5.1 A major factor affecting the long term performance of insulating materials is thermal degradation. It is possible that factors, such as moisture and vibration, will cause failures after the material has been weakened by thermal degradation.5.2 An electrical insulating varnish is effective in protecting electrical equipment only as long as it retains its physical and electrical integrity.5.3 The thermal degradation of the varnish results in weight loss, porosity, crazing, and generally a reduction in flexibility. Degradation of the varnish can be detected by a decrease in dielectric strength, which is therefore used as the failure criterion for this test method.5.4 Electrical insulating varnishes undergo flexing in service due to vibration and thermal expansion. For this reason, this functional test includes flexing and elongation of the insulation. The electrodes used in this test method are designed to elongate the outer surface of the specimen 2 % with respect to the neutral axis of the base fiber while being tested for dielectric breakdown.1.1 This test method covers the determination of the relative thermal endurance of flexible electrical insulating varnishes by determining the time necessary at elevated temperatures to decrease the dielectric breakdown of the varnish to an arbitrarily selected value when applied to a standard glass fiber fabric.1.2 This test method does not apply to varnishes that lose a high percentage of their dielectric breakdown voltage when flexed before elevated temperature exposure as prescribed in the screening test (Section 9). Examples of such varnishes are those used for high speed armatures and laminated structures. Also, this test method is not applicable to varnishes which distort sufficiently during thermal elevated temperature exposure so that they cannot be tested using the curved electrode assembly.1.3 Thermal endurance is expressed in terms of a temperature index.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.NOTE 1: There is no equivalent IEC or ISO standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method covers procedures for the qualitative detection of rosin in varnishes by the Lieberman-Storch Test, and the Halphen-Hicks Test. The rosin may be present as either free rosin (abietic acid), esterified rosin, or as metal salts.1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.>

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This guide covers the proper selection and use of procedures for testing varnishes. Properties of liquid varnishes that may be tested are as follows: appearance; color (Gardner, tristimulus, and Platinum-Cobalt scale); viscosity (Gardner-Holdt bubble time, Ford cup efflux, and high precision kinematic viscosity); specific gravity; volatile content; nonvolatile matter; flash point (tag closed-cup, Pensky Martens, tag open-cup, and Setaflash closed tester); skinning; acid value; reactivity of paint liquids; quantitative rosin content; and qualitative rosin content (Lieberman-Storch and Halphen-Hicks). Drying and curing properties that may be tested are drying and print free time. Finally, properties of dry varnish that may be tested are as follows: gloss (specular gloss and reflective haze); resistance of dried films to water and alkali; abrasion resistance by carborundum air blast, falling abrasive, and Taber abraser; exterior durability; color of dried film; and clear floor sealers.1.1 This guide covers the selection and use of procedures for testing varnishes. Some test methods are included, but most sections refer to specific ASTM test methods.1.2 Varnishes may be applied under such diverse conditions to so many different surfaces and their dried films may be subjected to so many kinds of wear and exposure, that it is not possible to assure desired performance from a single selection of test methods and numerical results. Those skilled in varnish technology may find partial assurance of obtaining desired qualities in various types of varnishes through careful selection of the methods covered and intelligent interpretation of results.1.3 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is useful for the evaluation of insulating varnish performance in high humidity exposure.1.1 This test method covers the mechanical performance of electrical insulating varnishes subjected to high humidity conditions.1.2 The values stated in SI units are to be regarded as standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See 7.1.NOTE 1: There is not ISO or IEC equivalent.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is useful for the evaluation of insulating varnish performance in chemical exposure.1.1 This test method covers the mechanical performance of insulating varnishes after exposure to various chemicals.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See 7.1.NOTE 1: There is no IEC/ISO equivalent.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Weight loss is useful for indicating:5.1.1 A form of degradation at elevated temperatures in air, and5.1.2 Evolution of volatiles that have the potential to affect other components.1.1 This test method covers the measurement of the loss in weight of cured electrical insulating varnishes on exposure to elevated temperature in air.1.2 The values stated in SI units are the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see Section 7.NOTE 1: IEC 60216 Part 2 is technically equivalent to this standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is useful in determining the performance of varnishes over enamelled magnet wire when subjected to the specified sodium chloride solution. It is useful in evaluating the resistance of varnished magnet wire to a diluted sodium chloride solution under applied voltage.1.1 This test method covers the electrical performance in a specified water solution of an insulating varnish applied over enamelled magnet wire.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 6.NOTE 1: There is no IEC method equivalent to this standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Control—The following tests are useful for control purposes during the manufacture and use of varnishes, and for determining the uniformity of batches:4.1.1 Specific gravity,4.1.2 Viscosity,4.1.3 Flash point, and4.1.4 Nonvolatile matter by weight.4.2 Performance—The following tests are useful for determining the performance of varnishes during application and use:4.2.1 Drainage,4.2.2 Time of drying,4.2.3 Build,4.2.4 Dielectric strength,4.2.5 Thermal endurance,4.2.6 Varnish compatibility,4.2.7 Salt water proofness, and4.2.8 Oil resistance.1.1 These test methods cover tests for solvent containing varnishes primarily intended to provide electrical, mechanical, and chemical protection for electrical equipment. These test methods include tests for control and performance as follows:Procedure SectionBuild 38 – 42Dielectric Strength 43 – 48Drainage 26 – 32Flash Point 18 – 20Nonvolatile Matter 21 – 25Oil Resistance 54 – 56Preparation of Test Specimens     7Specific Gravity  9 – 12Temperature Index 49 – 50Time of Drying 33 – 37Varnish Compatibility 51 – 53Viscosity 13 – 171.2 Where the entire test method is included in this standard, the precision and bias are not known unless given in the stated method.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 5.NOTE 1: There is no equivalent IEC standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is used to determine the effect of exposure to elevated temperatures on the bond strength of combinations of magnet wire insulations and electrical insulating varnishes. The results are used as a guide for the comparison and selection of varnishes and combinations of varnishes and magnet wire insulation for specific applications. Test Methods D1932 and D3251 describe additional tests for determining the thermal endurance of insulating varnishes. A comprehensive evaluation of thermal characteristics includes a comparison of the thermal endurance determined in these different ways.5.2 This test method is useful for research and product qualifications purposes.1.1 This test method covers the determination of the thermal endurance of electrical insulating varnishes alone or in combinations with magnet wire insulation. Changes in the helical coil bond strength are used as the test criteria. The coils are made from bare aluminum or copper wire, or from film- or fiber-insulated magnet wire.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.NOTE 1: There is no similar or equivalent IEC standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific precautionary statement, see Section 7.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Values obtained by flexural test provides information with regard to the bond strength of the particular varnish in combination with a particular type of magnet wire, when measured under conditions described in this test method.1.1 This test method covers the determination of the bond strength of an electrical insulating varnish when applied to a twisted coil of film-insulated magnet wire. The use of a particular type of film-insulated wire will show the values for that combination of film coating and varnish.1.2 The values stated in inch-pound units are the standard. The values given in parentheses are for information only.NOTE 1: Although this standard and Method C of IEC 61033 differ in approach or detail, data obtained using either are technically equivalent.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in Section 7.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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