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10.1 Full-scale bending testing is an effective way to determine flexural properties of structural glued laminated timber (glulam) beams. However, testing of large glulam members is cost prohibitive. Mathematical models, when confirmed by full-scale test results, are useful tools to assign flexural properties for glulam. This practice provides guidelines for sampling and testing full-scale glulam beams to determine their flexural properties and to validate mathematical models intended for use in assigning flexural design values.1.1 This practice describes procedures for full scale testing of structural glued laminated timber (glulam) to determine or verify characteristic values used to calculate flexural design properties. Guidelines are given for: (1) testing individual structural glued laminated timber lay-ups (with no modeling), (2) testing individual glulam combinations (with limited modeling), and (3) validating models used to predict characteristic values.1.2 This practice is limited to procedures for establishing flexural properties (Modulus of Rupture, MOR, and Modulus of Elasticity, MOE). Some of the principles for sampling and analysis presented may be applicable to other properties. However, other properties may require additional testing considerations that are beyond the scope of this practice.1.3 This practice is not intended to supersede the provisions of Practice D3737, but provides an alternative method for establishing characteristic values. Lay-up combinations developed in accordance with Practice D3737 are not required to be governed by this standard.NOTE 1: The models described by Practice D3737 have been developed and modified based on more than 50 years of experience and many test programs. In some cases, however, it may be desirable to develop a new model based on other input properties or using lumber materials or grades not covered by that standard.1.4 Details of production, inspection, and certification are beyond the scope of this document. However, for test results to be representative of production, quality control systems shall be in place to ensure consistent quality. Manufacturing shall conform to recognized manufacturing standards such as ANSI A190.1 or CSA O122.1.5 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This practice presents the two standard methods for determining the strength values of clear wood of different species in the unseasoned condition, unadjusted for end use, applicable to the establishment of working stresses for different solid wood products such as lumber, laminated wood, plywood, and round timbers. Method A provides for the use of the results of surveys of wood density involving extensive sampling of forest trees, in combination with the data obtained from standard strength tests. The average strength properties are obtained from wood density survey data through linear regression equations establishing the relation of specific gravity to the several strength properties. Method B, on the other hand, provides for the establishment of tables of strength values based on standard tests of small clear specimens in the unseasoned condition for use when data from density surveys are not available. Separate tables are employed to present the data on woods grown in the United States and on woods grown in Canada. Guidelines for the interpretation of the data in terms of assigned values, information basic to the translation of the clear wood values into working stresses, presently available data with appropriate provisions for their application and use, and methods for estimating some useful mechanical properties by relating them to other properties are presented herein as well.1.1 This practice covers the determination of strength values for clear wood of different species in the unseasoned condition, unadjusted for end use, applicable to the establishment of design values for different solid wood products such as lumber, laminated wood, plywood, and round timbers. Presented are:1.1.1 Procedures by which test values obtained on small clear specimens may be combined with density data from extensive forest surveys to make them more representative,1.1.2 Guidelines for the interpretation of the data in terms of assigned values for combinations of species or regional divisions within a species to meet special marketing needs, and1.1.3 Information basic to the translation of the clear wood values into design values for different solid wood products for different end uses.1.1.4 For species where density survey data are not as yet available for the re-evaluation of average strength properties, the presently available data from tests made under the sampling methods and procedures of Test Methods D143 or Practice E105 are provided with appropriate provision for their application and use. Because of the comprehensive manner in which the density survey is undertaken, it follows that the re-evaluated strength data are intended to be representative of the forest stand, or rather large forest subdivisions.1.1.5 Some useful mechanical properties (tensile strengths parallel and perpendicular to grain, modulus of rigidity for a longitudinal-transverse plane, and transverse modulus of elasticity) have not been extensively evaluated. Methods are described for estimating these properties by their relation to other properties.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Precision statements for calculated values can be developed using this approach. Users can also evaluate how an individual test method’s precision influences the variability of calculated values.4.2 The standard deviation of a calculated value that is the sum, difference, product, or quotient of two or more test method results, each with their own precision statement, can be calculated so long as the individual variables (that is, test results) are independent and the standard deviations are small relative to their mean values. These restrictions are usually met in ASTM methods. In those cases where these restrictions are not met, other methods can be used. Only cases complying with the restrictions are covered in this standard.1.1 Material and mixture properties such as air voids and voids in mineral aggregates (VMA) are calculated from two or three test results, combined in simple mathematical relationships. The standard deviation equations for these calculated values can be developed using a mathematical process called “propagation of errors” (also called “propagation of uncertainty”). This practice includes uncertainty equations for four forms or material and mixture equations: when two test results are (1) added or subtracted, (2) multiplied together, (3) one divided by the other, and (4) two test results divided by a third.1.2 This approach to calculating standard deviation equations is only valid when the distributions of the test results from the two standards are independent (that is, not correlated).1.3 The accuracy of a calculated standard deviation is dependent on the accuracy of the standard deviations used for the individual test result methods.1.4 Values for the mean and standard deviation for each test method are needed to determine the standard deviation for a calculated value.1.5 Examples of how to use these equations are shown in Appendix X1.1.6 A brief explanation of how standard deviation equations are derived for more complicated material and mixture equations is also included.1.7 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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AbstractThese alternative test methods cover the indicator procedure for determining the total, primary, secondary, and tertiary amine values of fatty amines. These procedures are not applicable to fatty amidoamines and fatty diamines. The apparatus includes Erlenmeyer flasks and magnetic stirrer. Reagent grade chemicals shall be used in all tests and includes the following: water, bromphenol blue indicator solution, bromcresol green indicator solution, chloroform, hydrochloric acid standard solution, isopropyl alcohol, phenyl isothiocyanate, and salicylaldehyde. The procedure of determining the total amine values are detailed and the formula of calculating the total amine values is given.1.1 These alternative test methods cover the indicator procedure for determining the total, primary, secondary, and tertiary amine values of fatty amines. These procedures are not applicable to fatty amidoamines and fatty diamines.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The spontaneous heating value of a substance is a measure of the ability of that substance to undergo self-heating reactions while supported by cellulosic or other fibrous material in air. It is an index of the autoignition tendency of the substance under such conditions.1.1 This test method covers the non-adiabatic determination of the spontaneous heating values (SHV) of liquids and solids. It is applicable to substances that are not completely volatile at the test temperature. Spontaneous heating values obtained by this test method are qualitative indications of the degree of self-heating that may be expected to occur upon exposure of the sample to air at the test temperature.1.2 Values obtained by this method are applicable to liquids and solids supported on cellulosic surfaces. They are not applicable to liquids on metal surfaces, on contaminated surfaces, or at pressures above atmospheric.1.3 Spontaneous heating values determined by the present test method are regarded only as qualitative measurements of self-heating which occurs under the conditions of the test. The test method does not purport to produce a quantitative measure of the enthalpy of reaction of the sample with air at a given test temperature. Such data can be obtained by the use of an adiabatic calorimeter. The existence, under the test conditions, of a positive temperature difference between the sample and the reference is evidence of a thermochemical reaction in the sample.1.4 The magnitude of the measured temperature difference is a semiquantitative indication of the enthalpy and rate of that reaction. Since factors such as heat loss from the sample to the bath and quenching of the reaction due to too rapid consumption of oxygen affect the amount and duration of the measured heat effect, care must be taken not to attribute too much quantitative significance to the test results. It is sufficient, for the purpose of this test, to determine whether or not the sample is capable of undergoing a self-heating reaction of sufficient magnitude and rapidity to produce a detectable thermal effect. The spontaneous heating value (SHV) can be lower than the test temperature. A negative result does not preclude spontaneous heating initiating at a temperature higher than the test temperature.1.5 This standard should be used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions and should not be used to describe or appraise the fire-hazard or fire-risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire-hazard assessment or a fire-risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard or fire risk of a particular end use.1.6 The values stated in SI units are to be regarded as the standard. In cases where materials, products or equipment are available in inch-pound units only, SI units are omitted.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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