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5.1 Free films are required for conducting tests to evaluate physical and mechanical properties such as tensile and elongation (Test Methods D2370), moisture vapor permeability (Test Methods D1653 and E96/E96M), microbiological activity resistance (Test Method D5590), and other physical properties of organic coatings where the substrate may interfere with the determination.1.1 This practice covers the preparation of free films of organic coatings for use in determining the physical properties of the coatings.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 These test methods cover the determination of the amount of apparent free phenol in synthetic phenolic resins or solutions used for coating purposes. The test method for isolation of the free phenol applies to all the commonly used resins except those containing p-phenyl-phenol. Test Method A applies to the simpler phenols up to and including the xylenols; Test Method B applies to the common alkylated phenols. >1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. >

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4.1 In general, steam treatment of FCC catalyst can be used either to compare a series of cracking catalysts at a simulated equilibrium condition or conditions, or to simulate the equilibrium condition of a specific cracking unit and a specific catalyst. This guide gives an example for the first purpose and an approach for the latter purpose.1.1 This guide covers the deactivation of fresh fluid catalytic cracking (FCC) catalyst by hydrothermal treatment prior to the determination of the catalytic cracking activity in the microactivity test (MAT) or the Advanced Cracking Evaluation (ACE) test.1.2 The hydrothermal treatment of fresh FCC catalyst, prior to the MAT or the ACE test, is important because the catalytic activity of the catalyst in its fresh state is an inadequate measure of its true commercial performance. During operation in a commercial cracking unit, the catalyst is deactivated by thermal, hydrothermal, and chemical degradation. Therefore, to maintain catalytic activity, fresh catalyst is added (semi) continuously to the cracking unit, to replace catalyst lost through the stack or by withdrawal, or both. Under steady state conditions, the catalyst inventory of the unit is called equilibrium catalyst. This catalyst has an activity level substantially below that of fresh catalyst. Therefore, artificially deactivating a fresh catalyst prior to determination of its cracking activity should provide more meaningful catalyst performance data.1.3 Due to the large variations in properties among fresh FCC catalyst types as well as between commercial cracking unit designs or operating conditions, or both, no single set of steam deactivation conditions is adequate to artificially simulate the equilibrium catalyst for all purposes.1.3.1 In addition, there are many other factors that will influence the properties and performance of the equilibrium catalyst. These include, but are not limited to: deposition of heavy metals such as Ni, V, and Cu; deposition of light metals such as Na; and contamination from attrited refractory linings of vessel walls. Furthermore, commercially derived equilibrium catalyst represents a distribution of catalysts of different ages (from fresh to >300 days). Despite these apparent problems, it is possible to obtain reasonably close agreement between the performances of steam deactivated and equilibrium catalysts. It is also recognized that it is possible to steam deactivate a catalyst so that its properties and performance poorly represent the equilibrium. It is therefore recommended that when assessing the performance of different catalyst types, a common steaming condition be used. Catalyst deactivation by metals deposition is not addressed in this guide, but is addressed in Guide D7206/D7206M.1.4 This guide offers two approaches to steam deactivate fresh catalysts. The first part provides specific sets of conditions (time, temperature, and steam pressure) that can be used as general pre-treatments prior to comparison of fresh FCC catalyst MAT activities (Test Method D3907) or activities plus selectivities (Test Methods D5154 and D7964).1.4.1 The second part provides guidance on how to pretreat catalysts to simulate their deactivation in a specific FCCU and suggests catalyst properties which can be used to judge adequacy of the simulation. This technique is especially useful when examining how different types of catalyst may perform in a specific FCCU, provided no other changes (catalyst addition rate, regenerator temperature, contaminant metals levels, etc.) occur. This approach covers catalyst physical properties that can be used as monitors to indicate the closeness to equilibrium catalyst properties.1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This test method covers the determination of free moisture in ceramic whiteware clays. Whiteware clays may be shipped as a bulk shipment in lumps, a bulk shipment of shredded or coarsely ground clay, or in bagged lots of ground or airfloated clay. Directions are given in this test method for obtaining representative samples of the clay shipment to be used in subsequent tests for the properties of the clay in the shipment. Percentage of free moisture shall be calculated to the nearest 0.1%.1.1 This test method covers the determination of free moisture in ceramic whiteware clays. Whiteware clays may be shipped as a bulk shipment in lumps, a bulk shipment of shredded or coarsely ground clay, or in bagged lots of ground or airfloated clay. Directions are given in this test method for obtaining representative samples of the clay shipment to be used in subsequent tests for the properties of the clay in the shipment.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The tack-free time is a measure of the surface cure time and may generally be correlated to a variety of useful parameters such as the time interval before the sealant (1) resists damage by touch or light surface contact, (2) resists job-site or airborne dirt pick-up, (3) resists impinging rainfall.5.2 The tack-free time is sometimes used as an on-the-job quality assurance test. A quality product that is consistent and reproducible will generally fall within a maximum and minimum tack-free time.5.3 This test for tack-free time can be used at any temperature and humidity. It is important that if a sealant will be used in a climate quite different than the standard conditions called out in this test method, then those conditions be used to test the sealant.1.1 This test method covers a procedure for the determination of the tack-free time property of single- and multi-component elastomeric sealants commonly used for sealing, caulking, and glazing in buildings and related construction.1.2 This test method is applicable to self-leveling and non-sag grades of sealant. Sealants requiring slight heating to facilitate extrusion from the cartridge or gun are also described by this test method.NOTE 1: See Specification C920 for type and grade definitions.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: Currently, there is no ISO standard similar to this specification.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Free halogens will react with any residual moisture in a solvent to form acid. These acids can cause corrosion to process and storage equipment used for halogenated solvents.4.2 The presence of free halogens in halogenated solvents is often an indication that the stabilizers in the solvent system are breaking down.4.3 This test method provides a means of detecting the presence of free halogens in halogenated solvents and their admixtures.1.1 This test method covers the evaluation of free halogens in halogenated organic solvents and their admixtures.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is intended for use in evaluating the ability of a container to withstand the sudden shock resulting from a free fall drop impact, or to evaluate the ability of a container and its inner packing to protect its contents during the sudden shock resulting from a free fall drop impact. This test method may also be used to compare the performance of different package designs. This test method may also permit observation of the progressive failure of a container and the damage to its contents.4.2 This test method is particularly suitable for containers that are normally handled manually during some part of their distribution cycle. Containers of such bulk or mass that they cannot be handled manually may be tested more satisfactorily in accordance with Test Method D880, Test Methods D6055, Test Methods D6179, or Test Methods D4003. See Practice D4169 for additional guidance.1.1 This test method covers procedures for the drop testing of loaded boxes, cylindrical containers, and bags and sacks by the free-fall method.1.2 For containers not exceeding 110 lb (50 kg), this test method fulfills the requirements of ISO Standards 2206:1987 and 2248:1985. These ISO standards may describe procedures that do not meet the requirements for this test method.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Free and bonded glycerin content reflects the quality of biodiesel. A high content of free glycerin may cause problems during storage, or in the fuel system, due to separation of the glycerin. A high total glycerin content can lead to injector fouling and may also contribute to the formation of deposits at injection nozzles, pistons, and valves.1.1 This test method covers the quantitative determination of total monoglyceride, total diglyceride, total triglyceride, and free and total glycerin in B-100 methyl esters by gas chromatography. The range of quantitation for monoglyceride is 0.009 % to 0.77860 % by mass, for diglyceride is 0.092353 % to 0.54475 % by mass, and for triglyceride is 0.00092857 % to 1.3881 % by mass. The range of quantitation for free glycerin is 0.0005714 % to 0.019533 % by mass and for total glycerin from 0.0090714 % to 0.42767 % by mass. This procedure is not applicable to vegetable oil methyl esters obtained from lauric oils, such as coconut oil and palm kernel oil.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification establishes the requirements for wrought forms and fabricated shapes of oxygen-free copper with UNS No. C10100 suitable for use in electron devices. Specimens shall be appropriately sampled and shall undergo hydrogen embrittlement (reverse bend) test, special macro examination, and special microscopical examination. Materials shall adhere to specified mechanical, dimensional, chemical composition, electrical resistivity, and grain size requirements.1.1 This specification establishes the requirements for wrought and fabricated shapes made from Copper UNS2 No. C10100, conforming to the chemical requirements of Specification B170, Grade 1, and suitable for use in electron devices.1.2 The requirements of this specification are in addition to those prescribed in the following product specifications appropriate to the material being ordered: B1, B2, B3, B75/B75M, B152/B152M, B170, B187/B187M, B188, B272, and B372. In case of conflict, however, this specification shall take precedence.1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3.1 Exception—grain sizes are in metric units and are standard.1.4 The following safety hazard caveat applies to sections 17.4, 17.5 and 18.7 of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 It has long been the practice to include in fuel specifications a requirement that the fuel be clear and bright and free of visible particulate matter (see Note 1). However, there has been no standard method for making this determination so that practices have differed. This test method provides standard procedures for the test.NOTE 1: Clean and bright is sometimes used in place of clear and bright. The meaning is identical.5.2 Procedure 1 provides a rapid pass/fail method for contamination in a distillate fuel. Procedure 2 provides a gross numerical rating of haze appearance, primarily as a communication tool. Other test methods, including Test Methods D2276, D2709, and D4860, permit quantitative determinations of contaminants. No relationship has been established between Procedure 2 and these quantitative methods.5.2.1 Test Method D8148 has established a correlating relationship with Procedure 2 appearance rating numbers by reporting a correlating instrument haze rating (IHR) based upon its spectroscopically determined haze clarity index (HCI). Supporting data can be found in RR:D02-1876.55.3 Limited laboratory evaluations of samples that have failed this clear and bright test indicate that an experienced tester can detect as little as 40 ppm of free water in the fuel.1.1 This test method covers two procedures for estimating the presence of suspended free water and solid particulate contamination in distillate fuels having distillation end points below 400 °C and an ASTM color of 5 or less.1.1.1 Both procedures can be used as field tests at storage temperatures, or as laboratory tests at controlled temperatures.1.1.2 Procedure 1 provides a rapid pass/fail method for contamination. Procedure 2 provides a gross numerical rating of haze appearance.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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