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5.1 The soil-lime pH test is performed as a test to indicate the soil-lime proportion needed to maintain the elevated pH necessary for sustaining the reactions required to stabilize a soil. The test derives from Eades and Grim.45.2 Performance tests are normally conducted in a laboratory to verify the results of this test method.5.3 This test method will not provide reliable information relative to the potential reactivity of a particular soil, nor will it provide information on the magnitude of increased strength to be realized upon treatment of this soil with the indicated percentage of lime.5.4 This test method can be used to estimate the percentage of lime as hydrated lime or quicklime needed to produce a lime stabilized soil. Common candidate soils contain clay minerals and have a Plasticity Index ≥10.5.5 Agricultural lime (crushed limestone) will not stabilize soil.NOTE 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method provides a means for estimating the soil-lime proportion requirement for stabilization of a soil. This test method is performed on soil passing the 425μm (No. 40) sieve. The optimum soil-lime proportion for soil stabilization is determined by tests of specific characteristics of stabilized soil such as unconfined compressive strength or plasticity index.1.2 Some highly alkaline by-products (lime kiln dust, cement kiln dust, carbide lime, and so forth) have been successfully used to stabilize soil. This test method is not intended for these materials and any such product would need to be tested for specific characteristics as indicated in 1.1.1.3 This test method is used to determine the percentage of lime that results in a soil-lime pH of approximately 12.4.NOTE 1: Under ideal laboratory conditions of 25°C and sea level elevation, the pH of the lime-soil-water solution should be 12.4.1.4 Lime is not an effective stabilizing agent for all soils. Some soil components such as sulfates, phosphates, organics, and iron can adversely affect soil-lime reactions and may produce erroneous results using this test method.1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.1.6.1 The procedures used to specify how data are collected/ recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis for engineering data.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This specification covers hydraulic hydrated lime for structural purposes. Hydraulic hydrated lime may be used in the scratch or brown coat of plaster, stucco, mortar, or in Portland-cement concrete either as blend, amendment, or admixture. The hydraulic hydrated lime shall conform to the chemical composition requirements for calcium oxide, magnesium oxide, silica, iron oxide, aluminum oxide, and carbon dioxide. The sample shall be subjected to the following test methods: chemical analysis; fineness; normal consistency; time of setting; autoclave expansion; and compressive strength.1.1 This specification covers hydrated hydraulic lime for structural purposes.1.2 Hydrated hydraulic lime may be used in the scratch or brown coat of plaster, stucco, mortar, or in portland-cement concrete either as blend, amendment, or admixture.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. Within the text, the inch-pound units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.4 The following precautionary caveat pertains only to the test method portion, Section 11 of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods can be used to ensure that the chemical composition of the glass meets the compositional specification required for the finished glass product.3.2 These test methods do not preclude the use of other methods that yield results within permissible variations. In any case, the analyst should verify the procedure and technique employed by means of a National Institute of Standards and Technology (NIST) standard reference material having a component comparable with that of the material under test. A list of standard reference materials is given in the NIST Special Publication 260,3 current edition.3.3 Typical examples of products manufactured using soda-lime silicate glass are containers, tableware, and flat glass.3.4 Typical examples of products manufactured using borosilicate glass are bakeware, labware, and fiberglass.3.5 Typical examples of products manufactured using fluoride opal glass are containers, tableware, and decorative glassware.1.1 These test methods cover the quantitative chemical analysis of soda-lime and borosilicate glass compositions for both referee and routine analysis. This would be for the usual constituents present in glasses of the following types: (1) soda-lime silicate glass, (2) soda-lime fluoride opal glass, and (3) borosilicate glass. The following common oxides, when present in concentrations greater than indicated, are known to interfere with some of the determinations in this method: 2 % barium oxide (BaO), 0.2 % phosphorous pentoxide (P2O5), 0.05 % zinc oxide (ZnO), 0.05 % antimony oxide (Sb2O3), 0.05 % lead oxide (PbO).1.2 The analytical procedures, divided into two general groups, those for referee analysis, and those for routine analysis, appear in the following order:    SectionsProcedures for Referee Analysis:    Silica 10  BaO, R2O2 (Al2O3 + P2O5), CaO, and MgO 11 – 15  Fe2O3, TiO2, ZrO2 by Photometry and Al2O3 by Com-     plexiometric Titration 16 – 22  Cr2O3 by Volumetric and Photometric Methods 23 – 25  MnO by the Periodate Oxidation Method 26 – 29  Na2O by the Zinc Uranyl Acetate Method and K2O by     the Tetraphenylborate Method 30 – 33  SO3 (Total Sulfur) 34 – 35  As2O3 by Volumetric Method 36 – 40     Procedures for Routine Analysis:    Silica by the Single Dehydration Method 42 – 44  Al2O3, CaO, and MgO by Complexiometric Titration,     and BaO, Na2O, and K2O by Gravimetric Method 45 – 51  BaO, Al2O3, CaO, and MgO by Atomic Absorption; and     Na2O and K2O by Flame Emission Spectroscopy 52 – 59  SO3 (Total Sulfur) 60  B2O3 61 – 62  Fluorine by Pyrohydrolysis Separation and Specific Ion     Electrode Measurement 63 – 66  P2O5 by the Molybdo-Vanadate Method 67 – 70  Colorimetric Determination of Ferrous Iron Using 1,10     Phenanthroline 71 – 76     1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 These test methods provide accurate and reliable analytical procedures to determine the chemical constituents of limestone, quicklime, and hydrated lime (see Note 1). The percentages of specific constituents which determine a material's quality or fitness for use are of significance depending upon the purpose or end use of the material. Results obtained may be used in relation to specification requirements.4.2 Because quicklime and hydrated lime quickly absorb water and carbon dioxide from the air, precision and bias are extremely dependent upon precautions taken during sample preparation and analysis to minimize excessive exposure to ambient conditions.NOTE 1: These test methods can be applied to other calcareous materials if provisions are made to compensate for known interferences.1.1 These test methods cover the chemical analysis of high-calcium and dolomitic limestone, quicklime, and hydrated lime. These test methods are classified as either standard (preferred) or alternative (optional).1.2 The standard test methods are those that employ classical gravimetric or volumetric analytical procedures and are typically those required for referee analyses where chemical specification requirements are an essential part of contractual agreement between buyer and seller.1.3 Alternative or optional test methods are provided for those who wish to use procedures shorter or more convenient than the standard methods for the routine determinations of certain constituents. Optional test methods may sometimes be preferred to the standard test methods, but frequently the use of modern and expensive instrumentation is indicated which may not be accessible to everyone. Therefore, the use of these test methods must be left to the discretion of each laboratory.1.4 The analytical procedures appear in the following order:  Section     Aluminum Oxide  15     Available Lime Index  28     Calcium and Magnesium Oxide:      Alternative EDTA Titration Method  31     Calcium Carbonate Equivalent  33     Calcium Oxide:      Gravimetric Method  16      Volumetric Method  17     Carbon Dioxide by Standard Method  22     Combined Oxides of Iron and Aluminum  12     Ferrous Iron  Appendix X5     Free Calcium Oxide  Appendix X6     Free Moisture in Hydrated Lime  21     Free Moisture in Limestone  20     Free Silica  29     Insoluble Matter Including Silicon Dioxide:      Standard Method   8      Optional Perchloric Acid Method   9     Insoluble Matter Other Than Silicon Dioxide  11     Loss on Ignition  19     Magnesium Oxide  18     Manganese:      Bismuthate Method  Appendix X4      Periodate (Photometric) Method  27     pH Determination of Alkaline Earth Solutions  34     Phosphorus:      Titrimetric Method  Appendix X3      Molybdovanadate Method  26     Silicon Dioxide  10     Strontium Oxide  Appendix X2     Sulfur Trioxide  23     Total Carbon:      Direct Combustion-Thermal Conductivity Cell      Method 32     Total Carbon and Sulfur:      Combustion/Infrared Detection Method  35     Total Iron:      Standard Method, Potassium Dichromate      Titration  13      Potassium Permanganate Titration Method  Appendix X1      Ortho-Phenanthroline, Photometric Method  14     Total Sulfur:      Sodium Carbonate Fusion  24      Combustion-Iodate Titration Method  25      Unhydrated Oxides  301.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 9.3, 10.2.1, 18.4.3, 31.6.4.2, X2.3.1, and X5.4.1.1.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This practice is designed to present in a standardized format information on the variability of limestone or lime from a single source over a period of time. It can be applied to all materials covered in Test Methods C25, C110, C1271, and C1301, and Specification C141.1.1 This practice is intended for use in instances where the purchaser desires information on the uniformity of limestone or lime produced at a single source. It is intended that this test method normally be used for the predominant material manufactured at a plant. Guidelines for sampling, testing and presentation of results (Table 1) are given.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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From these tests the relative expansive potential of soil-lime mixtures containing varying amounts of lime can be evaluated. From such an evaluation, the amount of lime required to reduce expansion to acceptable levels can be determined. The data can then be used for the design and specification requirements for subgrades and structural fills where expansive soils are encountered and it is desired to give a certain degree of expansion-shrinkage control to structure foundations and road subgrades. The tests will also show if the specific soils are amenable to lime stabilization.Note 2—The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 These test methods provide procedures for conducting expansion, shrinkage, and uplift pressure tests on compacted soil-lime mixtures and can be used to determine the lime content required to achieve desired control of volume changes caused by increases or decreases of moisture.1.2 The tests can be used to determine (a) the magnitude of volume changes under varying load conditions, (b) the rate of volume change, and (c) the magnitude of pressure change as moisture changes of the soil-lime mixture take place. The permeability of soil-lime mixture can also, if desired, be determined at the various load conditions.Note 1—Changes in field conditions can have major effects on the expansion and shrinkage characteristics of expansive soils. Therefore, to the greatest extent possible, initial and anticipated future field conditions should be duplicated, particularly with respect to moisture and density.1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, D37401.3.1 The method used to specify how data are collected, calculated, or recorded in this standard is not directly related to the accuracy to which the data can be applied in design or other uses, or both. How one applies the results obtained using this standard is beyond its scope.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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定价: 515元 / 折扣价: 438 加购物车

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This specification covers four types of pozzolanic hydraulic lime for structural purposes which include use in mortar, scratch, brown, and finish (stucco) coats of interior or exterior plaster. The four types of pozzolanic hydraulic lime are classified according to the minimum hydrated lime content, maximum hydraulic cement content, and specific performance requirements. Test specimens shall be stored in a moist room or cabinet wherein the storage surface shall be in equilibrium with the space to ensure no moisture loss. The specimens shall be subjected to testing to determine conformance to the following requirements: water soluble alkali, sulfur trioxide content, carbon dioxide content, fineness, maximum time of initial and final set, autoclave expansion, air content, water retention, and compressive strength.1.1 This standard covers four types of pozzolanic hydraulic lime for structural purposes which include use in mortar, scratch, brown, and finish (stucco) coats of interior or exterior plaster.1.1.1 PHL—Pozzolanic hydraulic lime for use in mortar, scratch, brown, and finish (stucco) coats of interior or exterior plaster.1.1.2 PHLc—PHL with a maximum 20 % binder weight of hydraulic cement.1.1.3 PHL-A—Air-entrained PHL.1.1.4 PHLc-A—Air-entrained PHLc.1.2 The values stated in SI units are to be regarded as standard.1.3 This specification classifies pozzolanic hydraulic lime by minimum hydrated lime content, maximum hydraulic cement content, and specific performance requirements.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

定价: 515元 / 折扣价: 438 加购物车

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定价: 515元 / 折扣价: 438 加购物车

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5.1 This test method is useful for the determination of elemental concentrations in the range of approximately 0.1 µgg-1 to 10 percent (%) (See Table X1.1) in soda-lime glass samples (7 and 8). A standard test method can aid in the interchange of data between laboratories and in the creation and use of glass databases.5.2 The determination of elemental concentrations in glass provides high discriminating value in the forensic comparison of glass fragments.5.3 This test method produces minimal destruction of the sample. Microscopic craters of 50 µm to 100 µm in diameter by 80 µm to 150 µm deep are left in the glass fragment after analysis. The mass removed per replicate is approximately 0.4 µg to 3 µg (6).5.4 Appropriate sampling techniques shall be used to account for natural heterogeneity of the materials at a microscopic scale.5.5 The precision, bias, and limits of detection of the method (for each element measured) shall be established during validation of the method. The measurement uncertainty of any concentration value used for a comparison shall be recorded with the concentration.5.6 Acid digestion of glass followed by either Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) or Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) can also be used for trace elemental analysis of glass, and offer similar detection levels and the ability for quantitative analysis. However, these methods are destructive, and require larger sample sizes and more sample preparation (Test Method E2330).5.7 Micro X-Ray Fluorescence (µ-XRF) uses comparable sample sizes to those used for LA-ICP-MS with the advantage of being non-destructive of the sample. Some of the drawbacks of µ-XRF include lower sensitivity and precision, and longer analysis time (Test Method E2926).5.8 Scanning Electron Microscopy with Energy Dispersive Spectrometry (SEM-EDS) is also available for elemental analysis, but it is of limited use for forensic glass source discrimination due to poor detection limits for higher atomic number elements present in glass at trace concentration levels. However, distinguishing between sources having similar RIs and densities is sometimes possible.1.1 This test method covers a procedure for the quantitative elemental analysis of the following seventeen elements: lithium (Li), magnesium (Mg), aluminum (Al), potassium (K), calcium (Ca), iron (Fe), titanium (Ti), manganese (Mn), rubidium (Rb), strontium (Sr), zirconium (Zr), barium (Ba), lanthanum (La), cerium (Ce), neodymium (Nd), hafnium (Hf) and lead (Pb) through the use of laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) for the forensic comparison of glass fragments. The potential of these elements to provide the best discrimination among different sources of soda-lime glasses has been published elsewhere (1-5).2 Silicon (Si) is also monitored for use as a normalization standard. Additional elements may be added as needed, for example, tin (Sn) can be used to monitor the orientation of float glass fragments.1.2 The method only consumes approximately 0.4 µg to 3 µg of glass per replicate and is suitable for the analysis of full thickness samples as well as irregularly shaped fragments as small as 0.1 mm by 0.1 mm by 0.2 mm (6) in dimension. The concentrations of the elements listed above range from the low parts per million (µgg-1) to percent (%) levels in soda-lime glass, the most common type encountered in forensic cases. This standard method can be applied for the quantitative analysis of other glass types; however, some modifications in the reference standard glasses and the element menu may be required.1.3 This standard is intended for use by competent forensic science practitioners with the requisite formal education, discipline-specific training (see Practice E2917), and demonstrated proficiency to perform forensic casework.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3155-11 Standard Test Method for Lime Content of Uncured Soil-Lime Mixtures (Withdrawn 2020) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

This test method can be used to determine the lime content of uncured soil-lime mixtures.Lime content in soil-lime mixtures is needed by agencies such as highway departments, to determine lime content in soil-lime mixtures for payments to contractors, to check compliance with specifications, or to check the efficacy of quality control measures.Lime content is also needed by producers of soil-lime mixtures who have to determine lime content for production control purposes.Note 1—The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.1.1 This test method covers the determination of the lime content of soil-lime mixtures sampled from a project under construction or at the pug-mill, or both.1.2 In soils with highly variable amounts of CaCo3 (such as caliche), it may be difficult to obtain a representative sample.1.3 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are provided for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This terminology refers to the terms relating to lime and limestone products as used by the industry.1.2 Where appropriate, the various terms defined below should be prefixed with one or other of the adjectives “high-calcium,” “magnesian,” or “dolomitic.” (Examples: dolomitic quicklime; high-calcium hydraulic hydrated lime; magnesian or dolomitic limestone.)1.3 The composition of a limestone should be given in terms of a percentage of the carbonates present. In limestone of interest to the lime industry, it is usually assumed that the material consists almost entirely of carbonates. Where this assumption is not valid, the percentage of noncarbonate material should be determined, and the composition expressed in terms of the carbonate material present.1.4 For specific application of lime or a limestone product, see the appropriate ASTM specification.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C206-14(2022) Standard Specification for Finishing Hydrated Lime Active 发布日期 :  1970-01-01 实施日期 : 

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