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5.1 This test method may be used for routine inspection purposes by subjecting a required number of specimens to the test conditions for a specified time and noting the number that fail. The cracking obtained with the test reagent is indicative of what may be expected from a wide variety of surface-active agents, soaps, and organic substances that are not absorbed appreciably by the polymer.5.2 Environmental stress-cracking is a property that is highly dependent upon the nature and level of the stresses applied and on the thermal history of the specimen (1). Under the conditions of the test method, high local multiaxial stresses are developed through the introduction of a controlled imperfection (2, 3). Environmental stress-cracking has been found to occur most readily under such conditions.NOTE 2: Different types of polyethylene plastics as defined in Specification D1248 are generally tested under different levels of strain and stress. When it is expressly desired to compare the types at equal levels of strain, the specimens for all types should be tested under Condition B, Table 1 (4) .(A) Dimensional values are not exactly equivalent. However, for referee purposes the metric units shall apply.(B) For referee purposes, concentration of Igepal will be consistent with the appropriate material standard. If no concentration is given, then 10 % volume solution shall be used.(C) At a temperature of 100°C, a full-strength reagent, rather than an aqueous solution of a reagent, is generally used because solutions tend to change their compositions by water evaporation losses during the period of test.5.3 Information from this test method is not intended to be used for direct application to engineering problems.NOTE 3: Caution should be used in comparing and ranking various ethylene plastics into distinct and separate groups by this test method (see Section 13 and Note 12).As thermal history is recognized as an important variable, test results by this test method employing laboratory molded samples cannot necessarily be expected to show agreement with test results from samples obtained by other means. The true performance potential of a given ethylene plastic may, however, best be determined with specimens obtained from commercially prepared items (5).1.1 This test method covers the determination of the susceptibility of ethylene plastics, as defined in Terminology D883, to environmental stress-cracking when subjected to the conditions herein specified. Under certain conditions of stress and in the presence of environments such as soaps, wetting agents, oils, or detergents, ethylene plastics may exhibit mechanical failure by cracking.1.2 The values stated in SI units are to be regarded as standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: There is no known ISO equivalent to this standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods measure certain chemical and physical properties of ethylene glycols and propylene glycols and may be used to determine compliance with specification in which limits are established for these properties. For those tests that use the procedure of another ASTM test method, that test method should be consulted for additional information on the significance and use of that test.3.2 Alternative test methods and technology for several of the methods can be found in the Appendix. Use of these methods is optional and individuals using the alternative methods should assure themselves that the method is sufficient and appropriate for the application. Precision data presented in this standard is only for the original test methods listed.1.1 These test methods cover the chemical and physical analysis of the commonly available grades of ethylene glycol, diethylene glycol, triethylene glycol, propylene glycol, and dipropylene glycol. The key sections appear in the following order:  Sections Purity of Reagents 4Specific Gravity 6 – 8Distillation Range 10 – 12Acidity 14 – 16Water 18 – 20Iron 22 – 24Color 26 – 28Gas Chromatographic Analysis 30 – 32Alternative Test Methods Appendix X11.2 Review the current appropriate Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.1.3 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard with the exception of foot-pound for apparatus descriptions.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods are intended mainly for referee purposes but may be used for quality control of rubber production. They may also be used in research and development work and for comparison of different rubber samples in a standard formula.3.2 These test methods may be used to obtain values for customer acceptance of rubber.1.1 These test methods specify the standard materials, test formulas, mixing procedures, and test methods for the evaluation and production control of ethylene propylene diene rubbers (EPDM).1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Determination of the percentage of KEE compound in sheet roofing is of concern to many specifiers and building owners. Method A, the faster method, is best used for quality control. Method B may apply better to research and development or investigative work.1.1 This test method pertains to the determination of the relative contents of ketone-ethylene-ester (KEE) and polyvinyl chloride (PVC) after their extraction from reinforced roofing membranes or fabrics. Based on proton nuclear magnetic resonance spectroscopy (1H-NMR), the method allows for the quantification of PVC with respect to an internal standard. The KEE content is then obtained by difference. The test method is not applicable to membranes or blends that contain high molecular weight polymers other than PVC and KEE.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Presence of paper, metal, or incompatible polymer contamination in poly(ethylene terephthalate) renders the recycled polymer unfit for use in secondary product manufacturing operations. This procedure is useful for identifying different types of contamination in recycled PET flakes.1.1 This practice covers an indication of the quality of recycled transparent poly(ethylene terephthalate) by examination of a wafer or plaque formed by melting a representative sample and quenching it to prevent crystallization.1.2 Specific contaminants and impurities such as aluminum particles, dirt particles, paper, and fibers are identified in the transparent wafer. This method is only limited to contamination observable through visual methods. If there are low levels (0–200 ppm) of certain types of contamination, which are transparent and partially/wholly miscible with PET, they will not be apparent through this method.1.3 The overall color of the plaque is indicative of oxidizable contaminants such as ethylene-vinyl acetate (EVA) glue residue and the number of bubbles present in the plaque gives an indication of the moisture content of the sample.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.NOTE 1: There is no known ISO equivalent to this standard.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The absorption coefficient of polyolefin polymer pigmented with carbon black is useful to judge the degree and uniformity of dispersion of the pigment, and the adequacy of the quantitative level of pigment addition. These factors are used to predict the performance of the polymer material in response to prolonged exposure to ultraviolet light as evidenced by minimal changes in specific properties.NOTE 1: This test method was developed to evaluate ethylene polymer materials pigmented with small particle size carbon blacks suitable for UV protection. It is not known how accurate and reproducible the test would be with larger (35 nm or greater) particle size blacks. However, for larger particle sizes of carbon black, such as furnace black at 275 nm, when there is at least 5 or higher percent of carbon black, the material pigmented as such has suitable UV protection.1.1 This test method measures the amount of light transmitted through a film of carbon black pigmented ethylene polymer.1.2 After calculation of the amount of light and film thickness, an absorption coefficient is calculated.1.3 Whenever two sets of values are presented, in different units, the values in the first set are the standard, while those in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D2647-18 Standard Specification for Crosslinkable Ethylene Plastics Historical 发布日期 :  1970-01-01 实施日期 : 

This specification covers a general classification system for crosslinkable ethylene plastics compounds. Two types of compounds are covered, namely, mechanical types in which mechanical strength properties are of prime importance in applications, and electrical types in which electrical insulating or conducting properties also are of prime importance in applications. These compounds shall be classified as: Type I; Type II; and Grade A. Tests shall be performed to determine the properties in accordance with the following test methods: conditioning; test conditions; ultimate elongation; elongation retention after aging; apparent modulus of rigidity; brittleness temperature; dielectric constant; dissipation factor; and degree of crosslinking.1.1 This specification covers a general classification system for crosslinkable ethylene plastics compounds (Note 1). The requirements specified herein are not necessarily applicable for use as criteria in determining suitability for the end use of a fabricated product.NOTE 1: It is to be noted that this specification describes materials that are available commercially in their uncrosslinked form. Therefore, they are crosslinkable compounds despite the fact that measurement of the parameters used for their classification and specification will usually be carried out after curing has been effected.1.2 Two types of compounds are covered, namely, mechanical types in which mechanical strength properties are of prime importance in applications, and electrical types in which electrical insulating or conducting properties also are of prime importance in applications.1.3 The parameters used to classify and specify the mechanical types are ultimate elongation, elongation retention after aging, apparent modulus of rigidity, and brittleness temperature.1.4 The parameters used to classify and specify the electrical types are ultimate elongation, elongation retention after aging, apparent modulus of rigidity, brittleness temperature, dielectric constant, dissipation factor, and volume resistivity.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.6 The following safety hazards caveat pertains only to the test methods portion, Section 7, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: There is no known ISO equivalent to this standard.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E1119-23 Standard Specification for Industrial Grade Ethylene Glycol Active 发布日期 :  1970-01-01 实施日期 : 

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