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5.1 This test method is used to determine the density expressed in g/mL for powdered or fine mesh carbon. Due to the nature of the small particles, the density of these carbon types cannot be measured using the same procedure as granular carbon.1.1 This test method covers the determination of the mechanically tapped density of powdered and fine mesh activated carbon. For the purpose of this test method, “powdered carbon” is defined as having a mean particle diameter less than 45 µm, and “fine mesh carbon” is defined as having a particle size predominately between 80 and 325 U.S. Standard mesh.1.2 The values in SI units are to be regarded as standard. No other units of measure are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Relative density (specific gravity) is the characteristic generally used for calculation of the volume occupied by the aggregate in various mixtures containing aggregate, including portland cement concrete, bituminous concrete, and other mixtures that are proportioned or analyzed on an absolute volume basis. Relative density (specific gravity) is also used in the computation of voids in aggregate in Test Method C29/C29M. Relative density (specific gravity) saturated surface dry (SSD) is used if the aggregate is at SSD, that is, if its absorption has been satisfied. Conversely, the relative density (specific gravity) oven dry (OD) is used for computations when the aggregate is dry or assumed to be dry.4.2 Apparent density and apparent relative density (apparent specific gravity) pertain to the solid material making up the constituent particles not including the pore space within the particles which is accessible to water.4.3 Absorption values are used to calculate the change in the mass of an aggregate due to water absorbed in the pore spaces within the constituent particles, when it is deemed that the aggregate has been in contact with water long enough to satisfy the absorption potential. The laboratory standard for absorption is that obtained after submerging dry aggregate for a prescribed period of time.NOTE 1: There are other test methods that have been used and continue to be used to determine these aggregate properties: Test Methods C127 and C128. This test method may result in values for these properties that are close to or divergent from values from other test methods.NOTE 2: The quality of the results produced by this standard are dependent upon the competence of the personnel performing the procedure and the capability, calibration, and the maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method covers the determination of relative density and absorption of fine aggregates by Method A and coarse and blended aggregates by Method B.1.2 A multi-laboratory precision and bias statement for coarse and combined aggregate tests in this standard has not been developed at this time. Therefore, this standard should not be used for acceptance or rejection of coarse and combined aggregate materials for purchasing purposes.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. Some values have only SI units because inch-pound equivalents are not used in practice.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides an indication of in-situ undrained shear strength of saturated fine-grained soils (clays and silts) or other saturated fine-grained geomaterials, such as mine tailings and organic muck. The test is applicable to soils with undrained strengths of less than 200 kPa [2 tsf]. Very sensitive soils can be remolded during vane insertion.5.2 This test method is used extensively in a variety of geotechnical explorations to evaluate rapid loading strength for total stress analysis of saturated fine-grained clays and silts. Since vane shear strength values are most always higher than field strengths for analyses (5.3) they often are checked or compared with other methods of measuring undrained shear strength. Cone Penetrometer Tests (Test Method D5778) and Unconsolidated Undrained Triaxial Compression (D2850) tests are most often performed for direct comparison to the vane shear strength data. Unconfined Compression (D2166/D2166M) testing could also be performed, but suffers from many possible errors from disturbance especially in fissured clays, and should only be performed with experience. For more information on how these tests are used for soft ground site exploration refer to Ladd and DeGroot.(1)45.3 The peak undrained shear resistance of the vane test is commonly corrected to determine the undrained shear strength for geotechnical analysis. The agency requesting the testing must interpret these data to determine applicability for strength analysis. It is beyond the scope of this standard to recommend applicability of vane testing for geotechnical analysis. For information on the general use of these correction factors, consult Appendix X1.5.4 This method is not applicable in unsaturated soils or in non-plastic silts, sands, gravels, or other high permeability soils. With the shearing rates described in this standard, sand lenses, if present, will allow total or partial drainage. Unsaturated soils and soils with higher permeability, in rapid shear, can dilate or collapse and generate negative or positive pore pressures which may, or may not, dissipate in the shearing process. It is important to check the soil type being tested. It is very beneficial to sample the soil either before or after testing, to understand the drainage conditions (permeability) of the soil tested.5.5 This method also applies to hand held vane shear tests performed at shallow depths, however, hand held equipment may be less accurate, because it may be more difficult to maintain vane/rod stability and verticality.NOTE 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Standard Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the field vane test in saturated clay and silt soils for determination of undrained shear strength. Knowledge of the nature of the soil in which each vane test is to be made is necessary for assessment of the applicability and interpretation of the test. The test is not applicable for sandy soils or non-plastic silts, which may allow drainage during the test.1.2 This test method addresses testing on land and for testing in drill holes or by self-drilling or continuous push methods from the ground surface. This method does not address specifically marine testing where special test requirements or variations in equipment may be required. The user is referred to ASTM STP 1014 for additional information on in-place vane shear testing used in marine exploration.21.3 This method is often used in conjunction with fluid rotary drilling (D5783), hollow-stem augers (D6151/D6151M), or cone penetration testing (D5778). Some apparatuses have the vane retracted in a protective shoe for advancement and incremental testing. Sampling, such as with thin wall tubes (D1587/D1587M) is often combined with vane testing. Subsurface geotechnical explorations are reported in accordance with Practice (D5434).1.4 Undrained shear strength and sensitivity of cohesive soils can also be measured in Laboratory Vane Test (D4648/D4648M).1.5 Units—The values stated in either SI units or inch-pound units [presented in brackets] are to be regarded separately as standard. The values in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this test method.1.5.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The rationalized slug unit is not given, unless dynamic (F = ma) calculations are involved.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.6.1 The procedures used to specify how data are collected/ recorded or calculated in this standard are regarded as the industry standard. In addition they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives, and it is common practice to increase or reduce significant digits or reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Particle-size distribution (gradation) is a descriptive term referring to the proportions by dry mass of a soil distributed over specified particle-size ranges. The gradation curve generated using this method yields the distribution of silt and clay size fractions present in the soil based on size definitions, not mineralogy or Atterberg limit classification.5.2 Unless the sedimentation sample is representative of the entire sample, the sedimentation results must be combined with a sieve analysis to obtain the complete particle size distribution.5.3 The clay size fraction is material finer than 2 µm. The clay size fraction is used in combination with the Plasticity Index (Test Methods D4318) to compute the activity, which provides an indication of the mineralogy of the clay fraction.5.4 The gradation of the silt and clay size fractions is an important factor in determining the susceptibility of fine-grained soils to frost action.5.5 The gradation of a soil is an indicator of engineering properties such as hydraulic conductivity, compressibility, and shear strength. However, soil behavior for engineering and other purposes is dependent upon many factors, such as effective stress, mineral type, structure, plasticity, and geological origin, and cannot be based solely upon gradation.5.6 Some types of soil require special treatment in order to correctly determine the particle sizes. For example, chemical cementing agents can bond clay particles together and should be treated in an effort to remove the cementing agents when possible. Hydrogen peroxide and moderate heat can digest organics. Hydrochloric acid can remove carbonates by washing and Dithionite-Citrate-Bicarbonate extraction can be used to remove iron oxides. Leaching with test water can be used to reduce salt concentration. All of these treatments, however, add significant time and effort when performing the sedimentation test and are allowable but outside the scope of this test method.5.7 The size limits of the sedimentation test are from about 100 µm to about 0.1 µm. The length of time required to obtain a stable initial reading on the hydrometer controls the upper range of results, and the test duration controls the lower range.5.8 The shape and density of the grains are important to the results. Stokes’ Law is assumed to be valid for spherical particles even though fine silt- and clay-sized particles are more likely to be plate-shaped and have greater mineral densities than larger particles.5.9 High plasticity clays develop structured water layers on their surfaces. According to Zhang and Lu3 this near surface water can be as dense as 1.4 g/L. This high-density structured water causes an error in this test method and shifts the particle size distribution curve upwards. Correction for the structured water is beyond the scope of this standard but values of percent passing above 100 % are possible and should not be excluded from the report.NOTE 5: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation by hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer of this fraction versus the log of the particle diameter.1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with results from a sieve analysis using D6913 to obtain the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.NOTE 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods D6913 (Note 2).NOTE 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”1.4 The terms “soil” and “material” are used interchangeably throughout the standard.1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than smaller particles. Stokes’ Law gives a governing equation used to determine the terminal velocity of a spherical particle falling through a stationary liquid. The terminal velocity is proportional to the square of the particle diameter. Therefore, particles are sorted by size in both time and position when settling in a container of liquid.1.5.1 Stokes’ Law has several assumptions which are: the particles are spherical and smooth; there is no interference between the particles; there is no difference between the current in the middle of the container and the sides; flow is laminar; and the particles have the same density. These assumptions are applied to soil particles of various shapes and sizes.1.6 A hydrometer is used to measure the fluid density and determine the quantity of particles in suspension at a specific time and position. The density of the soil-water suspension depends upon the concentration and specific gravity of the soil particles and the amount of dispersant added. Each hydrometer measurement at an elapsed time is used to calculate the percentage of particles finer than the diameter given by Stokes’ Law. The series of readings provide the distribution of material mass as a function of particle size.1.7 This test method does not cover procurement of the sample or processing of the sample prior to obtaining the reduced sample in any detail. It is assumed that the sample is obtained using appropriate methods and is representative of site materials or conditions. It is also assumed that the sample has been processed such that the reduced sample accurately reflects the particle-size distribution (gradation) of this finer fraction of the material.1.8 Material Processing—Material is tested in the moist or as-received state unless the material is received in an air-dried state. The moist preparation method shall be used to obtain a sedimentation test specimen from the reduced sample. Air-dried preparation is only allowed when the material is received in the air-dried state. The method to be used may be specified by the requesting authority; however, the moist preparation method shall be used for referee testing.1.9 This test method is not applicable for the following soils:1.9.1 Soils containing fibrous peat.1.9.2 Soils containing less than approximately 5 % of fine-grained material (Note 1).1.9.3 Soils containing extraneous matter, such as organic solvents, oil, asphalt, wood fragments, or similar items (Note 3).NOTE 3: If extraneous matter, such as wood, can be easily removed by hand, it is permissible to do so. However, there may be cases where the extraneous matter is being evaluated as part of the material and it should not be removed from the material.1.9.4 Materials that contain cementitious components, such as cement, fly ash, lime, or other stabilization admixtures.1.10 This test method may not produce consistent test results within and between laboratories for the following soils. To test these soils, this test method must be adapted and these adaptations documented.1.10.1 Soils that flocculate during sedimentation. Such materials may need to be treated to reduce salinity or alter the pH of the suspension.1.10.2 Friable soils in which processing changes the gradation of the soil. Typical examples of these soils are some residual soils, most weathered shales, decomposed granites, and some weakly cemented soils.1.10.3 Soils that will not readily disperse, such as glauconitic clays or some dried plastic clays.1.11 Samples that are not soils, but are made up of particles may be tested using this method. The applicable sections above should be used in applying this standard.1.12 Units—The values stated in SI units are to be regarded as standard. Except the sieve designations, they are identified using the “alternative” system in accordance with Practice E11, such as 3-in. and No. 200, instead of the “standard” designation of 75-mm and 75-µm, respectively. Reporting of test results in units other than SI shall not be regarded as non-conformance with this test method. The use of balances or scales recording pounds of mass (lbm) shall not be regarded as nonconformance with this standard.1.13 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.1.13.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this test method to consider significant digits used in analysis methods for engineering or other data.1.14 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.15 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The particle size of fine mesh and powdered activated carbon is sometimes used to evaluate filter cake filtration rates and the filter penetration in filtering applications.5.2 The selection and handling of fine mesh or powdered activated carbon, and operation of processes using fine mesh or powdered activated carbon, requires the knowledge of the particle size.5.3 This test method is intended for single sieve testing only. For determination of particle size distribution of a sample, the test must be repeated using sieves with different openings.NOTE 1: Relative humidity (RH) can affect the repeatability and accuracy of this test. Activated carbon not at equilibrium with the RH of the ambient air may lose or gain weight accordingly, dependent upon whether the carbon picks up or loses moisture.1.1 This test method covers the determination of the particle size of powdered activated carbons using an air-jet sieve device. For purposes of this test method, powdered activated carbon is defined as activated carbon in particle sizes predominantly in a range of 80 mesh (0.180 mm) through 500 mesh (0.025 mm).1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The ring shear test is suited to the relatively rapid determination of drained residual shear strength because of the short drainage path through the thin specimen, the constant cross-sectional area of the shear surface during shear, unlimited rotational displacement in one direction, and the capability of testing one specimen under different effective normal stresses to obtain clay particles that are oriented parallel to the direction of shear to obtain residual shear strength envelope.5.2 The apparatus allows a reconstituted specimen to be overconsolidated and presheared prior to drained shearing. Overconsolidation and preshearing of the reconstituted specimen significantly reduces the horizontal displacement required to reach a residual condition, and therefore, reduces soil extrusion, wall friction, and other problems (Stark and Eid, 1993)3. This simulates a preexisting shear surface along which the drained residual strength can be mobilized.5.3 The ring shear test specimen is annular so the angular displacement differs from the inner edge to the outer edge. At the residual condition, the shear strength is constant across the specimen so the difference in shear stress between the inner and outer edges of the specimen is negligible.NOTE 1: Notwithstanding the statements on precision and bias contained in this test method: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent testing. Users of this test method are cautioned that compliance with Practice D3740 does not ensure reliable testing. Reliable testing depends on several factors; Practice D3740 provides a means of evaluating some of those factors.1.1 Fine-grained soils in this Test Method are restricted to soils containing no more than 15 % fine sand (100 % passing the 425 μm (No. 40) sieve and no more than 15 % retained on the 75 μm (No. 200) sieve).A Summary of Changes section appears at the end of this standard.1.2 This test method provides a procedure for performing a torsional ring shear test under a drained condition to determine the residual shear strength of fine-grained soils. This test method is performed by shearing a reconstituted, overconsolidated, presheared specimen at a controlled displacement rate until the constant drained shear resistance is established on a single shear surface determined by the configuration of the apparatus.1.3 In this test, the specimen rotates in one direction until the constant or residual shear resistance is established. The amount of rotation is converted to displacement using the average radius of the specimen and multiplying it by numbers of degrees traveled and 0.0174.1.4 An intact specimen or a specimen with a natural shear surface can be used for testing. However, obtaining a natural slip surface specimen, determining the direction of field shearing, and trimming and aligning the usually non-horizontal shear surface in the ring shear apparatus is difficult. As a result, this test method focuses on the use of a reconstituted specimen to determine the residual strength. An unlimited amount of continuous shear displacement can be achieved to obtain a residual strength condition in a ring shear device.1.5 A shear stress-displacement relationship may be obtained from this test method. However, a shear stress-strain relationship or any associated quantity, such as modulus, cannot be determined from this test method because the height of the shear zone unknown, so an accurate or representative shear strain cannot be determined.1.6 The selection of effective normal stresses and determination of the shear strength parameters for design analyses are the responsibility of the professional or office requesting the test. Generally, three or more effective normal stresses are applied to a test specimen in a multi-stage test or a new specimen can be used for each effective normal stress to determine the drained residual failure envelope.1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. The values given in parentheses are mathematical conversions to inch-pound units. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.1.8 All measured and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026 unless superseded by this standard.1.8.1 The procedures used to specify how data are collected/recorded or calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method assigns an empirical value to the relative amount, fineness, and character of clay-like material present in the test specimen.5.2 A minimum sand equivalent value may be specified to limit the permissible quantity of clay-like or clay-size fines in an aggregate.5.3 This test method provides a rapid field method for determining changes in the quality of aggregates during production or placement.NOTE 3: The quality of the results produced by this standard are dependent upon the competence of the personnel performing the procedure and the capability, calibration, and the maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method is intended to serve as a rapid field correlation test. The purpose of this test method is to indicate, under standard conditions, the relative proportions of clay-size or plastic fines and dust in granular soils and fine aggregates that pass the 4.75 mm (No. 4) sieve. The term “sand equivalent” expresses the concept that most granular soils and some fine aggregates are mixtures of desirable coarse particles, sand-size particles, and generally undesirable clay or plastic fines and dust.NOTE 1: For fine aggregates containing clean dust of fracture (clay-size particles that are not clay minerals), test results will depend on the amount of fines present in the material. In this case, other tests such as Methylene Blue Value (AASHTO T 330) or X-ray diffraction (XRD) may be needed to determine if the fines are deleterious.NOTE 2: Some agencies perform the test on material with a top size smaller than the 4.75 mm (No. 4) sieve. This is done to avoid trapping the clay-size or plastic fines and dust below flaky shaped 4.75 to 2.36 mm (No. 4 to 8) sized particles. Testing smaller top sized material may lower the numerical results of the test.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.2.1 Regarding sieves, per Specification E11 subsection 1.3, “the values stated in SI units shall be considered standard for the dimensions of the sieve cloth openings and the wire diameter used in the sieve cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames, pans, and covers.” When sieve mesh sizes are referenced, the alternate inch-pound designations are provided for information purposes and enclosed in parentheses.1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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AbstractThese test methods cover the testing of fine wire, flat or round, approximately 0.010 in. (0.25 mm) and smaller in diameter or thickness, used in electronic devices and lamps. Chemical analysis of the material shall be made in accordance with the requirements prescribed. The procedures in determining the out-of-roundness, edgewise curvature of ribbon, and straightness of straightened round wire are presented in details. Tension test and electrical resistivity test shall be performed to meet the requirements prescribed.1.1 These test methods cover the testing of fine wire, flat or round, approximately 0.010 in. (0.25 mm) and smaller in diameter or thickness, used in electronic devices and lamps.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The ring shear apparatus maintains the cross-sectional area of the shear surface constant during shear and shears the specimen continuously in one rotational direction for any magnitude of shear displacement and along the entire specimen cross-sectional area.5.2 The ring shear apparatus allows a reconstituted specimen to be consolidated at the desired normal stress prior to drained shearing. This simulates the field conditions under which complete softening develops in overconsolidated clays, claystones, mudstones, and shales that do not have a pre-existing shear surface, sheared bedding planes, joints, or faults as described by Skempton (19702 and 19773) and unfailed compacted fill slopes (Gamez and Stark 20144) because the fully softened strength corresponds to the peak shear strength of a normally consolidated fine-grained soil. The fully softened strength is only applicable to the soil zones that are subject to the environmental deterioration and applied shear stresses that lead to soil softening, deterioration of soil fabric, and strength loss, which may not be relevant to all slopes and all depths. The fully softened strength should be used in an effective stress/drained stability analysis using a stress dependent strength envelope for slopes with no prior shearing.5.3 The ring shear test is suited to the determination of the drained fully softened shear strength because of the short drainage path through the thin specimen, small post-peak strength loss in a normally consolidated specimen, and the constant cross-sectional area.5.4 The ring shear test specimen is annular so the angular displacement differs from the inner radius to the outer radius. This is not significant because a normally consolidated specimen does not exhibit a large post-peak strength loss so the difference in peak shear resistance at the inner radius and outer radius at different displacements is not significant and the ratio of the inner to outer radii of the ring is greater than 0.5 in accordance with Hvorslev (1936)6.NOTE 1: Notwithstanding the statements on precision and bias contained in this test method: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent testing. Users of this test method are cautioned that compliance with Practice D3740 does not ensure reliable testing. Reliable testing depends on several factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method provides a procedure for performing a torsional ring shear test under a drained condition to measure the fully softened shear strength and stress dependent strength envelope of fine-grained soils (using a reconstituted normally consolidated specimen). The fully softened strength and the corresponding stress dependent effective stress strength envelope are used to evaluate the stability of slopes that do not have a pre-existing shear surface but have been subjected to environmental conditions and shear stresses that lead to soil softening, deterioration of the soil fabric, and strength loss. It has been shown (Skempton 19702 and 19773) that under these conditions and within the depth zones that have undergone softening, first-time slope failures can occur at effective stress levels that correspond to a fully softened strength envelope. It has also been shown empirically (Skempton 19702 and 19773) that fully softened strength of fine grained soils can be approximated by the peak strength of a reconstituted and normally consolidated specimen. In this test method, reconstituted and normally consolidated specimens are sheared at a controlled and constant displacement rate until the peak shear resistance has been obtained. Generally, the drained fully softened failure envelope is determined at three or more effective normal stresses. A separate test specimen must be used for each normal stress to measure the fully softened strength otherwise a post-peak or even drained residual strength will be measured if the same specimen is used at the same or at another effective normal stress because of the existence of a prior shear surface.1.2 The ring shear apparatus allows a reconstituted specimen to be normally consolidated at the desired normal stress prior to drained shearing. The test results closely simulate the fully softened strength of stiff natural fine-grained soils (Skempton 19702 and 19773) and compacted fills of fine-grained soils (Gamez and Stark 20144). This simulates the mobilized shear strength in overconsolidated clays, claystones, mudstones, and shales in natural slopes and compacted fill in manmade slopes, such as, dams, levees, and highway embankments, after the soil has fully softened and attained the fully softened strength condition.1.3 A shear stress-displacement relationship may be obtained from this test method. However, a shear stress-strain relationship or any associated quantity, such as modulus, cannot be determined from this test method because defining the height of the shear zone is difficult and needed in the shear strain calculations. As a result, the height of this shear zone is unknown, so an accurate or representative shear strain can therefore not be determined.1.4 The selection of normal stresses and final determination of the shear strength envelope for design analyses and the criteria to interpret and evaluate the test results are the responsibility of the engineer or entity requesting the test.1.5 Units—The values stated in SI units are to be regarded as the standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The shear strength of a specimen depends on the method of shearing, soil type, vertical consolidation stress, time of consolidation, rate of strain, and prior stress history of the soil.5.2 In this test, the shear strength is measured under constant volume conditions that are equivalent to undrained conditions for a saturated specimen; hence, the test is applicable to field conditions wherein soils have fully consolidated under one set of stresses, and then are subjected to changes in stress without time for further drainage to take place.5.3 The constant volume (undrained) strength is a function of stress conditions. In this test method, the strength is measured under plane strain conditions and the principle stresses continuously rotate due to the application of shear stress. This simple shear stress condition occurs in many field situations including zones below a long embankment and around axially loaded piles.5.4 The state of stress within the simple shear specimen is not sufficiently defined nor uniform enough to allow rigorous interpretation of the results. Expressing the data in terms of the shear stress and vertical effective stress on the horizontal plane is useful for engineering purposes, but should not be confused with the effective stress parameters derived from other shear tests having better defined states of stress.5.5 The values of the secant shear modulus can be used to estimate the initial settlements of embankments built on saturated cohesive soils due to undrained shear deformations.5.6 The data and the rate of consolidation from the consolidation portion of this test are comparable to results obtained using Test Methods D2435 provided that the more rigorous consolidation procedure of Test Methods D2435 is followed.5.6.1 When using wire reinforced membranes the vertical displacements measured from Test Methods D2435 are somewhat smaller than for the direct simple shear test because the direct simple shear (DSS) specimen's lateral confinement is less rigid.5.6.2 The estimated preconsolidation pressure is comparable provided the specimen is loaded sufficiently into the normally consolidated range.1.1 This test method defines equipment specifications and testing procedures for the measurement of constant volume strength and stress-strain characteristics of cohesive soils after one-dimensional consolidation using a constant rate of simple shear deformation mode of loading. The constant volume condition is equivalent to the undrained condition for saturated specimens.1.2 This test method is written specifically for devices that test rectangular parallelepiped or cylindrical specimens. Other more general devices, such as the torsional shear hollow cylinder, may be used to perform consolidated constant volume simple shear tests but are beyond the scope of this test method.1.3 This test method is applicable to testing intact, laboratory reconstituted, and compacted soils, however, it does not include specific guidance for reconstituting or compacting test specimens.1.4 It shall be the responsibility of the agency requesting this test to specify the magnitude of the vertical consolidation stress prior to constant volume shear and, when appropriate, the maximum vertical consolidation stress, which will result in an overconsolidated specimen.1.5 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this test method.1.5.1 In the engineering profession it is customary practice to use, interchangeably, units representing both mass and force, unless dynamic calculations (F=Ma) are involved. This implicitly combines two separate systems of units, that is, the absolute system and the gravimetric system. It is scientifically undesirable to combine two separate systems within a single standard. This test method has been written using SI units; however, inch-pound conversions are given in the gravimetric system, where the pound (lbf) represents a unit of force (weight). The use of balances or scales recording pounds of mass (lbm), or the recording of density in lb/ft3 should not be regarded as nonconformance with this test method.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.6.1 The procedures used to specify how data are collected/recorded or calculated in this test standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this test standard to consider significant digits used in analysis methods for engineering design.1.6.2 Measurements made to more significant digits or better sensitivity than specified in this standard shall not be regarded a nonconformance with this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1137-05 Standard Test Method for Degradation of Fine Aggregate Due to Attrition (Withdrawn 2011) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

The tendency of some fine aggregates, including those that comply with the requirements of Specification C 33, to degrade from the grinding action in a concrete mixer may affect mixing water demand, entrained air, and slump. When it is suspected that degradation during mixing is a problem, this test method may be useful for evaluating the extent of the problem.This test method is of use for preliminary screening to indicate the need for further evaluation through petrographic examination (Guide C 295) or testing the quality of mortar, or concrete, or both made from the fine aggregate in question.This test method is of use for comparing the results obtained with unknown materials against those with materials of known performance in concrete.1.1 This test method provides a procedure for indicating the relative degree to which a fine aggregate is likely to degrade due to the mixing and agitation of hydraulic cement concrete.1.2 The values given in SI units are to be regarded as the standard. The values given in inch-pound units are for information only.1.3 The text of this test method references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this test method.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is used primarily to determine the grading of materials proposed for use as aggregates or being used as aggregates. The results are used to determine compliance of the particle size distribution with applicable specification requirements and to provide necessary data for control of the production of various aggregate products and mixtures containing aggregates. The data may also be useful in developing relationships concerning porosity and packing.5.2 Accurate determination of material finer than the 75-μm (No. 200) sieve cannot be achieved by use of this test method alone. Use Test Method C117 for determination of material finer than the 75-μm (No. 200) sieve by washing.5.3 Refer to methods of sampling and testing in Specification C637 for heavyweight aggregates.1.1 This test method covers the determination of the particle size distribution of fine and coarse aggregates by sieving.1.2 Some specifications for aggregates which reference this test method contain grading requirements including both coarse and fine fractions. Instructions are included for sieve analysis of such aggregates.1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.NOTE 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size. Specification E11 cites the following with respect to SI units versus inch-pound units as standard. “The values stated in SI units shall be considered standard for the dimensions of the sieve cloth openings and the wire diameters used in the sieve cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames, pans,” and covers.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is of significance in making a final determination of the acceptability of fine aggregates with respect to the requirements of Specification C33/C33M concerning organic impurities.5.2 This test method is applicable to those samples which, when tested in accordance with Test MethodC40/C40M, have produced a supernatant liquid with a color darker than the standard listed in Table 1 of C40/C40M (Organic plate No. 3, Gardner Color Standard No. 14, Circular Disk No. 14 or prepared color solution).5.3 Many specifications provide for the acceptance of fine aggregate producing a darker color in the Test Method C40/C40M test, if testing by this test method indicates the strength of the mortar cubes prepared with the unwashed fine aggregate is comparable to the strength of mortar cubes made with the washed fine aggregate.1.1 This test method covers the determination of the effect on mortar strength of the organic impurities in fine aggregate, whose presence is indicated using Test Method C40/C40M. Comparison is made between compressive strengths of mortar made with washed and unwashed fine aggregate.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in the practice.NOTE 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.(Warning—Fresh hydraulic cementitous mixtures are caustic and may cause chemical burns to exposed skin and tissue upon prolonged exposure.)21.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C70-20 Standard Test Method for Surface Moisture in Fine Aggregate Active 发布日期 :  1970-01-01 实施日期 : 

4.1 This test method is not widely used. However, it is a convenient procedure for field or plant determination of moisture content of fine aggregate if specific gravity values are known and if drying facilities are not available. It can be used to adjust the aggregate mass for moisture content and to determine surface moisture contribution to mixing water in portland cement concrete.4.2 The accuracy of the test method depends upon accurate information on the bulk specific gravity of the material in a saturated surface-dry condition.1.1 This test method covers field determination of the amount of surface moisture in fine aggregate by displacement in water.1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method is for measuring the apparent packing density of catalyst or catalyst carrier powders that are smaller than 0.8 mm in diameter.1.1 This test method covers the determination of the apparent packing density of fine catalyst and catalyst carrier powders smaller than 0.8 mm in diameter.1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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