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1.1 This practice describes the operation and production control of metal powder bed fusion (PBF) machines and processes to meet critical applications such as commercial aerospace components and medical implants. The requirements contained herein are applicable for production components and mechanical test specimens using powder bed fusion (PBF) with both laser and electron beams.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The test can be used to evaluate the following:5.1.1 Classification or Comparison of Powders—There are several parameters that can be used to classify powders relative to each other, the most useful being the measured shear stresses, cohesion, flow function and angle of internal friction.5.1.2 Sensitivity Analysis—The shear cell can be used to evaluate the relative effects of a range of powder properties and/or environmental parameters such as (but not limited to) humidity, particle size and size distribution, particle shape and shape distribution, moisture content and temperature.5.1.3 Quality Control—The test can, in some circumstances, be used to assess the flow properties of a raw material, intermediate or product against pre-determined acceptance criteria.5.1.4 Storage Vessel Design—Mathematical models exist for the determination of storage vessel design parameters which are based on the flow properties of powders as generated by shear cell testing, requiring shear testing at a range of consolidating stresses as well as the measurement of the wall friction angle with respect to the material of construction of the storage vessel. The methods are detailed in Refs. (1-3).2NOTE 1: The quality of the result produced by this test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this test method are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors (4).Practice D3740 was developed for agencies engaged in the testing and/or inspection of soil and rock. As such it is not totally applicable to agencies performing this test method. However, users of this test method should recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this practice. Currently there is no known qualifying national authority that inspects agencies that perform this test method.1.1 This method covers the apparatus and procedures for measuring the incipient failure properties of a powder as a function of the normal stress for a given level of consolidation. The method also allows the further determination of the unconfined yield strength, internal friction angles, cohesion, flow function, major principal stress and wall friction angle (with the appropriate wall coupon fitted to the correct accessory).1.2 These parameters are most commonly used for the design of storage hoppers and bins using industry standard calculations and procedures. They can also provide relative classification or comparison of the flow behavior of different powders or different batches of the same powder if similar stress and shear regimes are encountered within the processing equipment.1.3 The apparatus is suitable for measuring the properties of powders with a maximum particle size of 1 mm. It is possible to test powders which have a small proportion of particles of 1 mm or greater, but they should be present in the bulk sample as no more than 5 % of the total mass in samples with a normal (Gaussian) size distribution.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.4.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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This document specifies the features of laser-based powder bed fusion of metals (PBF-LB/M) and provides detailed design recommendations.Some of the fundamental principles are also applicable to other additive manufacturing (AM) processes, provided that due consideration is given to the process-specific features.This document also provides a state of the art review of design guidelines associated with the use of powder bed fusion (PBF) by bringing together relevant knowledge about this process and by extending the scope of ISO/ASTM 52910.

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This document specifies the features of laser-based powder bed fusion of polymers (LB-PBF-P) and provides detailed design recommendations. Some of the fundamental principles are also applicable to other additive manufacturing (AM) processes, provided that due consideration is given to process-specific features. This document also provides a state-of-the-art review of design guidelines associated with the use of powder bed fusion (PBF) by bringing together relevant knowledge about this process and by extending the scope of ISO/ASTM 52910.

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5.1 The ability of sintered powder metallurgy stainless steel parts/specimens to resist corrosion when immersed in sodium chloride solution is important to their end use. Causes of unacceptable corrosion may be incorrect alloy, contamination of the parts by iron or some other corrosion-promoting material or improper sintering of the parts (for example, undesirable carbide and nitride formations caused by poor lubricant burnoff or improper sintering atmosphere).5.2 This standard may be part of a purchase agreement between the PM parts producer and the purchaser of the parts (Method 1). It may also be used to optimize part or specimen production parameters (Method 2).1.1 These test methods cover a procedure for evaluating the ability of sintered PM stainless steel parts/specimens to resist corrosion when immersed in a sodium chloride (NaCl) solution.1.2 Corrosion resistance is evaluated by one of two methods. In Method 1, the stainless steel parts/specimens are examined periodically and the time to the first appearance of staining or rust is used to indicate the end point. In Method 2, continued exposure to the sodium chloride solution is used to monitor the extent of corrosion as a function of time.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 A major factor affecting the life of insulating materials is thermal degradation. It is possible that other factors, such as moisture and vibration, will cause failures after the material has been weakened by thermal degradation.5.2 Electrical insulation is effective in electrical equipment only as long as it retains its physical and electrical integrity. The following are potential indicators of thermal degradation: weight change, porosity, crazing, and generally a reduction in flexibility. Thermal degradation is usually accompanied by an ultimate reduction in dielectric breakdown.5.3 This test method is useful in determining the thermal endurance of coating powders applied over a steel substrate material.1.1 This test method provides a procedure for evaluating thermal endurance of coating powders by determining the length of aging time at selected elevated temperatures required to achieve dielectric breakdown at room temperature at a pre-determined proof voltage. Thermal endurance is expressed in terms of a temperature index.1.2 This test method is applicable to insulating powders used over a substrate material of steel.1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems is likely to result in non-conformance with the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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