concentrations for the individual components; however, the user must verify the accuracy if the procedures are used for components with concentrations outside the specified ranges.1.2 This test method is applicable also to spark-ignition engine fuel blends containing oxygenated components. However, in this case, the oxygenate content must be determined by Test Methods D5599 or D4815.1.3 Benzene co-elutes with 1-methylcyclopentene. Benzene content must be determined by Test Method D3606 or D5580.1.4 Toluene co-elutes with 2,3,3-trimethylpentane. Toluene content must be determined by Test Method D3606 or D5580.1.5 Although a majority of the individual hydrocarbons present are determined, some co-elution of compounds is encountered. If this procedure is utilized to estimate bulk hydrocarbon group-type composition (PONA) the user of such data should be cautioned that error may be encountered due to co-elution and a lack of identification of all components present. Samples containing significant amounts of naphthenic (for example, virgin naphthas) constituents above n-octane may reflect significant errors in PONA type groupings. Based on the interlaboratory cooperative study, this procedure is applicable to samples having concentrations of olefins less than 20 % by mass. However, significant interfering coelution with the olefins above C7 is possible, particularly if blending components or their higher boiling cuts such as those derived from fluid catalytic cracking (FCC) are analyzed, and the total olefin content may not be accurate. Many of the olefins in spark ignition fuels are at a concentration below 0.10 %; they are not reported by this test method and may bias the total olefin results low.1.5.1 Total olefins in the samples may be obtained or confirmed, or both, by Test Method D1319 (volume %) or other test methods, such as those based on multidimensional PONA type of instruments.1.6 If water is or is suspected of being present, its concentration may be determined, if desired, by the use of Test Method D1744. Other compounds containing sulfur, nitrogen, and so forth, may also be present, and may co-elute with the hydrocarbons. If determination of these specific compounds is required, it is recommended that test methods for these specific materials be used, such as Test Method D5623 for sulfur compounds.1.7 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method was developed to evaluate automotive engine oils for protection against oil thickening and engine wear during moderately high-speed, high-temperature service.5.2 The increase in oil viscosity obtained in this test indicates the tendency of an oil to thicken because of oxidation. In automotive service, such thickening can cause oil pump starvation and resultant catastrophic engine failures.5.3 The deposit ratings for an oil indicate the tendency for the formation of deposits throughout the engine, including those that can cause sticking of the piston rings in their grooves. This can be involved in the loss of compression pressures in the engine.5.4 The camshaft and lifter wear values obtained in this test provide a measure of the anti-wear quality of an oil under conditions of high unit pressure mechanical contact.5.5 The test method was developed to correlate with oils of known good and poor protection against oil thickening and engine wear. Specially formulated oils that produce less than desirable results with unleaded fuels were also used during the development of this test.5.6 The Sequence IIIG engine oil test has replaced the Sequence IIIF test and can be used in specifications and classifications of engine lubricating oils, such as the following:5.6.1 Specification D4485,5.6.2 Military Specification MIL-PRF-2104, and5.6.3 SAE Classification J183.1.1 This test method covers an engine test procedure for evaluating automotive engine oils for certain high-temperature performance characteristics, including oil thickening, varnish deposition, oil consumption, as well as engine wear. Such oils include both single viscosity grade and multiviscosity grade oils that are used in both spark-ignition, gasoline-fueled engines, as well as in diesel engines.1.1.1 Additionally, with nonmandatory supplemental requirements, a IIIGA Test (Mini Rotary Viscometer and Cold Cranking Simulator measurements), a IIIGVS Test (EOT viscosity increase measurement), or a IIIGB Test (phosphorous retention measurement) can be conducted. These supplemental test procedures are contained in Appendix X1, Appendix X2, and Appendix X3, respectively.NOTE 1: Companion test methods used to evaluate engine oil performance for specification requirements are discussed in SAE J304.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exception—Where there is no direct SI equivalent such as screw threads, national pipe threads/diameters, and tubing size.1.3 This test method is arranged as follows:  SectionIntroduction   1Referenced Documents 2Terminology 3Summary of Test Methods 4 5Apparatus 6 Laboratory 6.1 Drawings 6.2 Specified Equipment 6.3 Test Engine 6.4  Engine Parts 6.4.1 Engine Speed and Load Control 6.5 Fluid Conditioning Module 6.6  Engine Cooling System 6.6.1 Flushing Tank 6.7 Coolant Mixing Tank 6.8 Condenser Cooling Systems 6.9 Engine Oil-Cooling System 6.10 Fuel System 6.11 Induction Air Supply Humidity, Temperature, and Pressure 6.12 Temperature Measurement 6.13  Thermocouple Location 6.13.1 Air-to-Fuel Ratio Determination 6.14  Injector Flow Testing 6.14.1 Exhaust and Exhaust Back Pressure Systems 6.15 Blowby Flow Rate Measurement 6.16 Pressure Measurement and Pressure Sensor Location 6.17Reagents and Materials 7 Test Fuel 7.1 Engine and Condenser Coolant 7.2 Coolant Additive 7.3 Coolant Preparation 7.4 Pre-Test Cleaning Materials 7.5 Sealing and Anti-seize Compounds 7.6Test Oil Sample Requirements 8Preparation of Apparatus 9 Condenser Cleaning 9.1 Intake Manifold Cleaning 9.2 Cleaning of Engine Parts (other than the block and heads) 9.3 Connecting Rod Cleaning 9.4 Engine Block Cleaning 9.5 Cylinder Head Cleaning 9.6 Engine Build-up Procedure 9.7  General Information 9.7.1  Special Parts 9.7.2  Hardware Information 9.7.3  Fastener Torque Specifications and Torquing Procedures 9.7.4   Main Bearing Cap Bolts 9.7.4.1   Cylinder Head Bolts 9.7.4.2   Torques for Miscellaneous Bolts, Studs, and Nuts 9.7.4.3 Parts Replacement 9.8 Engine Block Preparation 9.9 Piston Fitting and Numbering 9.10  Piston Ring Fitting 9.10.1 Pre-Test Camshaft and Lifter Measurements 9.11 Camshaft Bearing Installation 9.12 Camshaft Installation 9.13 Main Bearings 9.14  Crankshaft Installation 9.14.1  Main Bearing Cap Installation 9.14.2 Crankshaft Sprocket 9.15 Camshaft Sprocket, and Timing Chain 9.16 Crankshaft End Play 9.17 Piston Pin Installation 9.18  Piston Installation 9.18.1 Harmonic Balancer 9.19 Connecting Rod Bearings 9.20 Engine Front Cover 9.21 Coolant Inlet Adapter 9.22 Oil Dipstick Hole 9.23 Oil Pan 9.24 Cylinder Head Assembly 9.25 Adjustment of Valve Spring Loads 9.26 Cylinder Head Installation 9.27 Hydraulic Valve Lifters 9.28 Pushrods 9.29 Valve Train Loading 9.30 Intake Manifold 9.31 Rocker Covers 9.32 Water Inlet Adapter 9.33 Condenser 9.34 Coolant Outlet Adapter 9.35 External Oil Cooling System 9.36 Oil Sample Valve 9.37 Ignition System 9.38 Throttle Body 9.39 Accessory Drive Units 9.40 Exhaust Manifolds, Water-Cooled 9.41 Engine Flywheel 9.42 Pressure Checking of Engine Coolant System 9.43 Lifting of Assembled Engines 9.44 Mounting the Engine on the Test Stand 9.45 External Cooling System Cleaning 9.46 Engine Coolant Jacket Cleaning (Flushing) 9.47 Coolant Charging 9.48 Test Oil Charging 9.49 Engine Oil Pump Priming 9.50Calibration 10 Laboratory and Engine Test Stand Calibration 10.1 Testing of Reference Oils 10.2 Reference Oil Test Frequency 10.3 Evaluation of Reference Oil Test Results 10.4 Status of Non-Reference Oil Tests Relative to Reference  Oil Test 10.5 Status of Test Stands Used for Non-Standard Tests 10.6 Data Acquisition and Control 10.7  Sample Rate 10.7.1  Measurement Accuracy 10.7.2  Temperature 10.7.3  Pressure 10.7.4  Flow 10.7.5  Speed 10.7.6  Load 10.7.7  Measurement Resolution 10.7.8  System Time Response 10.7.9  Quality Index 10.7.10Engine Operating Procedure 11 Dipstick and Hole Plug 11.1 Dipstick Hole O-ring 11.2 Engine Start-up and Shutdown Procedures 11.3 Start-up 11.4 Scheduled Shutdown 11.5 Non-Scheduled Shutdowns 11.6 Oil Sampling 11.7 Oil Leveling 11.8 Air-to-Fuel-Ratio Measurement and Control 11.9 Air-to-Fuel Ratio Verification 11.10 Blowby Flow Rate Measurement 11.11 NOx Determinations 11.12 Data Recording 11.13 Initial run (10 min) 11.14 Engine Oil Quality Testing (100 h) 11.15 Test Termination 11.16Determination of Test Results 12 Engine Disassembly 12.2 Preparation of Parts for Rating of Sticking, Deposits,  and Plugging 12.3 Piston Deposit Rating 12.4 Post-Test Camshaft and Lifter Wear Measurements 12.5 Viscosity Test 12.6 Testing Oil Samples for Wear Metals 12.7 Blowby Flow Rate Measurements 12.8 Oil Consumption Computation 12.9 Photographs of Test Parts 12.10 Retention of Representative Test Parts 12.11 Severity Adjustments 12.12 Determination of Operational Validity 12.13Report 13 Report Forms 13.1 Precision of Reported Units 13.4Precision and Bias 14Keywords 15ASTM Test Monitoring Center: Organization Annex A1ASTM Test Monitoring Center: Calibration Procedures Annex A2ASTM Test Monitoring Center: Maintenance Activities Annex A3ASTM Test Monitoring Center: Related Information Annex A4Sequence IIIG Test Parts Replacement Guidelines Annex A5Sequence IIIG Determination Volume of Engine Oil in Pan Annex A6Sequence IIIG Test Fuel Analysis Annex A7Sequence IIIG Test Report Forms and Data Dictionary Annex A8Sequence IIIG Test Air-to-Fuel Ratio Control Flow Chart Annex A9Sequence IIIG Test Set Points and Control States Annex A10Sequence IIIG Quality Index Upper and Lower Values Annex A11Sequence IIIG Engine Oil Level Worksheet Annex A12Blowby Flow Rate Determination Annex A13Safety Hazards Annex A14Sequence IIIG Blueprint Listing Annex A15Fluid Condition Module Components Annex A16Engine Build Worksheets Annex A17Engine Oil Cooling System Schematic Annex A18Guidelines For Hardware Subject To First-In/First-Out Criteria Annex A19Sequence IIIGA Test Procedure Appendix X1Sequence IIIGVIS Test Procedure Appendix X2Sequence IIIGB Test Procedure Appendix X31.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are provided in 6.14.1.1 and 7.1.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers requirements for fuel grade methyl tertiary-butyl ether utilized in commerce, terminal blending, or downstream blending with fuels for spark-ignition engines. The following test methods shall be conducted to meet the specified requirements: appearance; sulfur; solvent-washed gum content; MTBE mass percentage; methanol mass percentage; API gravity; density; copper strip corrosion; water content; vapor pressure; and color.1.1 This specification covers requirements for fuel grade methyl tertiary-butyl ether utilized in blending with gasolines at 1 % to 15 % by volume (equivalent to 2.7 % by weight oxygen) for use as automotive spark-ignition engine fuel covered by Specification D4814 as well as other automotive fuel applications involving MTBE. Other MTBE grades may be available for blending that are not covered by this specification.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method was developed to evaluate automotive engine oils for protection against oil thickening and piston deposits during moderately high-speed, hightemperature service.5.1.1 The increase in kinematic viscosity of the oil indicates the tendency of an oil to thicken because of oxidation. In automotive service, such thickening can cause oil pump starvation and resultant catastrophic engine failures.5.1.2 The deposit ratings for an oil indicate the tendency for the formation of deposits throughout the engine, including those that can cause sticking of the piston rings in their grooves. In automotive service, such ring sticking can cause a loss of compression pressures in the engine.5.2 The test method was developed to correlate with oils of known good and poor protection against oil thickening and piston deposits. Specially formulated oils that produce less than desirable results with unleaded fuels were also used during the development of this test.5.3 The Sequence IIIH engine oil test has been recommended as a replacement for the Sequence IIIG test and is expected to be used in specifications and classifications of engine lubricating oils, such as the following:5.3.1 Specification D4485.5.3.2 Military Specification MIL-PRF-2104.5.3.3 SAE Classification J183.1.1 This test method covers an engine test procedure for evaluating automotive engine oils for certain high-temperature performance characteristics, including oil thickening (as measured by kinematic viscosity increase), piston deposits, ring sticking, oil consumption, and phosphorus retention. Such oils include both single-viscosity and multiviscosity grade oils that are used in both spark-ignition, gasoline-fueled engines, as well as in diesel engines.1.1.1 Additionally, with nonmandatory supplemental requirements, a Sequence IIIHA Test (Mini Rotary Viscometer and Cold Cranking Simulator measurements), or a Sequence IIIHB Test (phosphorus retention measurement) can be conducted. These supplemental test procedures are contained in Appendix X1 and Appendix X2, respectively.NOTE 1: Companion test methods used to evaluate engine oil performance for specification requirements are discussed in SAE J304.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exceptions: 1.2.1.1 Where there is no direct SI equivalent such as screw threads, national pipe threads/diameters, tubing sizes, and valve sizes and springs.1.2.1.2 The ring end gaps in Table A8.7, the dimensions for the blowby ventilation support bracket in Fig. A3.2, and the torque wrenches in Table A8.1 are in inch-pound units.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are provided in 6.11.6, 7.1, 7.2.1, and 7.3.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The practice for taking a sample of molten metal during production and producing a chill cast disk, used in conjunction with the following appropriate quantitative spark atomic emission spectrochemical methods, Test Methods E607 and E1251, is suitable for use in manufacturing control or certifying, or both, that the entire lot of alloy sampled meets established composition limits.5.2 The practice for melting a piece of a product to produce a chill cast disk analyzed in conjunction with the following appropriate quantitative spark atomic emission spectrochemical methods, Test Methods E607 and E1251, is suitable, if a representative sample is taken, for determining if the piece sampled meets Aluminum Association composition limits.5.3 The practice for direct analysis of product is suitable for determining an approximate composition of the piece analyzed.1.1 These practices describe procedures for producing a chill cast disk sample from molten aluminum during the production process, and from molten metal produced by melting pieces cut from products.1.2 These practices describe a procedure for obtaining qualitative results by direct analysis of product using spark atomic emission spectrometry.1.3 These practices describe procedures for preparation of samples and products prior to analysis.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 6.1 and 7.2.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Test Method—The data obtained from the use of this test method provide a comparative index of the fuel-saving capabilities of automotive engine oils under repeatable laboratory conditions. A BL has been established for this test to provide a standard against which all other oils can be compared. The BL oil is an SAE 20W-30 grade fully formulated lubricant. The test procedure was not designed to give a precise estimate of the difference between two test oils without adequate replication. The test method was developed to compare the test oil to the BL oil. Companion test methods used to evaluate engine oil performance for specification requirements are discussed in the latest revision of Specification D4485.5.2 Use—The Sequence VIE test method is useful for engine oil fuel economy specification acceptance. It is used in specifications and classifications of engine lubricating oils, such as the following:5.2.1 Specification D4485.5.2.2 API 1509.5.2.3 SAE Classification J304.5.2.4 SAE Classification J1423.1.1 This test method covers an engine test procedure for the measurement of the effects of automotive engine oils on the fuel economy of passenger cars and light-duty trucks with gross vehicle weight 3856 kg or less. The tests are conducted using a specified spark-ignition engine with a displacement of 3.6 L (General Motors)4 on a dynamometer test stand. It applies to multi-viscosity oils used in these applications.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exceptions—Where there is no direct equivalent such as the units for screw threads, National Pipe threads/diameters, tubing size, and single source supply equipment specifications. Additionally, Brake Specific Fuel Consumption (BSFC) is measured in kilogram per kilowatt hour.1.3 This test method is arranged as follows:Subject SectionIntroduction   1Referenced Documents 2Terminology 3Summary of Test Method 4 5Apparatus 6General 6.1Test Engine Configuration 6.2Laboratory Ambient Conditions 6.3Engine Speed and Torque Control 6.4Dynamometer 6.4.1Dynamometer Torque 6.4.2Engine Cooling System 6.5External Oil System 6.6Fuel System 6.7Fuel Flow Measurement 6.7.2Fuel Temperature and Pressure Control to the Fuel Flow Meter 6.7.3Fuel Temperature and Pressure Control to Engine Fuel Rail 6.7.4Fuel Supply Pumps 6.7.5Fuel Filtering 6.7.6Engine Intake Air Supply 6.8Intake Air Humidity 6.8.1Intake Air Filtration 6.8.2Intake Air Pressure Relief 6.8.3Temperature Measurement 6.9Thermocouple Location 6.9.5AFR Determination 6.10Exhaust and Exhaust Back Pressure Systems 6.11Exhaust Manifolds 6.11.1Laboratory Exhaust System 6.11.2Exhaust Back Pressure 6.11.3Pressure Measurement and Pressure Sensor Locations 6.12Engine Oil 6.12.2Fuel to Fuel Flow Meter 6.12.3Fuel to Engine Fuel Rail 6.12.4Exhaust Back Pressure 6.12.5Intake Air 6.12.6Intake Manifold Vacuum/Absolute Pressure 6.12.7Coolant Flow Differential Pressure 6.12.8Crankcase Pressure 6.12.9Engine Hardware and Related Apparatus 6.13Test Engine Configuration 6.13.1ECU (Power Control Module) 6.13.2Thermostat Block-Off Adapter Plate 6.13.3Wiring Harness 6.13.4Thermostat Block-Off Plate 6.13.5Oil Filter Adapter Plate 6.13.6Modified Throttle Body Assembly 6.13.7Fuel Rail 6.13.8Miscellaneous Apparatus Related to Engine Operation 6.14Reagents and Materials 7Engine Oil 7.1Test Fuel 7.2Engine Coolant 7.3Cleaning Materials 7.4Preparation of Apparatus 8Test Stand Preparation 8.2Engine Preparation 9Cleaning of Engine Parts 9.2Engine Assembly Procedure 9.3General Assembly Instructions 9.3.1Bolt Torque Specifications 9.3.2Sealing Compounds 9.3.3Harmonic Balancer 9.3.5Thermostat 9.3.6Coolant Inlet 9.3.7Oil Filter Adapter 9.3.8Dipstick Tube 9.3.9Sensors, Switches, Valves, and Positioners 9.3.10Ignition System 9.3.11Fuel Injection System 9.3.12Intake Air System 9.3.13Engine Management System 9.3.14Accessory Drive Units 9.3.15Exhaust Manifolds 9.3.16Engine Flywheel and Guards 9.3.17Lifting of Assembled Engines 9.3.18Engine Mounts 9.3.19Non-Phased Camshaft Gears 9.3.20Internal Coolant Orifice 9.3.21Calibration 10Stand/Engine Calibration 10.1Procedure 10.1.1Reporting of Reference Results 10.1.2Analysis of Reference/Calibration Oils 10.1.3Instrument Calibration 10.2Engine Torque Measurement System 10.2.3Fuel Flow Measurement System 10.2.4Coolant Flow Measurement System 10.2.5Thermocouple and Temperature Measurement System 10.2.6Humidity Measurement System 10.2.7Other Instrumentation 10.2.8Test Procedure 11External Oil System 11.1Flush Effectiveness Demonstration 11.2Preparation for Oil Charge 11.3Initial Engine Start-Up 11.4New Engine Break-In 11.5Oil Charge for Break-In 11.5.2Break-In Operating Conditions 11.5.3Standard Requirements for Break-In 11.5.4Routine Test Operation 11.6Start-Up and Shutdown Procedures 11.6.1Flying Flush Oil Exchange Procedures 11.6.2Test Operating Stages 11.6.3Stabilization to Stage Conditions 11.6.4Stabilized BSFC Measurement Cycle 11.6.5BLB1 Oil Flush Procedure for BL Oil Before Test Run 1 11.6.6BSFC Measurement of BLB1 Oil Before Test Oil Run 2 11.6.7BLB2 Oil Flush Procedure for BL Oil Before Test Oil 11.6.8BSFC Measurement of BLB2 Oil Before Test Oil 11.6.9Percent Delta Calculation for BLB1 vs. BLB2 11.6.10Test Oil Flush Procedure 11.6.11Test Oil Aging, Phase I 11.6.12BSFC Measurement of Aged (Phase I) Test Oil 11.6.13Test Oil Aging, Phase II 11.6.14BSFC Measurement of Aged (Phase II) Test Oil 11.6.15Oil Consumption and Sampling 11.6.16Flush Procedure for BL Oil (BLA) After Test Oil 11.6.17General Test Data Logging Forms 11.6.18Diagnostic Review Procedures 11.6.19Determination of Test Results 12Final Test Report 13Precision and Bias 14Keywords 15Annexes  ASTM Test Monitoring Center Organization Annex A1ASTM Test Monitoring Center: Calibration Procedures Annex A2ASTM Test Monitoring Center: Maintenance Activities Annex A3ASTM Test Monitoring Center: Related Information Annex A4Detailed Specifications and Drawings of Apparatus Annex A5Oil Heater Bolton 255 Refill Procedure Annex A6Engine Part Number Listing Annex A7Safety Precautions Annex A8Sequence VIE Test Report Forms and Data Dictionary Annex A9Statistical Equations for Mean and Standard Deviations Annex A10Determining the Oil Sump Full Level and Consumption Annex A11Fuel Injection Evaluation Annex A12Pre-test Maintenance Checklist Annex A13Blow-by Ventilation System Requirements Annex A14Calculation of Test Results Annex A15Calculation of Un-weighted Baseline Shift Annex A16Non-Phased Cam Gear and Position Actuator Installation and GM Short Block Assembly Procedure Annex A17Procedure  Procurement of Test Materials Annex A18Alternate Fuel Approval Requirements Annex A19Appendix  Useful Information Appendix X11.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The chemical composition of cast iron alloys shall be determined accurately in order to ensure the desired metallurgical properties. This procedure is suitable for manufacturing control and inspection testing.1.1 This test method covers the analysis of cast iron by spark atomic emission spectrometry for the following elements in the ranges shown (Note 1):    Ranges, %  Elements Applicable Range, % Quantitative Range, %A         Carbon 1.9 to 3.8 1.90  to 3.8  Chromium 0 to 2.0 0.025 to 2.0  Copper 0 to 0.75 0.015 to 0.75  Manganese 0 to 1.8 0.03  to 1.8  Molybdenum 0 to 1.2 0.01  to 1.2  Nickel 0 to 2.0 0.02  to 2.0  Phosphorus 0 to 0.4 0.005 to 0.4  Silicon 0 to 2.5 0.15  to 2.5  Sulfur 0 to 0.08 0.01  to 0.08  Tin 0 to 0.14 0.004 to 0.14  Titanium 0 to 0.12 0.003 to 0.12  Vanadium 0 to 0.22 0.008 to 0.22NOTE 1: The ranges of the elements listed have been established through cooperative testing of reference materials. These ranges can be extended by the use of suitable reference materials.1.2 This test method covers analysis of specimens having a diameter adequate to overlap the bore of the spark stand opening (to effect an argon seal). The specimen thickness should be sufficient to prevent overheating during excitation. A heat sink backing may be used. The maximum thickness is limited only by the height that the stand will permit.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Some process catalysts used in petroleum and chemical refining can be poisoned when trace amounts of sulfur bearing materials are contained in the feedstocks. This test method can be used to determine sulfur in process feeds sulfur in finished products, and can also be used for purposes of regulatory control.1.1 This test method covers the determination of total sulfur in liquid hydrocarbons, boiling in the range from approximately 25 °C to 400 °C, with viscosities between approximately 0.2 cSt and 20 cSt (mm2/s) at room temperature.1.2 Three separate interlaboratory studies (ILS) on precision, and three other investigations that resulted in an ASTM research report, have determined that this test method is applicable to naphthas, distillates, engine oil, ethanol, Fatty Acid Methyl Ester (FAME), and engine fuel such as gasoline, oxygen enriched gasoline (ethanol blends, E-85, M-85, RFG), diesel, biodiesel, diesel/biodiesel blends, and jet fuel. Samples containing 1.0 mg/kg to 8000 mg/kg total sulfur can be analyzed (Note 1).NOTE 1: Estimates of the pooled limit of quantification (PLOQ) for the precision studies were calculated. Values ranged between less than 1.0 mg/kg and less than 5.0 mg/kg (see Section 9 and 16.1).1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For warning statements, see 3.1, 7.3, 7.4, Section 8, and 9.1.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers butanol intended to be blended with gasoline at 1 to 12.5 volume % for use as an automotive spark-ignition engine fuel. It addresses performance requirements, workmanship, sampling, containers, sample handling, and test methods.1.1 This specification covers butanol intended to be blended with gasoline at 1 % to 12.5 % by volume for use as an automotive spark-ignition engine fuel.1.1.1 Butanol contains 22 % by mass oxygen. The mass percent of oxygen of a butanol blend with gasoline depends on the volume percent of butanol blended, the density of the butanol isomer, and the density of the base blendstock.1.1.2 The maximum limit on blending is not a performance limit but a current regulatory limit in the United States.1.2 This specification covers three butanol isomers: 1-butanol, 2-butanol, and 2-methyl-1-propanol. This specification specifically excludes 2-methyl-2-propanol (that is, tert-butyl alcohol).1.2.1 Tert-butyl alcohol has different physical properties (melting point, water miscibility) than the other three isomers.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Test Method—The data obtained from the use of this test method provide a comparative index of the fuel-saving capabilities of automotive engine oils under repeatable laboratory conditions. A BL has been established for this test to provide a standard against which all other oils can be compared. The BL oil is an SAE 20W-30 grade fully formulated lubricant. The test procedure was not designed to give a precise estimate of the difference between two test oils without adequate replication. The test method was developed to compare the test oil to the BL oil. Companion test methods used to evaluate engine oil performance for specification requirements are discussed in the latest revision of Specification D4485.5.2 Use—The Sequence VID test method is useful for engine oil fuel economy specification acceptance. It is used in specifications and classifications of engine lubricating oils, such as the following:5.2.1 Specification D4485.5.2.2 API 1509.5.2.3 SAE Classification J304.5.2.4 SAE Classification J1423.1.1 This test method covers an engine test procedure for the measurement of the effects of automotive engine oils on the fuel economy of passenger cars and light-duty trucks with gross vehicle weight 3856 kg or less. The tests are conducted using a specified spark-ignition engine with a displacement of 3.6 L (General Motors)4 on a dynamometer test stand. It applies to multi viscosity grade oils used in these applications.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Exceptions—Where there is no direct equivalent such as the units for screw threads, National Pipe threads/diameters, tubing size, and single source supply equipment specifications. Additionally, Brake Fuel Consumption (BSFC) is measured in kilograms per kilowatthour.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This test method is arranged as follows:Subject SectionIntroduction   1Referenced Documents 2Terminology 3Summary of Test Method 4 5Apparatus 6General 6.1Test Engine Configuration 6.2Laboratory Ambient Conditions 6.3Engine Speed and Torque Control 6.4Dynamometer 6.4.1Dynamometer Torque 6.4.2Engine Cooling System 6.5External Oil System 6.6Fuel System 6.7Fuel Flow Measurement 6.7.2Fuel Temperature and Pressure Control to the Fuel Flowmeter 6.7.3Fuel Temperature and Pressure Control to Engine Fuel Rail 6.7.4Fuel Supply Pumps 6.7.5Fuel Filtering 6.7.6Engine Intake Air Supply 6.8Intake Air Humidity 6.8.1Intake Air Filtration 6.8.2Intake Air Pressure Relief 6.8.3Temperature Measurement 6.9Thermocouple Location 6.9.5AFR Determination 6.10Exhaust and Exhaust Back Pressure Systems 6.11Exhaust Manifolds 6.11.1Laboratory Exhaust System 6.11.2Exhaust Back Pressure 6.11.3Pressure Measurement and Pressure Sensor Locations 6.12Engine Oil 6.12.2Fuel to Fuel Flowmeter 6.12.3Fuel to Engine Fuel Rail 6.12.4Exhaust Back Pressure 6.12.5Intake Air 6.12.6Intake Manifold Vacuum/Absolute Pressure 6.12.7Coolant Flow Differential Pressure 6.12.8Crankcase Pressure 6.12.9Engine Hardware and Related Apparatus 6.13Test Engine Configuration 6.13.1ECU (Power Control Module) 6.13.2Thermostat Block-Off Adapter Plate 6.13.3Wiring Harness 6.13.4Oil Pan 6.13.5Engine Water Pump Adapter Plate 6.13.6Thermostat Block-Off Plate 6.13.7Oil Filter Adapter Plate 6.13.8Modified Throttle Body Assembly 6.13.9Fuel Rail 6.13.10Miscellaneous Apparatus Related to Engine Operation 6.14Reagents and Materials 7Engine Oil 7.1Test Fuel 7.2Engine Coolant 7.3Cleaning Materials 7.4Preparation of Apparatus 8Test Stand Preparation 8.2Engine Preparation 9Cleaning of Engine Parts 9.3Engine Assembly Procedure 9.4General Assembly Instructions 9.4.1Bolt Torque Specifications 9.4.2Sealing Compounds 9.4.3Harmonic Balancer 9.4.5Thermostat 9.4.6Coolant Inlet 9.4.7Oil Filter Adapter 9.4.8Dipstick Tube 9.4.9Sensors, Switches, Valves, and Positioners 9.4.10Ignition System 9.4.11Fuel Injection System 9.4.12Intake Air System 9.4.13Engine Management System 9.4.14Accessory Drive Units 9.4.15Exhaust Manifolds 9.4.16Engine Flywheel and Guards 9.4.17Lifting of Assembled Engines 9.4.18Engine Mounts 9.4.19Non-Phased Camshaft Gears 9.4.20Internal Coolant Orifice 9.4.21Calibration 10Stand/Engine Calibration 10.1Procedure 10.1.1Reporting of Reference Results 10.1.2Instrument Calibration 10.2Engine Torque Measurement System 10.2.3Fuel Flow Measurement System 10.2.4Coolant Flow Measurement System 10.2.5Thermocouple and Temperature Measurement System 10.2.6Humidity Measurement System 10.2.7Other Instrumentation 10.2.8Test Procedure 11External Oil System 11.1Flush Effectiveness Demonstration 11.2Preparation for Oil Charge 11.3Initial Engine Start-Up 11.4New Engine Break-In 11.5Oil Charge for Break-In 11.5.2Break-In Operating Conditions 11.5.3Standard Requirements for Break-In 11.5.4Routine Test Operation 11.6Start-Up and Shutdown Procedures 11.6.1Flying Flush Oil Exchange Procedures 11.6.2Test Operating Stages 11.6.3Stabilization to Stage Conditions 11.6.4Stabilized BSFC Measurement Cycle 11.6.5BLB1 Oil Flush Procedure for BL Oil Before Test Run 1 11.6.6BSFC Measurement of BLB1 Oil Before Test Oil 11.6.7BLB2 Oil Flush Procedure for BL Oil Before Test Oil Run 2 11.6.8BSFC Measurement of BLB2 Oil Before Test Oil 11.6.9Percent Delta Calculation for BLB1 vs. BLB2 11.6.10Test Oil Flush Procedure 11.6.11Test Oil Aging, Phase I 11.6.12BSFC Measurement of Aged (Phase I) Test Oil 11.6.13Test Oil Aging, Phase II 11.6.14BSFC Measurement of Aged (Phase II) Test Oil 11.6.15Oil Consumption and Sampling 11.6.16Flush Procedure for BL Oil (BLA) After Test Oil 11.6.17General Test Data Logging Forms 11.6.18Diagnostic Review Procedures 11.6.19Determination of Test Results 12Report 13Precision and Bias 14Keywords 15Annexes  ASTM Test Monitoring Center: Organization Annex A1ASTM Test Monitoring Center: Calibration Procedures Annex A2ASTM Test Monitoring Center: Maintenance Activities Annex A3ASTM Test Monitoring Center: Related Information Annex A4Detailed Specifications and Drawings of Apparatus Annex A5Oil Heater Cerrobase Refill Procedure Annex A6Engine Part Number Listing Annex A7Safety Precautions Annex A8Report Format Annex A9Statistical Equations for Mean and Standard Deviations Annex A10Oil Sump Full Level Determination Consumption Measurement Calibration Procedure Annex A11Fuel Injector Evaluation Annex A12Pre-test Maintenance Checklist Annex A13Blow-by Ventilation System Requirements Annex A14Calculation of Test Results Annex A15Calculation of Unweighted Baseline Shift Annex A16Non–Phased Cam Gear and Position Actuator Installation Procedure Annex A17   Appendix  Procurement of Test Materials Appendix X11.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method for the spectrometric analysis of metals and alloys is primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use this test method will be analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.1.1 This test method covers the simultaneous determination of 21 alloying and residual elements in carbon and low-alloy steels by spark atomic emission vacuum spectrometry in the mass fraction ranges shown Note 1.Element Composition Range, %Applicable Range,Mass Fraction %A Quantitative Range,Mass Fraction %BAluminum 0 to 0.093 0.006 to 0.093Antimony 0 to 0.027 0.006 to 0.027Arsenic 0 to 0.1 0.003 to 0.1Boron 0 to 0.007 0.0004 to 0.007Calcium 0 to 0.003 0.002 to 0.003Carbon 0 to 1.1 0.02 to 1.1Chromium 0 to 8.2 0.007 to 8.14Cobalt 0 to 0.20 0.006 to 0.20Copper 0 to 0.5 0.006 to 0.5LeadC 0 to 0.2 0.002 to 0.2Manganese 0 to 2.0 0.03 to 2.0Molybdenum 0 to 1.3 0.007 to 1.3Nickel 0 to 5.0 0.006 to 5.0Niobium 0 to 0.12 0.003 to 0.12Nitrogen 0 to 0.015 0.01 to 0.055Phosphorous 0 to 0.085 0.006 to 0.085Silicon 0 to 1.54 0.02 to 1.54Sulfur 0 to 0.055 0.001 to 0.055Tin 0 to 0.061 0.005 to 0.061Titanium 0 to 0.2 0.001 to 0.2Vanadium 0 to 0.3 0.003 to 0.3Zirconium 0 to 0.05 0.01 to 0.05NOTE 1: The mass fraction ranges of the elements listed have been established through cooperative testing2 of reference materials.1.2 This test method covers analysis of specimens having a diameter adequate to overlap and seal the bore of the spark stand opening. The specimen thickness can vary significantly according to the design of the spectrometer stand, but a thickness between 10 mm and 38 mm has been found to be most practical.1.3 This test method covers the routine control analysis in iron and steelmaking operations and the analysis of processed material. It is designed for chill-cast, rolled, and forged specimens. Better performance is expected when reference materials and specimens are of similar metallurgical condition and composition. However, it is not required for all applications of this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The delta octane number (ΔO.N.) measure can quantify the difference of in-line blended spark-ignition engine fuel or process stream material octane number to a desired octane number to aid in optimizing control of blender facilities or refinery process units.5.2 The ΔO.N. measure, summed with a comparison reference fuels O.N. provides either research or motor octane number value of the current in-line blended spark-ignition engine fuel or process stream material.5.3 Through the use of cumulative flow-proportioned averaging of the repetitive ΔO.N. results, in accordance with Practice D6624, an average octane number can be assigned to a tender or batch of in-line blended spark-ignition engine fuel.1.1 This test method covers the quantitative online determination by direct comparison of the difference in knock rating or delta octane number of a stream sample of spark-ignition engine fuel from that of a comparison reference fuel.1.2 This test method covers the methodology for obtaining an octane number using the measured delta octane number and the octane number of the comparison reference fuel.1.3 The comparison reference fuel is required to be of essentially the same composition as the stream sample to be analyzed and can be a secondary fuel termed standard fuel or a tertiary fuel termed prototype fuel.1.4 The test method utilizes a knock testing unit/automated analyzer system that incorporates computer control of a standardized single-cylinder, four-stroke cycle, variable compression ratio, carbureted, CFR engine with appropriate auxiliary equipment using either Test Method D2699 Research method or Test Method D2700 Motor method operating conditions.1.4.1 Knock measurements are based on operation of both fuels at the fuel-air ratio that produces maximum knock intensity for that fuel.1.4.2 Measured differences in knock intensity are scaled to provide a positive or negative delta octane number of the stream sample from the comparison reference fuel when the fuels are compared at the same compression ratio.1.4.3 Measured differences in compression ratio are scaled from the appropriate guide table to provide a positive or negative delta octane number of the stream sample from the comparison reference fuel when the fuels are compared at the same knock intensity.1.5 This test method is limited to testing 78 to 102 octane number spark-ignition engine fuels using either research or motor method conditions.1.6 The octane number difference between the stream sample and the applicable comparison reference fuel is self-limiting by specifications imposed upon the standard and prototype fuels.1.7 Specifications for selection, preparation, storage, and dispensing of standard and prototype fuels are provided. Detailed procedures for determination of an appropriate assigned octane number for both standard and prototype fuels are also incorporated.1.8 The values of operating conditions are stated in SI units and are considered standard. The values in parentheses are historical inch-pound units. The standardized CFR engine measurements continue to be expressed in inch-pound units only because of the extensive and expensive tooling that has been created for this equipment.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific warning statements, see Section 8 and Annex A1.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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