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ASTM D4220/D4220M-14 Standard Practices for Preserving and Transporting Soil Samples (Withdrawn 2023) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

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5.1 This standard classifies soils from any geographic location into categories representing the results of prescribed laboratory tests to determine the particle-size characteristics, the liquid limit, and the plasticity index.5.2 The assigning of a group name and symbol(s) along with the descriptive information required in Practice D2488 can be used to describe a soil to aid in the evaluation of its significant properties for engineering use.5.3 The various groupings of this classification system have been devised to correlate in a general way with the engineering behavior of soils. This standard provides a useful first step in any field or laboratory investigation for geotechnical engineering purposes.5.4 This standard may also be used as an aid in training personnel in the use of Practice D2488.5.5 This standard may be used in combination with Practice D4083 when working with frozen soils.NOTE 5: Notwithstanding the statements on precision and bias contained in this standard: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this test method are cautioned that compliance with Practice D3740 does not in itself assure reliable testing. Reliable testing depends on several factors; Practice D3740 provides a means for evaluating some of those factors.1.1 This practice describes a system for classifying mineral and organo-mineral soils for engineering purposes based on laboratory determination of particle-size characteristics, liquid limit, and plasticity index and shall be used when precise classification is required.NOTE 1: Use of this standard will result in a single classification group symbol and group name except when a soil contains 5 to 12 % fines or when the plot of the liquid limit and plasticity index values falls into the crosshatched area of the plasticity chart. In these two cases, a dual symbol is used, for example, GP-GM, CL-ML. When the laboratory test results indicate that the soil is close to another soil classification group, the borderline condition can be indicated with two symbols separated by a slash. The first symbol should be the one based on this standard, for example, CL/CH, GM/SM, SC/CL. Borderline symbols are particularly useful when the liquid limit value of clayey soils is close to 50. These soils can have expansive characteristics and the use of a borderline symbol (CL/CH, CH/CL) will alert the user of the assigned classifications of expansive potential.1.2 The group symbol portion of this system is based on laboratory tests performed on the portion of a soil sample passing the 3-in. (75-mm) sieve (see Specification E11).1.3 As a classification system, this standard is limited to naturally occurring soils.NOTE 2: The group names and symbols used in this test method may be used as a descriptive system applied to such materials as shale, claystone, shells, crushed rock, etc. See Appendix X2.1.4 This standard is for qualitative application only.NOTE 3: When quantitative information is required for detailed designs of important structures, this test method must be supplemented by laboratory tests or other quantitative data to determine performance characteristics under expected field conditions.1.5 This standard is the ASTM version of the Unified Soil Classification System. The basis for the classification scheme is the Airfield Classification System developed by A. Casagrande in the early 1940s.2 It became known as the Unified Soil Classification System when several U.S. Government Agencies adopted a modified version of the Airfield System in 1952.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This practice offers a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Hydraulically operated stationary piston samplers are used to gather soil samples for laboratory or field testing and analysis for geologic investigations, soil chemical composition studies, and water quality investigations. The sampler is sometimes used when attempts to recover unstable soils with thin-walled tubes, Practice D1587/D1587M, are unsuccessful. Examples of a few types of investigations in which hydraulic stationary piston samplers may be used include building site foundation studies containing soft sediments, highway and dam foundation investigations where softer soil formation need evaluation, wetland crossings utilizing floating structures, and hazardous waste site investigations. Hydraulically operated stationary piston samplers provide specimens necessary to determine the physical and chemical composition of soils and, in certain circumstances, contained pore fluids (see Guide D6169/D6169M).5.2 Hydraulically operated stationary piston samplers can provide relatively intact soil samples of soft or loose formation materials for testing to determine accurate information on the physical characteristics of that soil. Samples of soft formation materials can be tested to determine numerous soil characteristics such as; soil stratigraphy, particle size, water content, permeability, shear strength, compressibility, and so forth. The chemical composition of soft formation soils can also be determined from the sample if provisions are made to ensure that clean, decontaminated tools are used in the sample gathering procedure. Field-extruded samples can be field-screened or laboratory-analyzed to determine the chemical composition of soil and contained pore fluids. Using sealed or protected sampling tools, cased boreholes, and proper advancement techniques can help in the acquisition of good representative samples. A general knowledge of subsurface conditions at the site is beneficial.5.3 The use of this practice may not be the correct method for investigations of softer formations in all cases. As with all sampling methods, subsurface conditions affect the performance of the sample gathering equipment and methods used. For example, research indicates that clean sands may undergo volume changes in the sampling process, due to drainage.5 The hydraulically operated stationary piston sampler is generally not effective for cohesive formations with unconfined, undrained shear strength in excess of 2.0 tons per square foot, coarse sands, compact gravelly tills containing boulders and cobbles, compacted gravel, cemented soil, or solid rock. These formations may damage the sample or cause refusal to penetration. A small percentage of gravel or gravel cuttings in the base of the borehole can cause the tube to bend and deform, resulting in sample disturbance. Certain cohesive soils, depending on their water content, can create friction on the thin-walled tube which can exceed the hydraulic delivery force. Some rock formations can weather into soft or loose deposits where the hydraulically operated stationary piston sampler may be functional. The absence of groundwater can affect the performance of this sampling tool, and since this sampling method can introduce water to the borehole, it may not be suitable for sampling above the groundwater table when water is utilized as the activation fluid. As with all sampling and borehole advancement methods, precautions must be taken to prevent cross-contamination of aquifers through migration of contaminates up or down the borehole. Refer to Guide D6286/D6286M on selecting drilling methods for environmental site characterization for additional information about work at hazardous waste sites.NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this practice are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.Practice D3740 was developed for agencies engaged in the laboratory testing and/or inspection of soil and rock. As such, it is not totally applicable to agencies performing this practice. However, user of this practice must recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this practice. Currently, there is no known qualifying national authority that inspects agencies that perform this practice.1.1 This practice covers a procedure for sampling of cohesive, organic, or fine-grained soils, or combination thereof, using a thin-walled metal tube that is inserted into the soil formation by means of a hydraulically operated piston. It is used to collect relatively intact soil samples suitable for laboratory tests to determine structural and chemical properties for geotechnical and environmental site characterizations.1.1.1 Guidance on preservation and transport of samples in accordance with Practice D4220/D4220M may apply. Samples for classification may be preserved using procedures similar to Class A. In most cases, a thin-walled tube sample can be considered as Class B, C, or D. Refer to Guide D6169/D6169M for use of the hydraulically operated stationary piston soil sampler for environmental site characterization. This sampling method is often used in conjunction with rotary drilling methods such as fluid rotary; Guide D5783; and hollow stem augers, Practice D6151/D6151M. Sampling data shall be reported in the field log in accordance with Guide D5434.1.2 The hydraulically operated stationary piston sampler is limited to soils and unconsolidated materials that can be penetrated with the available hydraulic pressure that can be applied without exceeding the structural strength of the thin-walled tube. This standard addresses typical hydraulic piston samplers used on land or shallow water in drill holes. The standard does not address specialized offshore samplers for deep marine applications that may or may not be hydraulically operated. This standard does not address operation of other types of mechanically advanced piston samplers. For information on other soil samplers, refer to Guide D6169/D6169M.1.3 Units—The values stated in either inch-pound units or SI units [presented in brackets] are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of results in units other than shall not be regarded as nonconformance with this standard.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.1.5 This practice does not purport to address all the safety concerns, if any, associated with its use and may involve use of hazardous materials, equipment, and operations. It is the responsibility of the user of this practice to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Also, the user must comply with prevalent regulatory codes, such as OSHA (Occupational Health and Safety Administration) guidelines, while using this practice. For good safety practice, consult applicable OSHA regulations and other safety guides on drilling.21.6 This practice offers a set of instructions for performing one or more specific operations. This practice cannot replace education or experience and should be used in conjunction with professional judgement. Not all aspects of this practice may be applicable in all circumstances. This practice is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “Standard” in the title means only that the document has been approved through the ASTM consensus process. This practice does not purport to comprehensively address all of the methods and potential issues associated with sampling of soil. Users should seek qualified professionals for decisions as to the proper equipment and methods that would be most successful for their site exploration. Other methods may be available for drilling and sampling of soil, and qualified professionals should have flexibility to exercise judgment as to possible alternatives not covered in this practice. The practice is current at the time of issue, but new alternative methods may become available prior to revisions, therefore, users should consult with manufacturers or producers prior to specifying program requirements.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The water content of a soil is used throughout geotechnical engineering practice both in the laboratory and in the field. The use of Test Methods D2216 for water content determination can be time consuming and there are occasions when a more expedient method is desirable. Drying by direct heating is one such method. Results of this test method have been demonstrated to be of satisfactory accuracy for use in field control work, such as in the determination of water content, and in the determination of in-place dry unit weight of soils.5.2 The principal objection to the use of the direct heating for water content determination is the possibility of overheating the soil, thereby yielding a water content higher than would be determined by Test Methods D2216. While not eliminating this possibility, the incremental drying procedure in this test method will minimize its effects. Some heat sources have settings or controls that can also be used to reduce overheating. Loose fitting covers or enclosures can also be used to reduce overheating while assisting in uniform heat distribution.5.3 The behavior of a soil when subjected to direct heating is dependent on its mineralogical composition, and as a result, no one procedure is applicable for all types of soils or heat sources. The general procedure of this test method applies to all soils, but test details may need to be tailored to the soil being tested.5.4 When this test method is to be used repeatedly on the same or similar soil from a given site, a correction factor can usually be determined by making several comparisons between the results of this test method and Test Methods D2216. A correction factor is valid when the difference is consistent for several comparisons, and is reconfirmed on a regular specified basis.5.5 This test method may not be appropriate when precise results are required, or when minor variations in water content will affect the results of other test methods, such as borderline situations where small variations in the measured water content could affect acceptance or rejection.5.6 This test method is not appropriate for specimens known to contain flammable organics or contaminants, and other test methods should be utilized in these situations.NOTE 1: The quality of the results produced by this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection. Users of this test method are cautioned that compliance with Practice D3740 does not in itself ensure reliable results . Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers procedures for determining the water content of soils by drying with direct heat, such as using a hotplate, stove, blowtorch, and the like.1.2 This test method can be used as a substitute for Test Methods D2216 when more rapid results are desired to expedite other phases of testing and slightly less accurate results are acceptable.1.3 When questions of accuracy between this test method and Test Methods D2216 arise, Test Methods D2216 shall be the referee method.1.4 This test method is applicable for most soil types. For some soils, such as those containing significant amounts of halloysite, mica, montmorillonite, gypsum, or other hydrated materials, highly organic soils or soils that contain dissolved solids, (such as salt in the case of marine deposits), this test method may not yield reliable water content values due to the potential for heating above 110°C or lack of means to account for the presence of precipitated solids that were previously dissolved.1.5 The values stated in SI units are to be regarded as standard. Performance of the test method utilizing another system of units shall not be considered non-conformance. The sieve designations are identified using the “standard” system in accordance with Specification E11, such as 2.0-mm and 19-mm, followed by the “alternative” system of No. 10 and 3/4-in., respectively, in parentheses.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in D6026, unless otherwise superseded by this standard.1.6.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.6.2 Significant digits are especially important if the water content will be used to calculate other relationships such as moist mass to dry mass or vice versa, wet unit weight to dry unit weight or vice versa, and total density to dry density or vice versa. For example, if four significant digits are required in any of the above calculations, then the water content has to be recorded to the nearest 0.1 %, for water contents below 100 %. This occurs since 1 plus the water content (not in percent) will have four significant digits regardless of what the value of the water content is (below 100 %); that is, 1 plus 0.1/100 = 1.001, a value with four significant digits. While, if three significant digits are acceptable, then the water content can be recorded to the nearest 1 %.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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4.1 Method A makes use of the same compaction equipment and molds commonly available in soil laboratories and used for other soil-cement tests. It is considered that Method A gives a relative measure of strength rather than a rigorous determination of compressive strength. Because of the lesser height to diameter ratio (1.15) of the cylinders, the compressive strength determined by Method A will normally be greater than that for Method B.4.2 Method B, because of the greater height to diameter ratio (2.00), gives a better measure of compressive strength from a technical viewpoint since it reduces complex stress conditions that may occur during the shearing of Method A specimens.4.3 In practice, Method A has been more commonly used than Method B. As a result, it has been customary to evaluate or specify compressive strength values as determined by Method A. A factor for converting compressive strength values based on height to diameter ratio is given in Section 8.3NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the determination of the compressive strength of soil-cement using molded cylinders as test specimens.1.2 Two alternative procedures are provided as follows:1.2.1 Method A—This procedure uses a test specimen prepared in a mold complying with Test Methods D698 (4.0 in. (101.6 mm) in diameter and 4.6 in. (116.8 mm) in height), sometimes referred to as a proctor mold, resulting in a height over diameter ratio of 1.15. This test method may be used only on materials with 30 % or less retained on the 19.0-mm (3/4-in.) sieve. See Note 2.1.2.2 Method B—This procedure uses a test specimen with a height over diameter ratio of 2.0 prepared in a cylindrical mold in accordance with Practice D1632 (2.8 in. (71.1 mm) in diameter and 9.0 in. (229 mm) in height). This test method is applicable to those materials that pass the 4.75-mm (No. 4) sieve.1.3 Units—The values stated in inch-pound units are to be regarded as standard, except as noted in below. The values given in parentheses are mathematical conversions to SI units, and are provided for information only and are not considered standard. Sieve sizes are identified by the standard designations in Specification E11. The alternative sieve size designation given in parentheses is for information only and does not represent a different standard sieve size.1.3.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs.1.3.2 The slug unit of mass is almost never used in commercial practice, that is, density, balances, etc. Therefore, the standard unit for mass in this standard is either kilogram (kg) or gram (g), or both. Also, the equivalent inch-pound unit (slug) is not given/presented in parentheses.1.3.3 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This implicitly combines two separate systems of units; that is, the absolute system and the gravitational system. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit for mass. However, the use of balances or scales, recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026 unless superseded by this test method.1.4.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is intended for use in the laboratory and as a research tool for determining relative compressive strength values for various soil-cement mixtures. It is not intended as an alternative for Test Method D1633 and the test values obtained by these two test methods are not interchangeable and not necessarily comparable. A comparison of strengths obtained by Test Methods D1633 and D1634 is given by Feld and Abrams.3NOTE 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the determination of the compressive strength of soil-cement, using portions of beams broken in flexure in accordance with Test Method D1635, as test specimens.1.2 Units—The values stated in inch-pound units are to be regarded as standard, except as noted below. The values given in parentheses are mathematical conversions to SI units, which are provided for information only and are not considered standard.1.2.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight) while the unit for mass is slugs.1.2.2 The slug unit of mass is almost never used in commercial practice; that is, density, balances, etc. Therefore, the standard unit for mass in this standard is either kilogram (kg) or gram (g), or both. Also, the equivalent inch-pound unit (slug) is not given/presented in parantheses.1.2.3 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This implicitly combines two separate systems of units; that is, the absolute system and the gravitational system. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit for mass. However the use of balances or scales, recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026 unless superseded by this test method.1.3.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Ultrasonic extraction using dilute nitric acid is a simpler and easier method for extracting lead from environmental samples than are traditional digestion methods that employ hot plate or microwave digestion with concentrated acids (3), (5), (7), (8). Hence, ultrasonic extraction may be used in lieu of the more rigorous strong acid/high temperature digestion methods (for example, see Ref (3) and Test Method E1613), provided that the performance is demonstrated using accepted criteria as delineated in Guide E1775.5.2 In contrast with hot plate or microwave digestion techniques, ultrasonic extraction is field-portable, which allows for on-site sample analysis.1.1 This practice covers an ultrasonic extraction procedure for the extraction of lead from environmental samples of interest in lead abatement and renovation (or related) work, for analytical purposes.1.2 Environmental matrices of concern include dry paint films, settled dusts, soils, and air particulates.1.3 Samples subjected to ultrasonic extraction are prepared for subsequent determination of lead by laboratory analytical methods.1.4 This practice includes, where applicable, descriptions of procedures for sample homogenization and weighing prior to ultrasonic extraction.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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