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5.1 Refer to Guide D8509.1.1 This practice provides instructions for modifying static open-hole tensile and compressive strength test methods to determine the fatigue behavior of composite materials subjected to cyclic tensile or compressive forces, or both. The composite material forms are limited to continuous-fiber reinforced polymer matrix composites in which the laminate is both symmetric and balanced with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1.2 This practice supplements Test Methods D5766/D5766M and D6484/D6484M with provisions for testing specimens under cyclic loading. Several important test specimen parameters, for example fatigue force (stress) ratio, are not mandated by this practice; however, repeatable results require that these parameters be specified and reported.1.3 This practice is limited to test specimens subjected to constant amplitude uniaxial loading, where the machine is controlled so that the test specimen is subjected to repetitive constant amplitude force (stress) cycles. Either engineering stress or applied force may be used as a constant amplitude fatigue variable. The repetitive loadings may be tensile, compressive, or reversed, depending upon the test specimen and procedure utilized.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.4.1 Within the text the inch-pound units are shown in brackets.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Refer to Guide D8509.1.1 This test method determines the open-hole tensile strength of multidirectional polymer matrix composite laminates reinforced by high-modulus fibers. The composite material forms are limited to continuous-fiber or discontinuous-fiber (tape or fabric, or both) reinforced composites in which the laminate is balanced and symmetric with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.2.1 Within the text the inch-pound units are shown in brackets.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 General—Conventional ultrasonics should be considered first for the detection of overt flaws such as delaminations in composites. Thereafter, AU should be considered for composites that are proved to be free of major flaws or discontinuities. The AU method is intended almost exclusively for assessing the collective effects of dispersed defects and subcritical flaw populations. These are material aberrations that influence AU measurements and also underlie mechanical property variations, dynamic load response, and impact and fracture resistance.5.2 Specific Advantages—The AU method can be used to evaluate composite laminate and bond quality using access to only one surface as, for example, the exterior surface of pressure vessels. It is unnecessary to utilize angle beam fixtures because the method can always be applied with probes at normal incidence. The method can be applied using dry coupling with elastomer pads attached to the probes, and there is no need to immerse the examination object in water.5.3 General Applications—The AU method was devised to assess diffuse discontinuity populations and any associated changes of the mechanical properties of composites and composite-like materials. The AU method has been used to evaluate fiber-reinforced composites (6), composite laminates (7), filament-wound pressure vessels (8), adhesive bonds (9), paper and wood products (10), and cable and rope (11). The method has been shown to be particularly practical for assessing the strength of adhesively bonded joints. It has also been shown to be useful for assessing microporosity (12), micro-cracking (13), hydrothermal aging (14), and damage produced by impacts (15) and fatigue (16).1.1 This guide explains the rationale and basic technology for the acousto-ultrasonic (AU) method. Guidelines are given for nondestructive evaluation (NDE) of flaws and physical characteristics that influence the mechanical properties and relative strength of composite structures (for example, filament-wound pressure vessels), adhesive bonds (for example, joints between metal plates), and interlaminar and fiber/matrix bonds in man-made composites and natural composites (for example, wood products).1.2 This guide covers technical details and rules that must be observed to ensure reliable and reproducible quantitative AU assessments of laminates, composites, and bonded structures. The underlying principles, prototype apparatus, instrumentation, standardization, examination methods, and data analysis for such assessments are covered. Limitations of the AU method and guidelines for taking advantage of its capabilities are cited.1.3 The objective of AU is to assess subtle flaws and associated strength variations in composite structures and bonded joints. Discontinuities such as large voids, disbonds, or extended lack of contact at interfaces can be assessed by other NDE methods such as conventional ultrasonics.1.4 Additional information may be found in the publications cited in the list of references at the end of this guide. The referenced works provide background on research, applications, and various aspects of signal acquisition, processing, and interpretation.1.5 Units—The values stated in either SI units or inch-pound units are to be regarded as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standards.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method measures quantitatively the effects of water soaking and drying, and their associated swelling and shrinking stresses on adhesive bonds in overlay-laminated assemblies.4.2 Adhesive bond performance is based on the ability of the adhesive and adhesive bonds to resist delamination during accelerated exposure to water and heat.4.3 Resistance to delamination when subjected to environmental factors is critical to the performance of the laminated assembly in service.4.4 This test method is to be used to determine the quality of adhesive bonds in overlay-wood core laminates after the adhesive has been certified by a specification appropriate for the product, class, and end use.1.1 This test method provides a procedure to determine the quality of bond between an overlay and a wood core in an adhesively bonded laminate. The quality of bond is determined by measuring the resistance to delamination of the adhesively bonded laminate when tested under specific conditions of preparation, conditioning, and testing. Such products include, but are not limited to, window and door components, such as stiles and rails, and other overlaid panels. Typical wood-based cores are finger-jointed lumber, particleboard, oriented strand board, and hardboard. Typical overlays would be veneer, high-pressure laminate, high-density polyethylene, and fiberglass-reinforced plastic.1.2 Adhesive bond performance as measured by resistance to delamination in this test method is suitable for use in adhesive product development, manufacturing quality control, and monitoring bonding processes.1.3 This test method does not provide guidance for determining bond line performance for plywood products.1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The procedure used for etching the copper foil from the base insulating materials may significantly affect the results of electrical tests. This is true primarily for two reasons. First, the geometry of the copper which remains and forms the electrodes is in part determined by the etching procedure; this is particularly true of closely spaced electrodes on the same surface when the property to be measured depends on the electrode geometry. Second, electrical conductance in the material, particularly surface conductance, may be affected by the chemicals used to etch the copper, the length of time of etching, and the manner in which the specimen is cleaned after etching. This practice standardizes the etching procedure in order to provide a basis for comparison of electrical properties of copper-clad electrical insulating materials and thermosetting laminates. Experience has shown that the test circuit can be accurately prepared using this procedure, and that the specimen will be substantially free of etching-induced, electrically-conductive contaminants. It is recognized that commercial processes utilized to manufacture printed circuits may differ appreciably from this practice. Therefore, the results of tests on specimens etched in accordance with this practice may differ from results obtained on specimens etched in a commercial process. Specimens should be etched in accordance with a procedure different from this practice, if it is desired to determine the influence of the different procedure on electrical properties.1.1 This practice describes a procedure for etching and cleaning copper-clad electrical insulating materials and thermosetting laminates for electrical testing.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements see 6.3 and 6.4.

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5.1 Refer to Guide D8509.1.1 This practice provides instructions for modifying static bearing test methods to determine the fatigue behavior of composite materials subjected to cyclic bearing forces. The composite material forms are limited to continuous-fiber reinforced polymer matrix composites in which the laminate is both symmetric and balanced with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1.2 This practice supplements Test Method D5961/D5961M with provisions for testing specimens under cyclic loading. Several important test specimen parameters (for example, fastener selection, fastener installation method, and fatigue force/stress ratio) are not mandated by this practice; however, repeatable results require that these parameters be specified and reported.1.3 This practice is limited to test specimens subjected to constant amplitude uniaxial loading, where the machine is controlled so that the test specimen is subjected to repetitive constant amplitude force (stress) cycles. Either engineering stress or applied force may be used as a constant amplitude fatigue variable. The repetitive loadings may be tensile, compressive, or reversed, depending upon the test specimen and procedure utilized.1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.4.1 Within the text the inch-pound units are shown in brackets.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers twelve grades of thermosetting laminate with copper foil cladded to one or both surfaces. These combination forms are intended primarily for use in fabrication of printed (etched) wiring or circuit boards. The laminates shall meet the following requirements: peel strength after solder float and at elevated temperature conditions; lengthwise and crosswise flexural strengths; flammability rating; water absorption; volume resistivity; dielectric breakdown parallel to laminations; dissipation factor; and permittivity. Warp or twist, and blistering requirements shall also be tested for conformance.1.1 This specification covers twelve grades of thermosetting laminate with copper foil bonded to one or both surfaces. These combination forms are intended primarily for use in fabrication of printed (etched) wiring or circuit boards.1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 Flexure tests on flat sandwich panel construction may be conducted to determine facesheet scarf or step joint compressive strength.5.2 This practice is limited to obtaining the compressive strength of the sandwich panel scarf and step joint facesheets. Due to the curvature of the flexural test specimen when loaded, facesheet compression strength from this test may not be equivalent to the facesheet compression strength of sandwich structures subjected to pure edgewise (in-plane) compression.5.3 Factors that influence the compressive response and should therefore be reported include the following: materials (laminate facesheet, core, and adhesive); methods of material fabrication; methods of material preparation, including surface preparation prior to bonding, lay-up, specimen facesheet stacking sequence, and overall thickness; core geometry (cell size); core density; adhesive thickness; joint taper ratio or step length; ply overlap length; relative thickness and stiffness of parent and repair laminates; adhesive bond stiffness; specimen preparation; specimen conditioning; environment of testing; specimen alignment; speed of testing; time at temperature; void content; and volume percent reinforcement. Properties, in the test direction, which may be obtained from this practice, include the following:5.3.1 Ultimate compressive strength (based on the nominal repair material thickness), (Frcu).5.3.2 Ultimate running load per ply, (Nj).NOTE 2: Concentrated forces on beams with thin facesheets and low density cores can produce results that are difficult to interpret, especially close to the failure point. Wider loading blocks and rubber pads may assist in distributing the forces.NOTE 3: To ensure that simple sandwich beam theory is valid, a good rule of thumb for the four-point bending test is the support span length divided by the sandwich thickness should be greater than 20 (S/d > 20) with the ratio of repair material facesheet thickness to core thickness less than 0.1 (hr/c < 0.1).1.1 This practice covers the procedure for determination of the compressive strength of a tapered or stepped bonded joint of polymer matrix composite materials. It is applicable to secondary bonded or co-bonded laminates with either unidirectional plies or woven fabric reinforcements. The materials to be bonded may be different systems. In the bondline, a separate adhesive material may or may not be used (example: adhesives may be used with a prepreg system or may not be used with a wet lay-up repair system). The range of acceptable test laminates and thicknesses are described in 8.2.7. The standard repair types are the same as for the tensile loading in Practice D8131/D8131M. While external patch repairs are not explicitly covered in this practice, these repairs could be tested as a non-standard specimen using this practice.1.2 This practice supplements Test Method D7249/D7249M for compressive loading of facesheet sandwich constructions by long beam flexure. Several important test specimen parameters (for example, joint length, ply overlaps, step depth, and taper ratio) are not mandated by this practice; however, these parameters are required to be specified and reported to support repeatable results.1.3 Unidirectional (0° ply orientation) composites as well as multi-directional composite laminates and fabric composites, can be tested.1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.4.1 Within the text, the inch-pound units are shown in brackets.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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