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1.1 This specification establishes the requirements for hard-drawn, seamless capillary tube made from Copper Alloy UNS Nos. C10800, C12000, or C12200.1.2 This tube is commonly supplied in straight lengths intended for restrictor applications such as metering lines for liquids and gases where close control over smoothness and diameter of the bore is required to insure uniform flow characteristics between tubes.1.3 Units—The values stated in inch pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The multidimensional approach permits all of the trace impurities to be well separated from the main vinyl chloride peak, thereby improving quantitative accuracy over established packed column methods.5.2 The minimum detection limit (MDL) for all components of interest has been shown to be well below 500 ppb for this test method.1.1 This is a general-purpose capillary-based test method for the determination of trace level impurities in high-purity vinyl chloride. This test method uses serially coupled capillary PLOT columns in conjunction with the multidimensional techniques of column switching and cryogenic trapping to permit the complete separation of the 11 key vinyl chloride impurities in a single 25-min run.NOTE 1: There is no known ISO equivalent to this standard.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 8.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method determines the purity of isophorone, as well as the concentration of various potential impurities, several of which are critical in the application of these solvents.1.1 This test method covers the determination of the purity of isophorone. This method also determines the impurities of the material in concentration level less than 0.5 mass %, which may include mesityl oxide (MSO), mesityl oxide-isomer, mesitylene, trimethyl cyclohexenone (TMCH), phorone, phorone-isomer, xylitone, and tetralone.1.2 Water cannot be determined by this test method and shall be measured by other appropriate ASTM procedure. The result is used to normalize the chromatographic data determined by this test method.1.3 For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The viscosity at 60 °C [140 °F] characterizes flow behavior and may be used for specification requirements for cutback asphalt and asphalt binders.NOTE 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method covers procedures for the determination of the apparent viscosity of asphalt binder by vacuum capillary viscometers at 60 °C [140 °F]. It is applicable to materials having viscosities in the range from 0.0036 to over 20 000 Pa·s [0.036 to over 200 000 P].NOTE 1: This test method is suitable for use at other temperatures, but the precision is based on determinations on asphalt binders at 60 °C [140 °F].NOTE 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The apparent viscosity for non-Newtonian asphalt binders varies with shear rate. When the flow is non-Newtonian in a capillary tube, the shear rate determined using this test method may be invalid. The presence of non-Newtonian behavior for the test conditions of this test can be verified by measuring the viscosity with viscometers having different-sized capillary tubes or with different pressure heads. The defined precision limits in Section 11 may not be applicable to non-Newtonian asphalt binders. Test Method D4957 may be a more applicable method for testing non-Newtonian asphalts.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.1.4 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 A measurement of the residual acrylonitrile in nitrile rubbers (NBR), styrene-acrylonitrile copolymers or ABS terpolymers will determine the polymer's suitability for various applications.4.2 Under optimum conditions, the minimum level of detection of RAN in NBR, SAN, or ABS terpolymers is approximately 50 ppb.1.1 This test method covers the determination of the residual acrylonitrile (RAN) content in nitrile-butadiene rubbers (NBR), styrene-acrylonitrile (SAN) copolymers, and rubber-modified acrylonitrile-butadiene-styrene (ABS) resins.1.2 Any components that can generate acrylonitrile in the headspace procedure will constitute an interference. The presence of 3-hydroxypropionitrile in latices limits this procedure to dry rubbers and resins.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 6.3 and 6.4.NOTE 1: There is no known ISO equivalent to this standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 These specifications cover operating instructions for glass capillary kinematic viscometers of all the types described in detail in Annex A1, Annex A2, and Annex A3 as follows:  Modified Ostwald viscometers, Annex A1  Suspended-level viscometers, Annex A2  Reverse-flow viscometers, Annex A31.2 The calibration of the viscometers is described in Section 6.1.3 This standard covers some widely used viscometers suitable for use in accordance with Test Method D445. Other viscometers of the glass capillary type which are capable of measuring kinematic viscosity within the limits of precision given in Test Method D445 may be used.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended to be used by all analysts using fused silica capillary chromatography. It contains the recommended steps for installation, preparation, proper installation, and continued column maintenance.1.1 This practice covers the installation and maintenance of fused silica capillary columns in gas chromatographs that are already retrofitted for their use. This practice excludes information on:1.1.1 Injection techniques.1.1.2 Column selection.1.1.3 Data acquisition.1.1.4 System troubleshooting and maintenance.1.2 For additional information on gas chromatography, please refer to Practice E260. For specific precautions, see 7.2.2.2(1), 7.2.2.2(2), 7.2.7, and 7.2.7.2.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safety information, see Section 6, 7.2.2.2(1), 7.2.2.2(2), 7.2.7, and 7.2.7.2.21.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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