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4.1 Nonvolatile content of printing inks is useful for specification acceptance between the producer and the user.4.2 In order to obtain accurate results for heatset systems within the specified 3-h heating time, the specimen film thickness must be less than 100 g/m2, and the oven must have forced ventilation. Thickness of the specimen film is less critical for liquid ink systems.1.1 These test methods cover the determination of weight content of nonvolatile matter in two types of printing inks.1.2 Test Method A is applicable to heatset-type printing inks and resin solutions; solvents in such systems typically have initial boiling points in the range from 240 to 275°C (470 to 535°F) and vapor pressures less than 0.2 mm Hg.1.3 Test Method B is applicable to liquid-type printing inks and vehicles based on aqueous or organic solvents that evaporate readily at ordinary room temperatures.NOTE 1: Test Method A (for heatset systems) specifies a specimen film thickness that is much thinner than those produced by related test methods; one exception is Test Method B in Test Methods D1259, which is recommended as a referee test.NOTE 2: Test Method B (for liquid ink systems) is similar to Test Method D2369 except that a solvent is not required for spreading the test specimen.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 A common set of definitions is essential to improve communication and avoid misunderstanding among manufacturers of printing ink, printing ink vehicles, resins, solvents, oils and all other components of printing ink vehicles.1.1 This standard contains the definitions of terms as used in reference to printing ink vehicles and related materials.1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method differentiates between web materials on the basis of their ability to cause wear on surfaces with which they come in contact. This test method can also be used to evaluate the wear resistance of different materials against such web materials.1.1 This test method covers the determination of the abrasiveness of ink-impregnated fabric printer ribbons and other web materials by means of a sliding wear test.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 These practices provide means of preparing small quantities of resin solution (in some procedures in an inert gas atmosphere using uniform, controlled heating).5.2 This practice provides quick ways to prepare a resin solution for quality control testing during the manufacture of resin solutions and vehicles. Samples can usually be prepared in approximately 30 to 45 minutes or less.5.3 These practices can be used to prepare commonly specified ink test solutions such as 33.3 % resin in alkali refined linseed oil, and 50 % resin in heat-set ink solvent (that is, C12 to C16 hydrocarbon petroleum distillate with initial boiling point (IBP) about 470°F).1.1 These practices describe laboratory procedures for preparing an oil-based ink resin solution in a high-boiling solvent using four pieces of lab equipment:(1) A hot oil bath (Sections 4 to 11),(2) A stirrer/hot plate (Sections 12 to 16),(3) An industrial blender (Sections 17 to 22), and(4) A hot air gun (Sections 23 to 27).ASTM Subcommittee D01.37 recommends using the hot oil bath procedure (Practice D5597) where possible.1.2 These practices use laboratory equipment generally available in a normal, well-equipped laboratory.1.3 One or several of these practices allows for rapid resin solution preparation (under 30 min, typical), can regulate the maximum temperature, can be done under an inert atmosphere, and can prevent the random solvent loss during preparation.1.4 These procedures are for use with ink resins intended mainly for oil-based offset and letterpress inks. The type of resins are typically, but not limited to C9 aromatic hydrocarbon resins, modified dicyclopentadiene resins, rosin pentaerythritol or glycerine esters, phenolic modified rosin esters, maleic anhydride modified rosin esters, and naturally occurring resins such as gilsonite.1.5 The typical high boiling solvents to be used include C12 to C16 petroleum distillates, 2,2,4 trimethyl 1,3-pentanediol di-isobutyrate,2 alkali refined linseed oil, tridecyl alcohol, or combinations of the above.1.6 To avoid fire or injury, or both, to the operator, these practices should not be used with low flash point solvents such as toluene or xylene. The minimum flash point of the solvents used should be 60°C (140°F) as determined by Test Method D56. (Warning—Users of this practice should be aware that the flash point of many solvents used for this test (as defined in Test Methods D56 and D1310) is exceeded in the heating cycle of this test method. Take safety precautions since there is the potential for vapor ignition. Do the methods outlined in a shielded exhaust hood, where there is access to a fire extinguisher if needed.)1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statement see 25.11.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice provides a means of preparing resin solutions by the “cold cut” method, modeling high-shear production dispersion techniques.1.1 These practices describe laboratory procedures for preparing a solvent or water based ink resin solution in low boiling solvent or alkaline water using two types of lab equipment; (1) an industrial blender (Sections 3 – 7), and (2) a laboratory roller mill (Sections 8 – 12).NOTE 1: ASTM Subcommittee D01.37 recommends using the industrial blender where possible.1.2 These practices use laboratory equipment generally available in a normal, well-equipped laboratory.1.3 These procedures are for use with ink resins intended mainly for liquid (for example, flexographic and rotogravure) inks. The type of resins is typically, but not limited to, acrylic and styrene/acrylic copolymers, polyamides, polyesters, polyvinylbutyral, and maleated/fumarated rosin esters.1.4 The typical low boiling solvents to be used include ethanol, isopropanol, n-propanol, ethyl acetate, isopropyl acetate, and n-propyl acetate. For water based ink resin solutions, water is used in combination with ammonium hydroxide or amines such as dimethylethanolamine, monoethanolamine, and triethylamine.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method has found acceptance in the lithographic ink industry in predicting rheological behavior of a vehicle under press conditions caused by extrusion, shear-thinning rollers and dot gain recovery.5.2 This test method is restricted within the torque limitations and strain resolution of the rheometer used.5.3 Results may not be reproducible if the vehicle is not homogenous.1.1 This test method covers the procedure for determining the viscoelastic properties of printing ink vehicles by measuring the G', G”, and tan delta using a controlled strain cone and plate oscillatory rheometer.1.2 This test method provides the flexibility of using several different types of rheometers to determine viscoelastic properties in ink vehicles.1.3 This test method is not intended for systems that are volatile at procedure temperatures as evaporation may occur effectively changing the percent solids before testing is finished and significantly altering the rheology.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Tinting strength is an essential property of printing ink dispersions. Although test results on wet drawdowns and tints do not guarantee equivalency of dry printed ink films, they provide useful parameters for quality assurance of established formulations, gaging relative degree of dispersion, and estimating the color value of colorants from different batches, sources, or grades.1.1 These test methods cover procedures for determining the relative tinting strength of paste-type printing ink dispersions by visual or instrumental evaluation of tints prepared by manual or automated mixing.1.2 These test methods are applicable to paste-type printing inks, flushed pigments, and other pigment dispersions that are essentially nonvolatile under ordinary room conditions and for which there is a wet reference standard of the same pigmentation and consistency. With proper choice of tinting base, they are applicable to dispersions of any color, including black and white.NOTE 1: The instrumental procedures for tinting strength are similar in principle to those described in Test Methods D387, D2745, D4838, and D6531.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Coarse particles in printing inks reduce the efficiency of the dispersion process, requiring not only extra milling passes, but also frequent changes in pump filters. In printing processes, they may cause excessive wear to metal plates, piling or localized retention of ink on blankets and plates, and water balance problems. Coarse particles also reduce color strength and the gloss of printed matter.4.2 This test method is suitable for quality control. The precision may be improved by the use of a specimen size larger than that prescribed.4.3 Test results are sensitive to the type of washout solvent used. Strong solvents are to be avoided because they may dissolve large particles of resin in the ink vehicle.1.1 This test method covers the determination of the weight concentration of coarse particles in printing ink dispersions by sieve retention.1.2 This test method is applicable to printing inks, flushed pigments, and other pigment dispersions that contain particles larger than 45 μm. With proper choice of solvent, it is applicable both to paste and liquid inks.NOTE 1: This test method is similar in principle to Test Methods D185. For particles under 25 μm, see Test Method D1316.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D2090-98 Standard Test Method for Clarity and Cleanness of Paint and Ink Liquids (Withdrawn 2007) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

1.1 This test method covers a procedure for the visual examination of any unpigmented liquid for use in paints and inks, including fatty oils and acids, drier solutions, solvents, miscellaneous chemicals, varnishes, resin solutions, clear lacquers, and other clear coatings for the presence or absence of undesirable components.1.2 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.>

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3.1 Poor adhesion of ink or coating to the base substrate can impact the readability of printed materials, affect the functionality of coated materials, or create a source of contamination. This practice provides a means for evaluating the adhesion of ink or coating to a flexible packaging material.3.2 For purposes of resolving inter-laboratory disagreements, test methods developed from this practice may be improved by defining and controlling the pressure and method of tape application, (for example, using weighted roller), and the speed and angle of tape removal.3.3 This practice does not address acceptability criteria. These need to be jointly determined by the user and producer of the product.1.1 This practice describes a means of evaluating ink or coating adhesion to flexible packaging materials. This practice is intended for use on flexible packaging materials whose surfaces are not damaged by the application and removal of tape.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Tinting strength is an essential property of printing ink dispersions. Although results on bulk tints do not guarantee equivalency of dry printed films, they provide useful parameters for quality control of production batches of bases and finished inks. Test results may also be used for color matching purposes.1.1 This test method covers the procedure for determining the relative tinting strength of waterbased ink systems using a computer-aided spectrophotometer.1.2 This test method is applicable to waterbased printing inks and bases to be used primarily in flexographic and gravure printing applications.1.3 This test method applies only to single, non-fluorescent pigmented colors and black ink systems for which there is a reference standard containing a pigment of the identical color index name and number.1.4 The procedure in this test method specifies placing tinted samples in a cuvette for spectrophotometric measurements. The use of thick wet drawdowns as in Test Methods D2066 are inappropriate due to severe floating problems with aqueous systems.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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