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5.1 Advanced ceramics usually display a linear stress-strain behavior to failure. Lack of ductility combined with flaws that have various sizes and orientations typically leads to large scatter in failure strength. Strength is not a deterministic property, but instead reflects the intrinsic fracture toughness and a distribution (size and orientation) of flaws present in the material. This standard is applicable to brittle monolithic ceramics which fail as a result of catastrophic propagation of flaws. Possible rising R-curve effects are also not considered, but are inherently incorporated into the strength measurements.5.2 Two- and three-parameter formulations exist for the Weibull distribution. This standard is restricted to the two-parameter formulation.5.3 Tensile and flexural test specimens are the most commonly used test configurations for advanced ceramics. Ring-on-ring and pressure-on-ring test specimens which have multi-axial states of stress are also included. Closed-form solutions for the effective volume and effective surfaces and the Weibull material scale factor are included for these configurations. This practice also incorporates size-scaling methods for C-ring test specimens for which numerical approaches are necessary. A generic approach for arbitrary shaped test specimens or components that utilizes finite element analyses is presented in Annex A3.5.4 The fracture origins of failed test specimens can be determined using fractographic analysis. The spatial distribution of these strength-controlling flaws can be over a volume or an area (as in the case of surface flaws). This standard allows for the conversion of strength parameters associated with either type of spatial distribution. Length scaling for strength-controlling flaws located along edges of a test specimen is not covered in this practice.5.5 The scaling of strength with size in accordance with the Weibull model is based on several key assumptions (5). It is assumed that the same specific flaw type controls strength in the various specimen configurations. It is assumed that the material is uniform, homogeneous, and isotropic. If the material is a composite, it is assumed that the composite phases are sufficiently small that the structure behaves on an engineering scale as a homogeneous and isotropic body. The composite must contain a sufficient quantity of uniformly distributed, randomly oriented reinforcing elements such that the material is effectively homogeneous. Whisker-toughened ceramic composites may be representative of this type of material. This practice is also applicable to composite ceramics that do not exhibit any appreciable bilinear or nonlinear deformation behavior. This standard and the conventional Weibull strength scaling with size may not be suitable for continuous fiber-reinforced composite ceramics. The material is assumed to fracture in a brittle fashion, a consequence of stress causing catastrophic propagation of flaws. The material is assumed to be consistent (batch to batch, day to day, etc.). It is assumed that the strength distribution follows a Weibull two-parameter distribution. It is assumed that each test piece has a statistically significant number of flaws and that they are randomly distributed. It is assumed that the flaws are small relative to the specimen cross section size. If multiple flaw types are present and control strength, then strengths may scale differently for each flaw type. Consult Practice C1239 and the example in 9.1 for further guidance on how to apply censored statistics in such cases. It is also assumed that the specimen stress state and the maximum stress are accurately determined. It is assumed that the actual data from a set of fractured specimens are accurate and precise. (See Terminology E456 for definitions of the latter two terms.) For this reason, this standard frequently references other ASTM standard test methods and practices which are known to be reliable in this respect.5.6 Even if test data has been accurately and precisely measured, it should be recognized that the Weibull parameters determined from test data are in fact estimates. The estimates can vary from the actual (population) material strength parameters. Consult Practice C1239 for further guidance on the confidence bounds of Weibull parameter estimates based on test data for a finite sample size of test fractures.5.7 When correlating strength parameters from test data from one specimen geometry to a second, the accuracy of the correlation depends upon whether the assumptions listed in 5.5 are met. In addition, statistical sampling effects as discussed in 5.6 may also contribute to variations between computed and observed strength-size scaling trends.5.8 There are practical limits to Weibull strength scaling that should be considered. For example, it is implicitly assumed in the Weibull model that flaws are small relative to the specimen size. Pores that are 50 μm (0.050 mm) in diameter are volume-distributed flaws in tension or flexural strength specimens with 5 mm or greater cross section sizes. The same may not be true if the cross section size is only 100 μm.1.1 This standard practice provides methodology to convert fracture strength parameters (primarily the mean strength and the Weibull characteristic strength) estimated from data obtained with one test geometry to strength parameters representing other test geometries. This practice addresses uniaxial strength data as well as some biaxial strength data. It may also be used for more complex geometries proved that the effective areas and effective volumes can be estimated. It is for the evaluation of Weibull probability distribution parameters for advanced ceramics that fail in a brittle fashion. Fig. 1 shows the typical variation of strength with size. The larger the specimen or component, the weaker it is likely to be.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5.1 The values stated in SI units are in accordance with IEEE/ASTM SI 10.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose strength is 50 MPa (~7 ksi) or greater. The test method may also be used with glass test specimens, although Test Methods C158 is specifically designed to be used for glasses. This test method may be used with machined, drawn, extruded, and as-fired round specimens. This test method may be used with specimens that have elliptical cross section geometries.4.2 The flexure strength is computed based on simple beam theory with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the rod diameter. The homogeneity and isotropy assumptions in the standard rule out the use of this test for continuous fiber-reinforced ceramics.4.3 Flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the loading rate, test environment, specimen size, specimen preparation, and test fixtures (1-3).3 This method includes specific specimen-fixture size combinations, but permits alternative configurations within specified limits. These combinations were chosen to be practical, to minimize experimental error, and permit easy comparison of cylindrical rod strengths with data for other configurations. Equations for the Weibull effective volume and Weibull effective surface are included.4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws in the material. Flaws in rods may be intrinsically volume-distributed throughout the bulk. Some of these flaws by chance may be located at or near the outer surface. Flaws may alternatively be intrinsically surface-distributed with all flaws located on the outer specimen surface. Grinding cracks fit the latter category. Variations in the flaws cause a natural scatter in strengths for a set of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this standard, is highly recommended for all purposes, especially if the data will be used for design as discussed in Refs (3-5) and Practices C1322 and C1239.4.5 The three-point test configuration exposes only a very small portion of the specimen to the maximum stress. Therefore, three-point flexural strengths are likely to be greater than four-point flexural strengths. Three-point flexure has some advantages. It uses simpler test fixtures, it is easier to adapt to high temperature and fracture toughness testing, and it is sometimes helpful in Weibull statistical studies. It also uses smaller force to break a specimen. It is also convenient for very short, stubby specimens which would be difficult to test in four-point loading. Nevertheless, four-point flexure is preferred and recommended for most characterization purposes.1.1 This test method is for the determination of flexural strength of rod-shaped specimens of advanced ceramic materials at ambient temperature. In many instances it is preferable to test round specimens rather than rectangular bend specimens, especially if the material is fabricated in rod form. This method permits testing of machined, drawn, or as-fired rod-shaped specimens. It allows some latitude in the rod sizes and cross section shape uniformity. Rod diameters between 1.5 and 8 mm and lengths from 25 to 85 mm are recommended, but other sizes are permitted. Four-point-1/4-point as shown in Fig. 1 is the preferred testing configuration. Three-point loading is permitted. This method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.FIG. 1 Four-Point-1/4-Point Flexure Loading Configuration1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose strength is 50 MPa (~7 ksi) or greater.4.2 The flexure stress is computed based on simple beam theory with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the beam thickness. The homogeneity and isotropy assumption in the standard rule out the use of this test for continuous fiber-reinforced ceramics.4.3 Flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the loading rate, test environment, specimen size, specimen preparation, and test fixtures. Specimen sizes and fixtures were chosen to provide a balance between practical configurations and resulting errors, as discussed in MIL-STD-1942(MR) and Refs (1, 2).4 Specific fixture and specimen configurations were designated in order to permit ready comparison of data without the need for Weibull-size scaling.4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws. Variations in these cause a natural scatter in test results for a sample of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this standard, is highly recommended for all purposes, especially if the data will be used for design as discussed in MIL-STD-1942(MR) and Refs (2-5) and Practices C1322 and C1239.4.5 The three-point test configuration exposes only a very small portion of the specimen to the maximum stress. Therefore, three-point flexural strengths are likely to be much greater than four-point flexural strengths. Three-point flexure has some advantages. It uses simpler test fixtures, it is easier to adapt to high temperature and fracture toughness testing, and it is sometimes helpful in Weibull statistical studies. However, four-point flexure is preferred and recommended for most characterization purposes.4.6 This method determines the flexural strength at ambient temperature and environmental conditions. The flexural strength under ambient conditions may or may not necessarily be the inert flexural strength.NOTE 7: time dependent effects may be minimized through the use of inert testing atmosphere such as dry nitrogen gas, oil, or vacuum. Alternatively, testing rates faster than specified in this standard may be used. Oxide ceramics, glasses, and ceramics containing boundary phase glass are susceptible to slow crack growth even at room temperature. Water, either in the form of liquid or as humidity in air, can have a significant effect, even at the rates specified in this standard. On the other hand, many ceramics such as boron carbide, silicon carbide, aluminum nitride, and many silicon nitrides have no sensitivity to slow crack growth at room temperature and the flexural strength in laboratory ambient conditions is the inert flexural strength.1.1 This test method covers the determination of flexural strength of advanced ceramic materials at ambient temperature. Four-point-1/4-point and three-point loadings with prescribed spans are the standard as shown in Fig. 1. Rectangular specimens of prescribed cross-section sizes are used with specified features in prescribed specimen-fixture combinations. Test specimens may be 3 by 4 by 45 to 50 mm in size that are tested on 40-mm outer span four-point or three-point fixtures. Alternatively, test specimens and fixture spans half or twice these sizes may be used. The method permits testing of machined or as-fired test specimens. Several options for machining preparation are included: application matched machining, customary procedure, or a specified standard procedure. This method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The test method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Fracture toughness, KIc, is a measure of the resistance to crack extension in a brittle material. These test methods may be used for material development, material comparison, quality assessment, and characterization.5.2 The pb and the vb fracture toughness values provide information on the fracture resistance of advanced ceramics containing large sharp cracks, while the sc fracture toughness value provides this information for small cracks comparable in size to natural fracture sources. Cracks of different sizes may be used for the sc method. If the fracture toughness values vary as a function of the crack size it can be expected that KIsc will differ from KIpb and KIvb. Table 1 tabulates advantages, disadvantages, and applicability of each method.1.1 These test methods cover the fracture toughness, KIc, determination of advanced ceramics at ambient temperature. The methods determine KIpb (precracked beam test specimen), KIsc (surface crack in flexure), and KIvb (chevron-notched beam test specimen). The fracture toughness values are determined using beam test specimens with a sharp crack. The crack is either a straight-through crack formed via bridge flexure (pb), or a semi-elliptical surface crack formed via Knoop indentation (sc), or it is formed and propagated in a chevron notch (vb), as shown in Fig. 1.1.6 Values expressed in these test methods are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The dynamic interaction between the athlete and the synthetic turf surface affects the comfort and the performance of the athlete. Interaction with a surface that has low amounts of deformation and shock absorption allows the player to run fast and turn quickly, but has the potential to cause discomfort and damage to the lower extremity joints. Synthetic turf surfaces having high deformation have lower energy restitution. Less of the energy exerted by the athlete returns from the surface, possibly increasing the fatigue for the performing athlete.1.1 This test method specifies a method for measuring force reduction, vertical deformation, and energy restitution of synthetic turf surfaces.1.2 This method is used to characterize properties of synthetic turf systems including the turf fabric, infill material, and shock pad (if applicable).1.3 It can be used for characterizing synthetic turf systems in laboratory environment or in the field.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.4.2 Generally, resistance to compression is the measure of the greatest strength of a monolithic advanced ceramic. Ideally, ceramics should be compressively stressed in use, although engineering applications may frequently introduce tensile stresses in the component. Nonetheless, compressive behavior is an important aspect of mechanical properties and performance. Although tensile strength distributions of ceramics are probabilistic and can be described by a weakest-link failure theory, such descriptions have been shown to be inapplicable to compressive strength distributions in at least one study (1).3 However, the need to test a statistically significant number of compressive test specimens is not obviated. Therefore, a sufficient number of test specimens at each testing condition is required for statistical analysis and design.4.3 Compression tests provide information on the strength and deformation of materials under uniaxial compressive stresses. Uniform stress states are required to effectively evaluate any nonlinear stress-strain behavior which may develop as the result of cumulative damage processes (for example, microcracking) which may be influenced by testing mode, testing rate, processing or compositional effects, microstructure, or environmental influences.4.4 The results of compression tests of test specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the strength and deformation properties in the entire full-size product or its in-service behavior in different environments.4.5 For quality control purposes, results derived from standardized compressive test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.1.1 This test method covers the determination of compressive strength including stress-strain behavior, under monotonic uniaxial loading of advanced ceramics at ambient temperature. This test method is restricted to specific test specimen geometries. In addition, test specimen fabrication methods, testing modes (force or displacement), testing rates (force rate, stress rate, displacement rate, or strain rate), allowable bending, and data collection and reporting procedures are addressed. Compressive strength as used in this test method refers to the compressive strength obtained under monotonic uniaxial loading. Monotonic loading refers to a test conducted at a constant rate in a continuous fashion, with no reversals from test initiation to final fracture.1.2 This test method is intended primarily for use with advanced ceramics that macroscopically exhibit isotropic, homogeneous, continuous behavior. While this test method is intended for use on monolithic advanced ceramics, certain whisker- or particle-reinforced composite ceramics, as well as certain discontinuous fiber-reinforced composite ceramics, may also meet these macroscopic behavior assumptions. Generally, continuous fiber ceramic composites (CFCCs) do not macroscopically exhibit isotropic, homogeneous, continuous behavior and, application of this test method to these materials is not recommended.1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Continuous fiber-reinforced ceramic composites are candidate materials for structural applications requiring high degrees of wear, erosion, corrosion resistance, and damage tolerance at high temperatures.5.2 The 1D and 2D CFCCs are highly anisotropic and their transthickness tensile and interlaminar shear strength are lower than their in-plane tensile and in-plane shear strength, respectively.5.3 Shear tests provide information on the strength and deformation of materials under shear stresses.5.4 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.5.5 For quality control purposes, results derived from standardized shear test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.1.1 This test method addresses the uniaxial compression of a double-notched test specimen to determine interlaminar shear strength of continuous fiber-reinforced ceramic composites (CFCCs) at elevated temperatures. Failure of the test specimen occurs by interlaminar shear between two centrally located notches machined halfway through the thickness of the test specimen and spaced a fixed distance apart on opposing faces (see Fig. 1). Test specimen preparation methods and requirements, testing modes (force or displacement control), testing rates (force rate or displacement rate), data collection, and reporting procedures are addressed.FIG. 1 Schematic of Uniaxial Compression of Double-Notched Test Specimen for the Determination of Interlaminar Shear Strength of CFCCs1.2 This test method is used for testing advanced ceramic or glass matrix composites with continuous fiber reinforcement having a laminated structure such as in unidirectional (1D) or bidirectional (2D) fiber architecture (lay-ups of unidirectional plies or stacked fabric). This test method does not address composites with nonlaminated structures, such as (3D) fiber architecture or discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics.1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are noted in 8.1 and 8.2.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This guide is a compilation of standards intended to provide assistance in selecting appropriate nondestructive examination for advanced ceramics, and in turn, to provide guidance for performing the examination, as well as ensuring the proper performance of the equipment. 1.1 This guide identifies and describes standard procedures and methods for nondestructive testing of advanced ceramics using radiology, ultrasonics, liquid penetrants, and acoustic emission. 1.2 This guide identifies existing standards for nondestructive testing that have been determined to be (or have been modified to be) applicable to the examination of advanced ceramics. These standards have been generated by, and are under the jurisdiction of, ASTM Committee E07 on Nondestructive Testing. Selection and application of these standards to be followed must be governed by experience and the specific requirements in each individual case, together with agreement between producer and user. 1.3 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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