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定价: 605元 / 折扣价: 515

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定价: 605元 / 折扣价: 515

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定价: 605元 / 折扣价: 515

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定价: 605元 / 折扣价: 515

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定价: 605元 / 折扣价: 515

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定价: 605元 / 折扣价: 515

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5.1 This test method is intended for use in the laboratory or in the field for evaluating the cleanliness of distillate fuels, and liquid bio fuels. It is not applicable to on or in-line applications.5.2 This test method offers advantage over traditional filtration methods in that it is a precise rapid test, and advantage over visual methods as it is not subjective.5.3 An increase in particle counts can indicate a change in the fuel condition caused by storage or transfer for example.5.4 High levels of particles can cause filter blockages and have a serious impact on the life of pumps, injectors, pistons and other moving parts. Knowledge of particle size in relation to the metallurgy can provide vital information especially if the hardness of particles is also known from other sources.5.5 This test method specifies a minimum requirement for reporting measurements in particle size bands (see A1.1.2). Some specific applications may require measurements in other particle size bands.5.6 Obtaining a representative sample and following the recommended sample and test specimen preparation procedures and timescales is particularly important with particle counting methods. (See Sections 8, 10, 14.1.4 and Note 8.)5.7 This test method can also be used to estimate the total particulate counts excluding free water droplets in aviation turbine fuels by a chemical pretreatment of the fuel. See Appendix X2.1.1 This test method uses a specific automatic particle counter2 (APC) to count and measure the size of dispersed dirt particles, water droplets and other particles, in light and middle distillate fuel, and bio fuels such as biodiesel and biodiesel blends, in the overall range from 4 µm(c) to 100 µm(c) and in the size bands ≥4 µm(c), ≥6 µm(c), and ≥14 µm(c).NOTE 1: ASTM and military specification fuels falling within the scope of this test method include Specifications: D975 grades 1D and 2D, D1655, D3699, D4814 (see 14.1.1.1), D6751, D7467, distillate grades of D396 and D2880, MIL-DTL-83133, and MIL-DTL-16884.NOTE 2: For the purposes of this test method, water droplets are counted as particles, and agglomerated particles are detected and counted as a single larger particle. Dirt includes biological particles. Although the projected area of a particle is measured, this is expressed as the diameter of a sphere for the purposes of this test method.NOTE 3: The notation (c), used with particle sizes, is used to denote that the apparatus has been calibrated in accordance with ISO 11171. Strictly this only applies to particles up to 50 µm.NOTE 4: This test method may be used for particle sizes bands up to 100 µm(c), however the precision has only been determined for the size bands ≥4 µm(c), ≥6 µm(c), and ≥14 µm(c). All measurements are per millilitre.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers finished pellets composed of sintered gadolinium oxide-uranium dioxide of any concentration for use in light-water reactors. Materials shall adhere to specified chemical (impurity content, stoichiometry, moisture content, and gadolinium oxide concentration), nuclear (isotopic content), and physical (dimensions, density, homogeneity, integrity, axial and circumferential surface cracks, cylindrical surface chips, pellets ends, cleanliness and workmanship, identification, and irradiation stability) requirements.1.1 This specification is for finished sintered (U,Gd)O2 pellets. It applies to (U,Gd)O2 pellets containing uranium (U) of any 235U concentration and any concentration of gadolinium oxide (Gd2O3) for use in nuclear reactors.1.2 This specification recognizes the presence of reprocessed U in the fuel cycle and consequently defines isotopic limits for (U,Gd)O2 pellets made from commercial grade UO2. Such commercial grade UO2 is defined so that, regarding fuel design and manufacture, the product is essentially equivalent to that made from unirradiated U. UO2 falling outside these limits cannot necessarily be regarded as equivalent and may thus need special provisions at the fuel fabrication plant or in the fuel design.1.3 This specification does not include (a) provisions for preventing criticality accidents, (b) requirements for health and safety, (c) avoidance of hazards, or (d) shipping precautions and controls. Observance of this specification does not relieve the user of the obligation to be aware of and conform to all applicable international, federal, state, and local regulations pertaining to possessing, shipping, processing, or using source or special nuclear material. Examples of U.S. Governmental documents are Code of Federal Regulations (Latest Edition), Title 10, Part 50, Title 10, Part 70, Title 10, Part 71, and Title 49, Part 173.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 The following precautionary caveat pertains only to the technical requirements portion, Section 4, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 515元 / 折扣价: 438 加购物车

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4.1 The degree of deacetylation of chitosan, as well at the molar mass and molar mass distribution, determines the functionality of chitosan in an application. For instance, functional and biological effects are highly dependent upon the composition and molar mass of the polymer.4.2 This test method describes procedures for measurement of molar mass of chitosan chlorides and glutamates, and chitosan base, although it in principle applies to any chitosan salt. The measured molar mass is that for chitosan acetate, since the mobile phase contains acetate as counter ion. This value can further be converted into the corresponding molar mass for the chitosan as a base, or the parent salt form (chloride or glutamate).4.3 Light scattering is one of very few methods available for the determination of absolute molar mass and structure, and it is applicable over the broadest range of molar masses of any method. Combining light scattering detection with size exclusion chromatography (SEC), which sorts molecules according to size, gives the ability to analyze polydisperse samples, as well as obtaining information on branching and molecular conformation. This means that both the number-average and mass-average values for molar mass and size may be obtained for most samples. Furthermore, one has the ability to calculate the distributions of the molar masses and sizes.4.4 Multi-angle laser light scattering (MALS) is a technique where measurements of scattered light are made simultaneously over a range of different angles. MALS detection can be used to obtain information on molecular size, since this parameter is determined by the angular variation of the scattered light. Molar mass may in principle be determined by detecting scattered light at a single low angle (LALLS). However, advantages with MALS as compared to LALLS are: (1) less noise at larger angles, (2) precision of measurements is improved by detecting at several angles, and (3) the ability to detect angular variation allows determination of size, branching, aggregation, and molecular conformation.4.5 Size exclusion chromatography uses columns, which are typically packed with polymer particles containing a network of uniform pores into which solute and solvent molecules can diffuse. While in the pores, molecules are effectively trapped and removed from the flow of the mobile phase. The average residence time in the pores depends upon the size of the solute molecules. Molecules that are larger than the average pore size of the packing are excluded and experience virtually no retention; these are eluted first, in the void volume of the column. Molecules, which may penetrate the pores will have a larger volume available for diffusion, they will be retained in the column for a time dependent upon their molecular size, with smaller molecules eluting after larger molecules.4.6 For polyelectrolytes, dialysis against the elution buffer has been suggested, in order to eliminate Donnan-type artifacts in the molar mass determination by light scattering (1, 2).5 However, in the present method, the size exclusion chromatography step preceding the light scatter detection is an efficient substitute for a dialysis step. The sample is separated on SEC columns with large excess of elution buffer for 30 to 40 min, and it is therefore in full equilibrium with the elution buffer when it reaches the MALS detector.1.1 This test method covers the determination of the molar mass of chitosan and chitosan salts intended for use in biomedical and pharmaceutical applications as well as in tissue engineered medical products (TEMPs) by size exclusion chromatography with multi-angle laser light scattering detection (SEC-MALS). A guide for the characterization of chitosan salts has been published as Guide F2103.1.2 Chitosan and chitosan salts used in TEMPs should be well characterized, including the molar mass and polydispersity (molar mass distribution) in order to ensure uniformity and correct functionality in the final product. This test method will assist end users in choosing the correct chitosan for their particular application. Chitosan may have utility as a scaffold or matrix material for TEMPs, in cell and tissue encapsulation applications, and in drug delivery formulations.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 590元 / 折扣价: 502 加购物车

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4.1 The composition and sequential structure of alginate, as well as the molar mass and molar mass distribution, determines the functionality of alginate in an application. For instance, the gelling properties of an alginate are highly dependent upon the composition and molar mass of the polymer.4.2 Light scattering is one of very few methods available for the determination of absolute molar mass and structure, and it is applicable over the broadest range of molar masses of any method. Combining light scattering detection with size exclusion chromatography (SEC), which sorts molecules according to size, gives the ability to analyze polydisperse samples, as well as to obtain information on branching and molecular conformation. This means that both the number-average and mass-average values for molar mass and size may be obtained for most samples. Furthermore, one has the ability to calculate the distributions of the molar masses and sizes.4.3 Multi-angle laser light scattering (MALS) is a technique where measurements are made simultaneously over a range of different angles and used to determine the scattering at 0°, which directly relates to molecular weight. MALS detection can be used to obtain information on molecular size, since this parameter is determined by the angular variation of the scattered light. This can be related to branching, aggregation, and molecular conformation. Molar mass can also be determined by detecting scattered light at a single low angle (LALS) and assuming that this is not significantly different from the scattering at 0°.4.4 Size exclusion chromatography uses columns, which are typically packed with polymer particles containing a network of uniform pores into which solute and solvent molecules can diffuse. While in the pores, molecules are effectively trapped and removed from the flow of the mobile phase. The average residence time in the pores depends upon the size of the solute molecules. Molecules that are larger than the average pore size of the packing are excluded and experience virtually no retention; these are eluted first, in the void volume of the column. Molecules which penetrate the pores will have a larger volume available for diffusion; their retention will depend on their molecular size, with the smaller molecules eluting last.4.5 For polyelectrolytes, dialysis against the elution buffer has been suggested, in order to eliminate Donnan-type artifacts in the molar mass determination by light scattering (1, 2).6 However, in the present method, the size exclusion chromatography step preceding the light scatter detection is an efficient substitute for a dialysis step. The sample is separated on SEC columns with large excess of elution buffer for 30 to 40 min, and it is therefore in full equilibrium with the elution buffer when it reaches the MALS detector.1.1 This test method covers the determination of the molar mass (typically expressed as grams/mole) of sodium alginate intended for use in biomedical and pharmaceutical applications as well as in tissue-engineered medical products (TEMPs) by size exclusion chromatography with multi-angle laser light scattering detection (SEC-MALS). A guide for the characterization of alginate has been published as Guide F2064.1.2 Alginate used in TEMPs should be well characterized, including the molar mass and polydispersity (molar mass distribution) in order to ensure uniformity and correct functionality in the final product. This test method will assist end users in choosing the correct alginate for their particular application. Alginate may have utility as a scaffold or matrix material for TEMPs, in cell and tissue encapsulation applications, and in drug delivery formulations.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

定价: 590元 / 折扣价: 502 加购物车

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5.1 Knowledge of the boiling point distribution of stabilized crude oils is important for the marketing, scheduling, and processing of crude oil in the petroleum industry. Test Method D7169 and IP 545 purport to give such a distribution in crude oils, but are susceptible to significant errors in the light ends portion of the distribution as well as in the mass recovery of the whole crude oil due to the interference imposed by the diluent solvent. This test method allows for more accurate determination of the front end of the boiling point distribution curve, in addition to providing important C1 to C9 (nonane) component level information, and more accurate mass recovery at C9 (nonane).1.1 This test method specifies a method to determine the boiling range distribution of hydrocarbons in stabilized crude oil up to and including n-nonane. A stabilized crude oil is defined as having a Reid Vapor Pressure equivalent to or less than 82.7 kPa. The results of this test method can be combined with those from Test Method D7169 and IP 545 to give a full boiling point distribution of a crude oil (see Appendix X3).1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This practice covers procedures for calibrating and determining performance of an optical liquid-borne particle counter (LPC) which uses an optical system based upon light extinction measurement. This practice is directed towards determination of accuracy and resolution of the LPC for characterizing the size and number of particles, which have been passed into the sample inlet of the LPC. Consideration of inlet sampling efficiency is not part of this practice.1.2 The procedures covered in this practice include those to measure sample volume and flow rate, zero count level, particle sizing and counting accuracy, particle sizing resolution, particle counting efficiency, and particle concentration limit.1.3 The particle size parameter reported in this practice is the equivalent optical diameter based on projected area of calibration particles with known physical properties dispersed in liquid. The manufacturer normally specifies the minimum diameter that can be reported by an LPC; the dynamic range of the LPC being used determines the maximum diameter that can be reported for a single sample. Typical minimum reported diameters are approximately 2 m, and a typical dynamic range specification will be approximately from 50 to 1.1.4 The counting rate capability of the LPC is limited by temporal coincidence of particles in the sensing volume of the LPC and by the saturation level or maximum counting rate capability of the electronic sizing and counting circuitry. Coincidence is defined as the simultaneous presence of more than one particle within the LPC optically defined sensing zone at any time. The coincidence limit is a statistical function of particle concentration in the sample and the sensing zone volume when particle size is insignificant in comparison to the sensing volume dimensions. This limitation may be modified by the presence of particles with dimension so large as to be a significant fraction of the sensing zone dimension. The saturation level rate of the electronic counting circuitry shall be specified by the manufacturer and is normally greater than the LPC recommended maximum counting rate for the particle concentrations used for any portion of this practice.1.5 Calibration in accordance with all parts of this practice may not be required for routine field calibration of an LPC unless significant changes have occurred in operation of the LPC or major component repairs or replacements have been made. The LPC shall then be taken to a suitable metrology facility for complete calibration. Normal routine field calibration may determine sample flow rate, zero count level, and particle sizing accuracy. The specific LPC functions to be calibrated shall be determined on the basis of agreement between the purchaser and the user. The maximum time interval between calibrations shall be determined by agreement between the purchaser and the user, but shall not exceed twelve months, unless LPC stability for longer periods is verified by measurements in accordance with this practice.This standard may involve hazardous materials, operation, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 This practice is useful as a screening basis for acceptance or rejection of transparencies during manufacturing so that units with identifiable flaws will not be carried to final inspection for rejection at that time.4.2 This practice may also be employed as a go-no go technique for acceptance or rejection of the finished product.4.3 This practice is simple, inexpensive, and effective. Flaws identified by this practice, as with other optical methods, are limited to those that produce temperature gradients when electrically powered. Any other type of flaw, such as minor scratches parallel to the direction of electrical flow, are not detectable.1.1 This practice covers a standard procedure for detecting flaws in the conductive coating (heater element) by the observation of polarized light patterns.1.2 This practice applies to coatings on surfaces of monolithic transparencies as well as to coatings imbedded in laminated structures.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 515元 / 折扣价: 438 加购物车

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4.1 Pressure-sensitive film tapes are supplied in roll form. For such a tape to be useful a strip of the tape must be easily dispensed or severed from the roll by means of a cutter found on most dispensers. This test method is a means of measuring the ease of this severing or dispensing of the tape.4.2 This test method provides information that can be used in material specifications for product design and quality assurance applications. It can be used in comparing different tape products on specific dispensing blades.4.3 This test method may be suited for office and stationery and tapes with acetate, cellophane, or light-duty plastic backings. Some tapes may be shown to be difficult to dispense under these conditions yet are readily dispensable with other dispensing systems.NOTE 1: Backings described in CID A-A-113 are typical backings.1.1 This test method covers the measurement of the force and elongation required to dispense pressure-sensitive film tape on a 1-in. core intended for office and stationery applications from a desk-top dispenser.1.2 The values stated in either SI or inch-pound units are to be regarded separately as standard. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The purpose of this practice is to provide the minimum requirements necessary for the establishment of a quality assurance and production acceptance program for a manufacturer of light sport aircraft.1.1 This practice establishes the minimum requirements for the development of a Quality Assurance and Production Acceptance Program, to be used for the manufacture of LSA's or LSA kits.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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