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3.1 This classification establishes a series of definite viscosity levels so that lubricant suppliers, lubricant users, and equipment designers will have a uniform and common basis for designating, specifying, or selecting the viscosity of industrial fluid lubricants.3.2 This classification is used to eliminate unjustified intermediate viscosities, thereby reducing the total number of viscosity grades used in the lubrication of industrial equipment.3.3 This system provides a suitable number of viscosity grades, a uniform reference temperature, a uniform viscosity tolerance, and a nomenclature system for identifying the viscosity characteristics of each grade.3.4 This system implies no evaluation of lubricant quality and applies to no property of a fluid other than its viscosity at the reference temperature. It does not apply to those lubricants used primarily with automotive equipment and identified with an SAE number.AbstractThis classification is applicable to all petroleum-base fluid lubricants and to those nonpetroleum materials which may be readily blended to produce fluid lubricants of a desired viscosity, that is, lubricants for bearings, gears, compressor cylinders, hydraulic fluids, etc. This classification is used to eliminate unjustified intermediate viscosities, thereby reducing the total number of viscosity grades used in the lubrication of industrial equipment. The lubricants shall be classified according to viscosity grades: ISO VG 2; ISO VG 3; ISO VG 5; ISO VG 7; ISO VG 10; ISO VG 15; ISO VG 22; ISO VG 32; ISO VG 46; ISO VG 68; ISO VG 100; ISO VG 150; ISO VG 220; ISO VG 320; ISO VG 460; ISO VG 680; ISO VG 1000; ISO VG 1500; ISO VG 2200; and ISO VG 3200.1.1 This classification is applicable to all petroleum-base fluid lubricants and to those nonpetroleum materials which may be readily blended to produce fluid lubricants of a desired viscosity, that is, lubricants for bearings, gears, compressor cylinders, hydraulic fluids, etc.1.2 This classification is applicable to fluids ranging in kinematic viscosity from 2 cSt to 3200 cSt (mm2/s) as measured at a reference temperature of 40 °C. In the category of petroleum-base fluids, this covers the range from kerosene to heavy cylinder oils.1.3 Fluids of either lesser or greater viscosity than the range described in 1.2 are, at present, seldom used as industrial lubricants. Should industrial practices change, then this system, based on a mathematical series of numbers, may be extended to retain its orderly progression.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is well suited for measuring the viscosity of glasses in ranges higher than those covered by parallel plate (see Test Method C1351M) and rotational viscometry (see Practice C965) methods. This test method is useful for providing information related to the behavior of glass after it has been formed into an object of commerce and in research and development.1.1 This test method covers the determination of glass viscosity from approximately 108 Pa·s to approximately 1013 Pa·s by measuring the rate of viscous bending of a simply loaded glass beam.2 Due to the thermal history of the glass, the viscosity may not represent conditions of thermal equilibrium at the high end of the measured viscosity range. Measurements carried out over extended periods of time at any temperature or thermal preconditioning will minimize these effects by allowing the glass to approach equilibrium structural conditions. Conversely, the method also may be used in experimental programs that focus on nonequilibrium conditions.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is well suited for measuring the viscosity of glasses between the range within which rotational viscometry (see Practice C965) is useful and the range within which beam bending viscometry is useful (see Test Method C1350M). It can be used to determine the viscosity/temperature curve in the region near the softening point (see Test Method C338). This test method is useful for providing information related to the behavior of glass as it is formed into an object of commerce, and in research and development.1.1 This test method covers the determination of the viscosity of glass from 104 Pa·s to 108 Pa·s by measuring the rate of viscous compression of a small, solid cylinder.21.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1200-23 Standard Test Method for Viscosity by Ford Viscosity Cup Active 发布日期 :  1970-01-01 实施日期 : 

5.1 This test method is useful for the determination of package and application viscosities of a number of paints and other coatings and in the thinning of these materials, but is limited to Newtonian or near-Newtonian liquids.5.2 There are other types of apparatus for measuring viscosity in the laboratory that produce more accurate results.1.1 This test method covers the determination of the viscosity of Newtonian or near-Newtonian paints, varnishes, lacquers, and related liquid materials with the Ford-type efflux viscosity cup. If the material is non-Newtonian, that is, shear-thinning or thixotropic, Test Method D2196 should be used.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Many petroleum products and some non-petroleum products are used as lubricants in the equipment, and the correct operation of the equipment depends upon the appropriate viscosity of the lubricant being used. Additionally, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.5.2 The viscosity of used oils is a commonly determined parameter in the oil industry to assess the effect of engine wear on the lube oils used, as well as the degradation of the engine parts during operation.5.3 The Houillon viscometer tube method offers automated determination of kinematic viscosity. Typically a sample volume of less than 1 mL is required for the analysis.1.1 This test method covers the measurement of the kinematic viscosity of transparent and opaque liquids; such as base oils, formulated oils, diesel oil, biodiesel, biodiesel blends, residual fuel oils, marine fuels, and used lubricating oils using a Houillon viscometer in automated mode.1.2 The range of kinematic viscosity capable of being measured by this test method is from 2 mm2/s to 2500 mm2/s (see Fig. 1). The range is dependent on the tube constant utilized. The temperature range that the apparatus is capable of achieving is between 20 °C and 150 °C, inclusive. However, the precision has only been determined for the viscosity range; 2 mm2/s to 478 mm2/s at 40 °C for base oils, formulated oils, diesel oil, biodiesel, and biodiesel blends; 3 mm2/s to 106 mm2/s at 100 °C for base oils and formulated oils; 25 mm2/s to 150 mm2/s at 40 °C and 5 mm2/s to 16 mm2/s at 100 °C for used lubricating oils; 25 mm2/s to 2500 mm2/s at 50 °C and 6 mm2/s to 110 mm2/s at 100 °C for residual fuels. As indicated for the materials listed in the precision section.FIG. 1 Houillon Viscometer Typical Viscosity Range of Tube ConstantsNOTE 1: Viscosity range of a Houillon tube is based on most practical flow time of 30 s to 200 s.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.5.2 Density is a fundamental physical property that can be used in conjunction with other properties to characterize both the light and heavy fractions of petroleum and petroleum products.5.3 Determination of the density or relative density of petroleum and its products is necessary for the conversion of measured volumes to volumes at the standard temperature of 15 °C.1.1 This test method covers and specifies a procedure for the concurrent measurement of both the dynamic viscosity, η, and the density, ρ, of liquid petroleum products and crude oils, both transparent and opaque. The kinematic viscosity, ν, can be obtained by dividing the dynamic viscosity, η, by the density, ρ, obtained at the same test temperature.1.2 The result obtained from this test method is dependent upon the behavior of the sample and is intended for application to liquids for which primarily the shear stress and shear rate are proportional (Newtonian flow behavior).1.3 The precision has only been determined for those materials, viscosity ranges, density ranges, and temperatures as indicated in Section 15 on Precision and Bias. The test method can be applied to a wider range of materials, viscosity, density, and temperature. For materials not listed in Section 15 on Precision and Bias, the precision and bias may not be applicable.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The viscosity of paint, inks and many related liquid materials is dependent on temperature. It is useful to know the extent of this dependence. One use of such information is to prepare a viscosity-temperature table or curve. Then, if ambient conditions do not allow the measurement of viscosity at the exact temperature stated in a specification or regulation, the viscosity measured at ambient temperature can be used to determine the viscosity at the temperature of interest through the use of the previously prepared table or curve. Viscosity measurements that cover a range of shear rates as well as temperatures could include shear rates associated with paint application or allow extrapolation to such shear rates. This information would enable a producer or user to estimate the effect on application of heating the paint.1.1 These test methods cover the use of rotational viscometers to determine the dependence of apparent viscosity of paints, inks and related liquid materials on temperature. The first method uses a standard rotational viscometer with concentric cylinder geometry running at a fixed rotational speed as the temperature is increased or decreased. The second method uses a rotational viscometer with cone and plate geometry running at a fixed rotational speed as the temperature is increased or decreased. The third method uses concentric cylinder or cone/plate geometry operated with a shear rate ramp at several discrete temperatures.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Viscosity values at the shear rate and temperature of this test method have been indicated to be related to the viscosity providing hydrodynamic lubrication in automotive and heavy duty engines in severe service.75.2 The viscosities of engine oils under such high temperatures and shear rates are also related to their effects on fuel efficiency and the importance of high shear rate, high temperature viscosity has been addressed in a number of publications and presentations.71.1 This test method covers the laboratory determination of the viscosity of engine oils at 150 °C and 1.0·106 s−1 using a viscometer having a slightly tapered rotor and stator called the Tapered Bearing Simulator (TBS) Viscometer.21.2 The Newtonian calibration oils used to establish this test method range from approximately 1.2 mPa·s to 7.7 mPa·s at 150 °C. The precision has only been determined for the viscosity range 1.47 mPa·s to 5.09 mPa·s at 150 °C for the materials listed in the precision section.1.3 The non-Newtonian reference oil used to establish the shear rate of 1.0·106 s−1 for this test method has a viscosity closely held to 3.55 mPa·s at 150 °C by using the absolute viscometry of the TBS.1.4 Manual, semi-automated, and fully automated TBS viscometers were used in developing the precision statement for this test method.1.5 Application to petroleum products such as base oils and formulated engine oils was determined in preparing the viscometric information for this test method.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6.1 This test method uses the milliPascal·second (mPa·s) as the unit of viscosity. This unit is equivalent to the centipoise (cP).1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 When an engine oil is cooled, the rate and duration of cooling can affect its yield stress and viscosity. In this laboratory test, a fresh engine oil is slowly cooled through a temperature range where wax crystallization is known to occur, followed by relatively rapid cooling to the final test temperature. These laboratory test results have predicted as failures the known engine oils that have failed in the field because of lack of oil pumpability.4 These documented field failing oils all consisted of oils normally tested at –25 °C. These field failures are believed to be the result of the oil forming a gel structure that results in either excessive yield stress or viscosity of the engine oil, or both.5.2 Cooling Profiles: 5.2.1 For oils to be tested at −20 °C or colder, Table X1.1 applies. The cooling profile described in Table X1.1 is based on the viscosity properties of the ASTM Pumpability Reference Oils (PRO). This series of oils includes oils with normal low-temperature flow properties and oils that have been associated with low-temperature pumpability problems (1-5).5 Significance for the −35 °C and −40 °C temperature profiles is based on the data collected from the “Cold Starting and Pumpability Studies in Modern Engines” conducted by ASTM (6, 7).5.2.2 For oils to be tested at −15 °C or −10 °C, Table X1.2 applies. No significance has been determined for this temperature profile because of the absence of appropriate reference oils. Similarly, precision of the test method using this profile for the −10 °C test temperature is unknown. The temperature profile of Table X1.2 is derived from the one in Table X1.1 and has been moved up in temperature, relative to Table X1.1, in consideration of the expected higher cloud points of the viscous oils tested at −15 °C and −10 °C.1.1 This test method covers the measurement of the yield stress and viscosity of engine oils after cooling at controlled rates over a period exceeding 45 h to a final test temperature between –10 °C and –40 °C. The precision is stated for test temperatures from –40 °C to –15 °C. The viscosity measurements are made at a shear stress of 525 Pa over a shear rate of 0.4 s–1 to 15 s–1. The viscosity as measured at this shear stress was found to produce the best correlation between the temperature at which the viscosity reached a critical value and borderline pumping failure temperature in engines.1.2 This test method contain two procedures: Procedure A incorporates several equipment and procedural modifications from Test Method D4684–02 that have shown to improve the precision of the test, while Procedure B is unchanged from Test Method D4684–02. Additionally, Procedure A applies to those instruments that utilize thermoelectric cooling technology or direct refrigeration technology of recent manufacture for instrument temperature control. Procedure B can use the same instruments used in Procedure A or those cooled by circulating methanol.1.3 Procedure A of this test method has precision stated for a yield range from less than 35 Pa to 210 Pa and apparent viscosity range from 4300 mPa·s to 270 000 mPa·s. The test procedure can determine higher yield stress and viscosity levels.1.4 This test method is applicable for unused oils, sometimes referred to as fresh oils, designed for both light duty and heavy duty engine applications. It also has been shown to be suitable for used diesel and gasoline engine oils. The applicability to petroleum products other than engine oils has not been determined.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5.1 Exception—This test method uses the SI based unit of milliPascal second (mPa·s) for viscosity which is equivalent to, centiPoise (cP).1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is useful for characterizing the flow behavior of asphalt emulsion residues and non-Newtonian asphalts. However, since non-Newtonian viscosity values depend on the level of shearing stress, its duration, and the shear history of the material, a non-Newtonian viscosity is not a unique material property. Instead, it is a parameter which is characteristic of the fluid-viscometer system under the conditions of the measurement procedure. Therefore, comparisons of non-Newtonian material behavior should only be made using apparent viscosities determined in similar viscometers under similar conditions of shearing stress and stress history. Procedures of sample preparation are especially important for repeatability or reproducibility of test results.NOTE 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capacity, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method describes procedures primarily designed to determine the apparent viscosities of residues obtained by distilling asphalt emulsions according to Test Method D6997. It is also recommended for use on non-Newtonian asphalts at any temperature within the capability of the apparatus. This test method is useful in characterizing rheological properties of non-Newtonian asphalts as a function of shear rate under the conditions of the test method. This test is run in straight open-end tube viscometers, normally at 60 °C, but is suitable for use at other temperatures. It is applicable over the range from 5 to 50 000 Pa·s.NOTE 1: The precision for this test method is based on determinations made at 60 °C.1.2 The values stated in SI units are to be regarded as the standard, except in reference to viscometer constant or calibration factor (K).1.3 Warning— Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheets (MSDS) for details and the EPA’s website (www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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