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5.1 This slug test field procedure is used in conjunction with a slug test analytical procedure, such as Test Method D4104 to provide quick and relatively inexpensive estimates of transmissivity.5.2 The slug test provides an advantage over pumping tests in that it does not require the disposal of the large quantities of water that may be produced. This is of special importance when testing a potentially contaminated aquifer. However, slug tests reflect conditions near the well, therefore are influenced by near-well conditions, such as gravel pack, poor well development, and skin effects, as a result, slug test results should be viewed as semi-quantitative in comparison to pumping test results.5.3 Slug tests may be made in aquifer materials of lower hydraulic conductivity than generally considered suitable for hydraulic testing with pumping tests.5.4 The method of data analysis (analytical procedure) should be known prior to the field testing to ensure that all appropriate dimensions and measurements are properly recorded. Selection of the analytical procedure can be aided by using Guide D4043, Test Method D5785, Test Method D5881, and Test Method D5912.NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the field procedure for performing an in situ instantaneous change in head (slug) test.1.2 This test method is used in conjunction with an analytical procedure such as Test Method D4104 to data analysis and to determine aquifer properties.1.3 Units—The values stated in either SI Units or inch-pound units are to be regarded separately as standard. The values in each system may not be exact equivalents; therefore each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this test method.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 Lubricating oils can be formulated with additives, which can act as detergents, anti-oxidants, anti-wear agents, and so forth. Some additives can contain one or more of calcium, copper, magnesium, phosphorus, sulfur, and zinc. This test method can be used to determine if the oils, additives, and additive packages meet specification with respect to content of these elements.4.2 Several additive elements and their compounds are added to the lubricating oils to give beneficial performance (Table 3).4.3 This test method can also be used to determine if lubricating oils, additives, and additive packages meet specification with respect to chlorine concentration. In this context, specification can refer to contamination.4.4 This test method is not intended for use on samples that contain some component that significantly interferes with the analysis of the elements specified in the scope.4.5 This test method can complement other test methods for lube oils and additives, including Test Methods D4628, D4927, D4951, and D5185.1.1 This test method covers the determination of calcium, chlorine, copper, magnesium, phosphorus, sulfur, and zinc in unused lubricating oils, additives, and additive packages by wavelength dispersive X-ray fluorescence spectrometry. Matrix effects are handled with mathematical corrections.1.2 For each element, the upper limit of the concentration range covered by this test method is defined by the highest concentration listed in Table 1. Samples containing higher concentrations can be analyzed following dilution.1.3 For each element, the lower limit of the concentration range covered by this test method can be estimated by the limit of detection (LOD)2 (see also 40 CFR 136 Appendix B) or limit of quantification (LOQ),2 both of which can be estimated from Sr, the repeatability standard deviation. LOD and LOQ values, determined from results obtained in the interlaboratory study on precision, are listed in Table 2.1.3.1 LOD and LOQ are not intrinsic constants of this test method. LOD and LOQ depend upon the precision attainable by a laboratory when using this test method.1.4 This test method uses regression software to determine calibration parameters, which can include influence coefficients (that is, interelement effect coefficients) (Guide E1361), herein referenced as alphas. Alphas can also be determined from theory using relevant software.1.5 Setup of this test method is intended for persons trained in the practice of X-ray spectrometry. Following setup, this test method can be used routinely.1.6 The values stated in either SI units or angstrom (Å) units are to be regarded separately as standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Withdrawal or injection well test field procedures are used with appropriate analytical procedures in appropriate hydrogeological sites to determine transmissivity and storage coefficient of aquifers and hydraulic conductivity of confining beds.5.2 Practice D3740 provides evaluation factors for the activities in this test method.NOTE 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.5.3 This test method may be limited due to the correspondence between the field situation determined by this test method and the simplifying assumptions of the analytical Test Methods D4105/D4105M or D4106 and D4043.1.1 This test method covers the field procedure for selecting well locations, controlling change (discharge or injection) rates, and measuring water levels used to analyze the hydraulic properties of an aquifer or aquifers and adjacent confining beds.1.2 This test method is used in conjunction with an analytical procedure such as Test Methods D4105/D4105M or D4106 to evaluate the data and determine aquifer properties.1.3 The appropriate field and analytical procedures are selected as described in Guide D4043.1.4 Limitations—The limitations of this test method are primarily related to the correspondence between the field situation determined by this test method and the simplifying assumptions of the analytical Test Methods D4105/D4105M or D4106 and D4043.1.5 Units—The values stated in SI units are to be regarded as standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.6.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.1.7 This test method offers a set of instructions for performing one or more operations. This document cannot replace education or experience and should be used in conjunction with professional judgement. Not all aspects of this standard may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a projects many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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