2.1 This test method may be used to quickly determine volume and bulk density of a refractory of any shape, provided it has sufficient structural integrity to permit handling. Thus it may be used on unfired or fired, strong or friable shapes.2.2 Since the test may be performed quickly, it has found application as manufacturing in-process control as well as in characterizing finished refractory products. Also it may be used to examine specimens after other test or service exposure.1.1 This test method covers the basic procedure for determining bulk density and volume of refractory shapes. This test is applicable to all refractory shapes or monoliths, burned or unburned, independent of composition or forming method, including materials that slake and hydrate. It is particularly suitable for determining bulk density and volume of complex shapes after forming, since results may be obtained in a matter of minutes.1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.2.1 Exception—The balance used in this standard is only available in SI units (Sections 3 – 6).1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see 3.2.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a procedure for determining the density and void content of freshly mixed pervious concrete.5.2 This test method is applicable to pervious concrete mixtures containing coarse aggregate with a nominal maximum size of 25 mm [1 in.] or smaller.5.3 The measured fresh density may be used as verification of mixture proportions.5.4 This method uses a standard consolidation procedure to measure fresh density and void content of a pervious concrete mixture as delivered. Test results are not intended to represent the density and void content of the in-place pervious concrete. This method shall not be used to determine the in-place void content or yield of the pervious concrete.5.5 The fresh density and void content calculated from this test method may be different when comparing the results from Procedure A with Procedure B. Results are only comparable when obtained using the same procedure (Procedure A or B).1.1 This test method covers determining the density of freshly mixed pervious concrete under standardized conditions and gives formulas for calculating the void content of pervious concrete. Test results are not intended to represent the in-place density and void content.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.4 The text of this test method references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this test method.

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5.1 Accurate determination of the density, relative density (specific gravity), or API gravity of petroleum and its products is necessary for the conversion of measured volumes to volumes or masses, or both, at the standard reference temperatures of 15 °C or 60 °F during custody transfer.5.2 This procedure is most suitable for determining the density, relative density (specific gravity), or API gravity of low viscosity transparent liquids. This procedure can also be used for viscous liquids by allowing sufficient time for the hydrometer to reach temperature equilibrium, and for opaque liquids by employing a suitable meniscus correction. Additionally for both transparent and opaque fluids the readings shall be corrected for the thermal glass expansion effect and alternative calibration temperature effects before correcting to the reference temperature.5.3 When used in connection with bulk oil measurements, volume correction errors are minimized by observing the hydrometer reading at a temperature close to that of the bulk oil temperature.5.4 Density, relative density, or API gravity is a factor governing the quality and pricing of crude petroleum. However, this property of petroleum is an uncertain indication of its quality unless correlated with other properties.5.5 Density is an important quality indicator for automotive, aviation and marine fuels, where it affects storage, handling and combustion.1.1 This test method covers the laboratory determination using a glass hydrometer in conjunction with a series of calculations, of the density, relative density, or API gravity of crude petroleum, petroleum products, or mixtures of petroleum and nonpetroleum products normally handled as liquids, and having a Reid vapor pressure of 101.325 kPa (14.696 psi) or less. Values are determined at existing temperatures and corrected to 15 °C or 60 °F by means of a series of calculations and international standard tables.1.2 The initial hydrometer readings obtained are uncorrected hydrometer readings and not density measurements. Readings are measured on a hydrometer at either the reference temperature or at another convenient temperature, and readings are corrected for the meniscus effect, the thermal glass expansion effect, alternative calibration temperature effects and to the reference temperature by means of the Petroleum Measurement Tables; values obtained at other than the reference temperature being hydrometer readings and not density measurements.1.3 Readings determined as density, relative density, or API gravity can be converted to equivalent values in the other units or alternative reference temperatures by means of Interconversion Procedures (API MPMS Chapter 11.5), or Adjunct to D1250 Guide for Petroleum Measurement Tables (API MPMS Chapter 11.1), or both, or tables, as applicable.1.4 The initial hydrometer readings determined in the laboratory shall be recorded before performing any calculations. The calculations required in Section 10 shall be applied to the initial hydrometer reading with observations and results reported as required by Section 11 prior to use in a subsequent calculation procedure (ticket calculation, meter factor calculation, or base prover volume determination).1.5 Annex A1 contains a procedure for verifying or certifying the equipment for this test method.1.6 The values stated in SI units are to be regarded as standard.1.6.1 Exception—The values given in parentheses are provided for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The heating value is a measure of the suitability of a pure gas or a gas mixture for use as a fuel; it indicates the amount of energy that can be obtained as heat by burning a unit of gas. For use as heating agents, the relative merits of gases from different sources and having different compositions can be compared readily on the basis of their heating values. Therefore, the heating value is used as a parameter for determining the price of gas in custody transfer. It is also an essential factor in calculating the efficiencies of energy conversion devices such as gas-fired turbines. The heating values of a gas depend not only upon the temperature and pressure, but also upon the degree of saturation with water vapor. However, some calorimetric methods for measuring heating values are based upon the gas being saturated with water at the specified conditions.5.2 The relative density (specific gravity) of a gas quantifies the density of the gas as compared with that of air under the same conditions.1.1 This practice covers procedures for calculating heating value, relative density, and compressibility factor at base conditions (14.696 psia and 60°F (15.6°C)) for natural gas mixtures from compositional analysis.2 It applies to all common types of utility gaseous fuels, for example, dry natural gas, reformed gas, oil gas (both high and low Btu), propane-air, carbureted water gas, coke oven gas, and retort coal gas, for which suitable methods of analysis as described in Section 6 are available. Calculation procedures for other base conditions are given.1.2 The values stated in inch-pound units are to be regarded as the standard. The SI units given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is useful as a repeatable, nondestructive technique to monitor in-place density and moisture of soil and rock along lengthy sections of horizontal, slanted, and vertical access holes or tubes. With proper calibration in accordance with Annex A1, this test method can be used to quantify changes in density and moisture content of soil and rock.5.2 This test method is used in vadose zone monitoring, for performance assessment of engineered barriers at waste facilities, and for research related to monitoring the movement of liquids (water solutions and hydrocarbons) through soil and rock. The nondestructive nature of the test allows repetitive measurements at a site and statistical analysis of results.5.3 The fundamental assumptions inherent in the density measurement portion of this test method are that Compton scattering and photoelectric absorption are the dominant interactions of the gamma rays with the material under test.5.4 The probe response, in counts, can be converted to wet density by comparing the detected rate of gamma radiation with previously established calibration data (see Annex A1).5.5 The probe count response may also be utilized directly for unitless, relative comparison with other probe readings.5.5.1 For materials of densities higher than that of about the density of water, higher count rates within the same soil type relate to lower densities and, conversely, lower count rates within the same soil type relate to higher densities.5.5.2 For materials of densities lower than the density of water, higher count rates within the same soil type relate to higher densities and, conversely, lower count rates within the same soil type relate to lower densities.5.5.3 Because of the functional inflection of probe response for densities near the density of water, exercise great care when drawing conclusions from probe response in this density range.5.6 The fundamental assumption inherent in the moisture measurement portion of this test is that the hydrogen contained in the water molecules within the soil and rock is the dominant neutron thermalizing media, so increased water content of the soil and rock results in higher count rates of the moisture content system of the instrument.1.1 This test method covers collection and comparison of logs of thermalized-neutron counts and back-scattered gamma counts along horizontal or vertical air-filled access tubes.1.2 For limitations, see Section 6, “Interferences.”1.3 The in situ water content in mass per unit volume and the density in mass per unit volume of soil and rock at positions or in intervals along the length of an access tube are calculated by comparing the thermal neutron count rate and gamma count rates respectively to previously established calibration data.1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. Within the text of this standard, SI units appear first followed by the inch-pound (or other non-SI) units in brackets1.4.1 Reporting the test results in units other than SI shall not be regarded as nonconformance with the standard.1.5 All observed and calculated values shall conform to the guide for significant digits and rounding established in Practice D6026.1.5.1 The procedures used to specify how data are collected, recorded, and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazards, see Section 8.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Loose density gives an indication of the degree of fiberization, harshness, and loftiness of asbestos fiber.1.1 This test method covers the determination of the loose density of asbestos fiber for Groups 5 to 9, inclusive (as determined by Test Method D3639/D3639M).21.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 Warning—Breathing of asbestos dust is hazardous. Asbestos and asbestos products present demonstrated health risks for users and for those with whom they come into contact. In addition to other precautions, when working with asbestos-cement products, minimize the dust that results. For information on the safe use of chrysoltile asbestos, refer to “Safe Use of Chrysotile Asbestos: A Manual on Preventive and Control Measures.”31.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard warning, see 1.3.

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3.1 This test method concerns the compaction of crushed coal to determine either its compacted or uncompacted bulk density, for purposes such as charging coke ovens.1.1 This test method covers two procedures for determining the bulk density of crushed coal less than 37.5 mm [1.5 in.] in size, such as is charged into coke ovens, as follows:1.1.1 Procedure A—The cone procedure for determining an uncompacted bulk density.1.1.1.1 Standard Method—Procedure employs the use of a 115 mm [4.5 in.] chute opening and a measuring box having dimensions of 305 mm x 305 mm x 305 mm [12.0 in. x 12.0 in. x 12.0 in.].1.1.1.2 Alternate Method—Procedure employs the use of a 203 mm [8.0 in.] chute opening and a measuring box having dimensions of 203 mm x 203 mm x 305 mm [8.0 in. x 8.0 in. x 12.0 in.] for coals with a total moisture greater than 7 %.1.1.2 Procedure B—The dropped-coal procedure for determining a compacted bulk density, comparable to actual bulk densities attained in coke ovens.1.2 This test method is not applicable to the testing of powdered coal as used in boiler plants, nor to the determination of the bulk density of coal in storage piles.1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The test method described is useful as a rapid, nondestructive technique for in-place measurements of bulk density of soil and soil-aggregate. Test results may be used for the determination of dry density if the water content of the soil or soil-aggregate is determined by separate means, such as those methods described in Test Methods D2216, D4643, D4944, and D4959.4.2 The test method is used for quality control and acceptance testing of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The nondestructive nature allows repetitive measurements at a single test location and statistical analysis of the results.4.3 Density—The fundamental assumptions inherent in the method is that Compton scattering is the dominant interaction and that the material is homogeneous.NOTE 3: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method describes the procedures for measuring in-place bulk density of soil and soil-aggregate using nuclear equipment with radioactive sources (hereafter referred to simply as “gauges”). These gauges are distinct from those described in Test Method D6938 insofar as:1.1.1 These gauges do not contain a system (nuclear or otherwise) for the determination of the water content of the material under measurement.1.1.2 These gauges have photon yields sufficiently low as to require the inclusion of background radiation effects on the response during normal operation.1.1.2.1 For the devices described in Test Method D6938, the contribution of gamma rays detected from the naturally-occurring radioisotopes in most soils (hereafter referred to as “background”) compared to the contribution of gamma rays used by the device to measure in-place bulk density is typically small enough to be negligible in terms of their effect on measurement accuracy. However, for these low-activity gauges, the gamma ray yield from the gauge is low enough that the background contribution from most soils compared to the contribution of gamma rays from the gauge is no longer negligible, and changes in this background can adversely affect the accuracy of the bulk density reading.1.1.2.2 In order to compensate for potentially differing background contribution to low-activity gauge measurements at different test sites, a background reading must be taken in conjunction with gauge measurements obtained at a given test site. This background reading is utilized in the bulk density calculation performed by the gauge with the goal of minimizing these background effects on the density measurement accuracy.1.2 For limitations see Section 5 on Interferences.1.3 The bulk density of soil and soil-aggregate is measured by the attenuation of gamma radiation where the source is placed at a known depth up to 300 mm [12 in.] and the detector(s) remains on the surface (some gauges may reverse this orientation).1.3.1 The bulk density of the test sample in mass per unit volume is calculated by comparing the detected rate of gamma radiation with previously established calibration data.1.3.2 Neither the dry density nor the water content of the test sample is measured by this device. However, the results of this test can be used with the water content or water mass per unit volume value determined by alternative methods to determine the dry density of the test sample.1.4 The gauge is calibrated to read the bulk density of soil or soil-aggregate.1.5 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.5.1 For purposes of comparing, a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal or significant digits in the specified limits.1.5.2 The procedures used to specify how data are collected/recorded and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting test results in units other than SI shall not be regarded as nonconformance with this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: Nuclear density gauge manuals and reference materials, as well as the gauge displays themselves, typically refer to bulk density as “wet density” or “WD.”NOTE 2: The term “bulk density” is used throughout this standard. This term has different definitions in Terminology D653, depending on the context of its use. For this standard, however, “bulk density” refers to, as defined in Terminology D653, “the total mass of partially saturated or saturated soil or rock per unit total volume.”1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a means of controlling smoke production in home heating equipment to an acceptable level. Excessive smoke density adversely affects efficiency by heat-exchanger fouling.5.2 The range of smoke densities covered by this test method is that which has been found particularly pertinent to home-heating application. It is more sensitive to small amounts of smoke than several other smoke tests as indicated in the following comparison:Smoke SpotNumber Icham, percentTransmission RingelmanSmoke Number0 100 02  95 04  80 06  54 08  18 09   0 09   0 0 to 51.1 This test method covers the evaluation of smoke density in the flue gases from burning distillate fuels. It is intended primarily for use with home heating equipment burning kerosine or heating oils. It can be used in the laboratory or in the field to compare fuels for clean burning or to compare heating equipment.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 Arbitrary and relative units are also used.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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