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5.1 The temperatures of opaque surfaces exposed to solar radiation are generally higher than the adjacent air temperatures. In the case of roofs or walls enclosing conditioned spaces, increased inward heat flows result. In the case of equipment or storage containers exposed to the sun, increased operating temperatures usually result. The extent to which solar radiation affects surface temperatures depends on the solar reflectance of the exposed surface. A solar reflectance of 1.0 (100 % reflected) would mean no effect on surface temperature while a solar reflectance of 0 (none reflected, all absorbed) would result in the maximum effect. Coatings of specific solar reflectance are used to change the temperature of surfaces exposed to sunlight. Coatings and surface finishes are commonly specified in terms of solar reflectance. The initial (clean) solar reflectance must be maintained during the life of the coating or finish to have the expected thermal performance.5.2 The test method provides a means for periodic testing of surfaces in the field or in the laboratory. Monitor changes in solar reflectance due to aging and exposure, or both, with this test method.5.3 This test method is used to measure the solar reflectance of a flat opaque surface. The precision of the average of several measurements is usually governed by the variability of reflectances on the surface being tested.5.4 Use the solar reflectance that is determined by this method to calculate the solar energy absorbed by an opaque surface as shown in Eq 1.5.4.1 Combine the absorbed solar energy with conductive, convective and other radiative terms to construct a heat balance around an element or calculate a Solar Reflectance Index such as that discussed in Practice E1980.1.1 This test method covers a technique for determining the solar reflectance of flat opaque materials in a laboratory or in the field using a commercial portable solar reflectometer. The purpose of the test method is to provide solar reflectance data required to evaluate temperatures and heat flows across surfaces exposed to solar radiation.1.2 This test method does not supplant Test Method E903 which measures solar reflectance over the wavelength range 250 nm to 2500 nm using integrating spheres. The portable solar reflectometer is calibrated using specimens of known solar reflectance to determine solar reflectance from measurements at four wavelengths in the solar spectrum: 380 nm, 500 nm, 650 nm, and 1220 nm. This technique is supported by comparison of reflectometer measurements with measurements obtained using Test Method E903. This test method is applicable to specimens of materials having both specular and diffuse optical properties. It is particularly suited to the measurement of the solar reflectance of opaque materials.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The most direct and accessible methods for obtaining the color coordinates of object colors are by instrumental measurement using spectrophotometers or colorimeters with either hemispherical or bidirectional optical measuring systems. This test method provides procedures for such measurement by reflectance spectrophotometry using a hemispherical optical measuring system.5.2 This test method is especially suitable for measurement of the following types of specimens for the indicated uses (Guide E179 and Practice E805):5.2.1 All types of object-color specimens to obtain data for use in computer colorant formulation.5.2.2 Object-color specimens for color assessment.5.2.2.1 For the measurement of plane-surface high-gloss specimens, the specular component should generally be excluded during the measurement.5.2.2.2 For the measurement of plane-surface intermediate-gloss specimens and of textured-surface specimens, including textiles, where the first-surface reflection component may be distributed over a wide range of angles, measurement may be made with the specular component included, but the resulting color coordinates may not correlate best with visual judgments of the color. The use of bidirectional geometry, such as 45/0 or 0/45, may lead to better correlations.5.2.2.3 For the measurement of plane-surface, low-gloss (matte) specimens, the specular component may either be excluded or included, as no significant difference in the results should be apparent.5.2.3 Specimens with bare metal surfaces for color assessment. For this application, the specular component should generally be included during the measurement.5.3 This test method is not recommended for measurement of the following types of specimens, for which the use of bidirectional measurement geometry (0/45 or 45/0) is preferable (Guide E179):5.3.1 Object-color specimens of intermediate gloss,5.3.2 Retroreflective specimens, and5.3.3 Fluorescent specimens (Practice E991).5.3.3.1 When there is doubt as to whether the specular component of reflection should be included or excluded, both measurements should be made, and the results correlated with visual judgments. Thereafter, the method with higher visual correlation should be utilized.5.3.3.2 When measurements of two specimens whose gloss, or texture, are substantially different from each other, are to be utilized in a color-difference comparison, generally the specular component should be included in each measurement. This has the effect of including in both measurements all the first surface reflections whether diffuse or specular. These first surface reflections are subtracted from each other in the color-difference equation, and differences in the body color remain, which is what is usually sought.1.1 This test method describes the instrumental measurement of the reflection properties and color of object-color specimens by the use of a spectrophotometer or spectrocolorimeter with a hemispherical optical measuring system, such as an integrating sphere.1.2 The test method is suitable for use with most object-color specimens. However, it should not be used for retroreflective specimens or for fluorescent specimens when highest accuracy is desired. Specimens having intermediate-gloss surfaces should preferably not be measured by use of this geometry.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Solar reflectance is an important factor affecting the temperature of a sunlit surface and that of the near-surface ambient air temperature. The test method described herein measures the solar reflectance of surfaces in natural sunlight.1.1 This test method covers the measurement of solar reflectance of various horizontal and low-sloped surfaces and materials in the field, using an albedometer or pyranometer. The test method is intended for use when the sun angle to the normal from a surface is less than 45°.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Mechanical properties of PEEK polymers, such as stiffness or yield strength, are influenced by the level of crystallinity.5 The reported crystallinity index determined by this test method has been correlated with percent crystallinity in PEEK polymers by wide-angle X-ray scattering (WAXS) experiments.2, 34.2 This test method may be useful for both process development, process control, product development, and research.1.1 This test method describes the collection of absorption spectra of polyetheretherketone (PEEK) polymer in filled and unfilled grades, as supplied by a vendor, and the subsequent calculation of the percent crystallinity. The material is evaluated by infrared spectroscopy. The intensity (height) of the absorbance peaks is related to the amount of crystalline regions present in the material.1.2 This test method can be used for PEEK consolidated forms, such as injection molded parts, as long as the samples are optically flat and smooth.1.3 The applicability of the infrared method to industrial and medical grade PEEK materials has been demonstrated by scientific studies.2, 3 Percentage of crystallinity is related to R-FTIR measurement by calibration through wide-angle x-ray scattering (WAXS) crystallinity measurements.2, 3 It is anticipated that this test method, involving the peak heights near 1305 cm-1 and 1280 cm-1, will be evaluated in an Interlaboratory Study (ILS) conducted according to Test Method E691.1.4 This test method does not suggest a desired range of crystallinity for specific applications.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Tinting strength is one of the most important properties of a white pigment. This test method provides a means of testing this property for quality control.4.2 This test method is a referee method, and the vehicle for preparing the dispersion and the black for tinting are suggested, but others may be used provided both the purchaser and the seller agree to the changes.4.3 The results obtained with a muller do not necessarily agree with industrial situations where different dispersing conditions exist. However, dispersing with a muller is a fast, relatively inexpensive way of testing tinting strength for routine quality control.1.1 This test method describes the procedure for determining the relative tinting strength of white pigments by reflectance measurements of black tints.1.2 This test method is applicable only for comparing the test pigment with a reference standard of the same type and grade.NOTE 1: Test Method D332 describes a procedure for visual assessment of blue-tinted samples.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method covers measurement of total luminous reflectance factor of opaque, nonfluorescent specimens by use of an integrating-sphere reflectometer with illumination at an angle of 30° from the surface normal and diffuse viewing with specular component included. 1.2 This test method is intended to be used for evaluation of total luminous reflectance factor of reflector lighting sheet material. It may be used for evaluation of other material when its specific geometry has been found to be applicable. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 The mean maximum reflectance of the vitrinite component in coal as determined by this test method is often used as an indicator of rank as presented in Classification D388, independent of petrographic composition, and in the characterization of coal as feedstock for carbonization, gasification, liquefaction, and combustion processes.5.2 This test method is for use in scientific and industrial research.1.1 This test method covers the microscopical determination of both the mean maximum and mean random reflectances measured in oil of polished surfaces of vitrinite and other macerals present in coals ranging in rank from lignite to anthracite. This test method can be used to determine the reflectance of other macerals.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The most direct and accessible methods for obtaining the color coordinates of object colors are by instrumental measurement using spectrophotometers or spectrocolorimeters with either hemispherical or bidirectional optical measuring systems. This test method provides procedures for such measurement by spectrophotometry using a bidirectional (0:45 or 45:0) optical measuring system. The method for color and color difference measurement using filter colorimeters is contained in Test Method E1347.5.2 This test method is especially suitable for measurement of the following types of specimens for the indicated uses (see also Guide E179 and Practice E805):5.2.1 Object-color specimens of any gloss level for color assessment.5.2.2 Object-color specimens with physically flat, smooth surfaces from which to obtain data for use in computer colorant formulation.5.2.3 Retroreflective specimens.NOTE 1: To ensure inter-instrument agreement in the measurement of specimens with intermediate gloss, for formulation, or of retroreflective specimens, significantly tighter tolerances than those given in Practice E1164, Influx and Efflux Conditions, 45°:Normal (45:0) and Normal:45° (0:45) Reflectance Factor section, may be required for the instrument angles of illumination and viewing. Information on the required tolerances is being developed.5.3 This test method is not recommended for measurement of specimens with bare metal surfaces for color assessment, for which the use of hemispherical measurement geometry, as with an integrating-sphere type instrument, is preferable (see Guide E179).1.1 This test method covers the instrumental measurement of the reflection properties and color of object-color specimens by use of a spectrophotometer or spectrocolorimeter with a bidirectional optical measuring system, such as annular, circumferential, or uniplanar 45:0 or 0:45 geometry.1.2 This test method is generally suitable for any non-fluorescent, flat object-color specimen. It is especially recommended for measuring retroreflective specimens and specimens of intermediate gloss.1.3 Procedures required for the measurement of fluorescent object color are given in Practice E991 and Practice E2153.1.4 Procedures required for the measurement of color using filter colorimeters are contained in Test Method E1347 and this standard does not address those instruments.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Hydrogen sulfide is an odorous substance which is offensive even at low concentrations in the atmosphere and toxic at higher levels. It may be a product of biological processes in the absence of oxygen, as may occur in municipal landfills. It is emitted from geothermal sources, occurs in oil and gas, and may be emitted from industrial processes. Measurement is required for air pollution studies, for pollution control, environmental justice based monitoring, and for plume characterization. This test method is intended for hydrogen sulfide content up to 3000 ppbv. Measurement of hydrogen sulfide above this concentration in gaseous fuels, carbon dioxide or other gaseous matrices is described in Test Method D4084. Equipment described is suitable for fixed site or for mobile monitoring.1.1 This test method covers the automatic continuous determination of hydrogen sulfide (H2S) in the atmosphere or in gaseous samples in the range from one part per billion by volume (1 ppb/v) to 3000 ppb/v. Information obtained may be used for air-pollution studies, fence-line monitoring, and other source emission monitoring.1.2 The range may be extended by appropriate dilution techniques or by equipment modification.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (See Section 9 for specific safety precautionary statements.)1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The solar reflectance of a DRM depends on the solar incidence angle. This method is intended to provide solar reflectance values for DRM roofing products.1.1 This test method covers a technique for determining the solar reflectance of a directionally reflective material using a commercial portable solar reflectometer, including but not limited to roofing materials with granules or surface design that results in angularly dependent reflectance. The purpose of the method is to evaluate the seasonal and annual solar reflectances of a directionally reflective roofing product.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Glazed apertures in buildings are commonly utilized for the controlled admission of both light and solar radiant heat energy into the structure. Other devices may also be used to reflect light and solar radiant heat into a building.5.1.1 Most of the solar radiant energy entering a building in this manner possesses wavelengths that lie between 300 and 2500 nm (3000 to 25 000 Å). Only the portion between 380 and 760 nm is visible radiation, however. In daylighting applications, it is therefore important to distinguish the solar radiant energy transmittance and reflectance of these materials from their luminous (visual or photometric) transmittance and reflectance.5.2 For comparisons of the energy and illumination performances of building fenestration systems it is important that the calculation or measurement, or both, of solar radiant and luminous transmittance and reflectance of materials used in fenestration systems use the same incident solar spectral irradiance distribution.5.2.1 Solar luminous transmittance and reflectance are important properties in describing the performance of components of solar illumination systems (for example, windows, clerestories, skylights, shading and reflecting devices) and other fenestrations that permit the passage of daylight as well as solar energy into buildings.5.3 This practice is useful for determining the luminous transmittance and reflectance of glazing materials and diffusely or quasi-diffusely reflecting materials used in daylighting systems. For the results of this practice to be meaningful, inhomogeneities or corrugations in the sample must not be large. Test Method E1175 (or Test Method E972) is available for sheet materials that do not satisfy this criterion.1.1 This practice describes the calculation of luminous (photometric) transmittance and reflectance of materials from spectral radiant transmittance and reflectance data obtained from Test Method E903.1.2 Determination of luminous transmittance by this practice is preferred over measurement of photometric transmittance by methods using the sun as a source and a photometer as detector except for transmitting sheet materials that are inhomogeneous, patterned, or corrugated.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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