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This practice establishes the standard procedures (including apparatus, reagents, and materials to be used) for taking samples of airborne particulate matter in a specific area in the aerospace industry, commonly called the cleanroom, where aerospace fluids are handled. This practiced is based on the impingement of particles on a filter membrane using a vacuum technique. The number of air samples required in a given area will depend on the geometric floor area, the disturbance to the uninterrupted airflow pattern, and the room volume.1.1 This practice covers a procedure for sampling airborne particulate matter larger than 5 m in size. The method is designed to be used in specific areas, commonly called cleanrooms in the aerospace industry, where aerospace fluids are handled.Note 1Practice F 50 is an alternative procedure.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method has the advantage of extreme simplicity. It is a crude and non-specific test method, but it is useful in the study of long-term trends. It requires very little investment in equipment and can be carried out without a large technically-skilled staff.5.2 This test method is useful for obtaining samples of settleable particulate matter for further chemical analysis (1).41.1 This test method covers a procedure for collection of dustfall and its measurement. This test method is not appropriate for determination of the dustfall rate in small areas affected by specific sources. This test method describes determination of both water-soluble and insoluble particulate matter.1.2 This test method is inappropriate for industrial hygiene use except where other more specific methods are also used.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method provides a means of automatically separating and collecting atmospheric particulate and acidic gaseous fluoride samples.5.2 Since the samples are collected on dry tapes, the samples are in a form which allows elution of the fluoride content with a small volume of eluent. Consequently, the method allows analyses of air samples taken for a time period as short as several minutes.1.1 This test method describes the automatic separation and collection on chemically treated paper tapes of particulate and gaseous forms of acidic fluorides in the atmosphere by means of a double paper tape sampler. The sampler may be programmed to collect and store individual air samples obtained over time periods from several minutes to 3 h. A 30.5-m (100-ft) tape will allow unattended operation for the automatic collection of up to 600 samples.1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are included for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Sources of particulate and water-soluble gaseous fluorides in the atmosphere include the fertilizers, aluminum reduction plants, phosphate processors, steel mills, coal burning operations, brick and tile manufacturers, and various less significant sources (5). Gaseous fluorides can cause adverse effects when ingested or inhaled by animals or humans, or absorbed by plants. The procedures documented in this test method provide a means of determining of particulate and water soluble gaseous fluoride in atmospheres.5.2 This test method provides a means of separation and collection of particulate and water soluble gaseous fluoride and provides samples that are convenient to analyze.1.1 This test method provides a procedure for separation and collection of particulate and water-soluble gaseous fluorides from the atmosphere on a chemically treated filter and in an impinger. The sampling rate may vary from 30  L/min (1.0 ft3/min) to 15 L/min (0.5 ft3/min) for longer sampling periods depending on the atmospheric fluoride concentration. This test method is not intended to be applied to gaseous fluorine compounds that are not water-soluble.1.2 There are several limitations of the test method:1.2.1 Although the acid-treated, medium retentive, prefilter has been shown to allow passage of HF, it restricts passage of particulate matter only as small as about 1 μm. Thus, smaller particulate matter may pass through the filter and be collected in or pass through the impingers.1.2.2 The maximum sample volume to be taken using this test method prior to changing the acid-treated prefilter is recommended as 12 m3. This recommendation is made to minimize any effects due to particulate matter build-up.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 7.4.3.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The sodium bicarbonate coated tube filter method provides a means of separating and collecting atmospheric gaseous fluoride and particulate fluoride samples.5.2 Since the samples are collected on the dry tube and filter, the fluoride may be eluted with a small volume of eluant (see Section 10 for specific instructions on fluoride elution). Elution into a small volume and the sensitivity of the analytical methods employed allow the analysis of the collected fluoride to fractional parts of a microgram per cubic metre on samples taken for a 12-h period.1.1 The sodium bicarbonate-coated glass tube and membrane filter method provides a means for the separation and collection of gaseous atmospheric forms of fluoride reactive with sodium bicarbonate and particulate forms of fluoride which are collected by a filter. The test method is applicable to 12-h sampling periods, collecting 1 to 500 μg of gaseous fluoride at a 15 L/min (0.5 ft3/min) sampling rate or about 0.1 to 50 μg/m3. The length of the sampling period can therefore be adjusted so that the amount of fluoride collected will fall within this range. The actual lower limit of the test method will depend upon the sensitivity of the analytical method employed and the quality of reagents used in tube preparation and analysis. It is recommended that the lower limit of detection should be considered as two times the standard deviation of the monthly arithmetic mean blank value. Any values greater than the blank by less than this amount should be reported as “blank value.”1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 In this test method, the amount of particulate generated into the air by operating a vacuum cleaner over a specific floor covering that is contaminated with dust will be determined. Particles from the motor, floor covering, and the test dust will all be measured. The amount of dust generated in the laboratory practice will differ from that in residential/commercial installations because of variations in floor coverings, soil and other solid particulate compositions, the vacuuming process used by individual operators, the air exchange rate of heating, ventilation, and air conditioning (HVAC) systems, and other factors.4.2 To provide a uniform basis for measuring the performance in 4.1, a standardized test chamber, equipment, floor covering material, and dust particulate are used in this test method.4.3 Due to the large range of generated particle counts observed among products in the vacuum cleaner industry at the present time, the test results of the maximum particle counts generated under this test method are expressed in Log10 equivalents for evaluation and comparison of product performance.1.1 This test method provides a laboratory test for the measurement of particulate generated as a direct result of the vacuuming process.1.2 This test method is applicable to all residential/commercial uprights, canisters, stickvacs, central vacuum systems, and combination cleaners.1.3 This test method applies to test dust removal from floor coverings not the removal of surface litter and debris.1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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