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4.1 These test methods are intended for use as control and acceptance tests. They are also applicable in the partial evaluation of materials for specific end uses and as a means for detecting changes in materials due to specific deteriorating causes.4.2 The steps involved in running this method are:4.2.1 Calibration of the viscometers,4.2.2 Preparation of solutions,4.2.3 Determination of efflux time,4.2.4 Calculation of relative viscosity (which requires the following),4.2.4.1 Determining the density of the polymer/formic acid solution, and4.2.4.2 Determining the absolute viscosity of the formic acid used.4.3 Solvents used to prepare concentrated solutions for use in this test method are formic acid (9.2.6.1) and m-cresol (9.2.6.2).4.4 Solvents used to prepare dilute solutions of various polyamides are designated in ASTM D6779, ISO 16396, and ISO 307. These include:4.4.1 Formic Acid—PA 6, PA 46, PA 66, PA 69, PA 610, PA MXD6 and corresponding copolyamides4.4.2 Sulfuric Acid—PA 6, PA 46, PA 66, PA 69, PA 610, PA 612, PA MXD6 and corresponding copolyamides4.4.3 m-cresol—PA 612, PA1010, PA1012, PA 11, PA 12, PA1212, PA 11/12 copolymers, PA 6T/66, PA 6I/66, PA 6I/6T, PA 6T/6I/66, PA 6T/6I, PA 6I/6T/664.4.4 Phenol/1,1,2,2-tetrachloroethane (where legal)—PA 6T/66, PA 6I/66, PA 6I/6T, PA 6T/6I/66, PA 6T/6I, PA 6I/6T/66, PA 6T/66, PA 6I/66, PA 6I/6T, PA 6T/6I/66, PA 6T/6I, PA 10T PA 6I/6T/66, PPA and copolyamides1.1 This test method covers the determination of relative viscosity as it applies to concentrated solutions of polyamide (PA).1.2 This test method does not address measures of viscosity derived from measurements with dilute solutions.1.3 The values stated in SI units are to be regarded as standard. The values given in brackets are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 1: This standard and ISO 307 address the same subject, buy the technical content is different.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Accurate determination of the density, relative density (specific gravity), or API gravity of petroleum and its products is necessary for the conversion of measured volumes to volumes or masses, or both, at the standard reference temperatures of 15 °C or 60 °F during custody transfer.5.2 This procedure is most suitable for determining the density, relative density (specific gravity), or API gravity of low viscosity transparent liquids. This procedure can also be used for viscous liquids by allowing sufficient time for the hydrometer to reach temperature equilibrium, and for opaque liquids by employing a suitable meniscus correction. Additionally for both transparent and opaque fluids the readings shall be corrected for the thermal glass expansion effect and alternative calibration temperature effects before correcting to the reference temperature.5.3 When used in connection with bulk oil measurements, volume correction errors are minimized by observing the hydrometer reading at a temperature close to that of the bulk oil temperature.5.4 Density, relative density, or API gravity is a factor governing the quality and pricing of crude petroleum. However, this property of petroleum is an uncertain indication of its quality unless correlated with other properties.5.5 Density is an important quality indicator for automotive, aviation and marine fuels, where it affects storage, handling and combustion.1.1 This test method covers the laboratory determination using a glass hydrometer in conjunction with a series of calculations, of the density, relative density, or API gravity of crude petroleum, petroleum products, or mixtures of petroleum and nonpetroleum products normally handled as liquids, and having a Reid vapor pressure of 101.325 kPa (14.696 psi) or less. Values are determined at existing temperatures and corrected to 15 °C or 60 °F by means of a series of calculations and international standard tables.1.2 The initial hydrometer readings obtained are uncorrected hydrometer readings and not density measurements. Readings are measured on a hydrometer at either the reference temperature or at another convenient temperature, and readings are corrected for the meniscus effect, the thermal glass expansion effect, alternative calibration temperature effects and to the reference temperature by means of the Petroleum Measurement Tables; values obtained at other than the reference temperature being hydrometer readings and not density measurements.1.3 Readings determined as density, relative density, or API gravity can be converted to equivalent values in the other units or alternative reference temperatures by means of Interconversion Procedures (API MPMS Chapter 11.5), or Adjunct to D1250 Guide for Petroleum Measurement Tables (API MPMS Chapter 11.1), or both, or tables, as applicable.1.4 The initial hydrometer readings determined in the laboratory shall be recorded before performing any calculations. The calculations required in Section 10 shall be applied to the initial hydrometer reading with observations and results reported as required by Section 11 prior to use in a subsequent calculation procedure (ticket calculation, meter factor calculation, or base prover volume determination).1.5 Annex A1 contains a procedure for verifying or certifying the equipment for this test method.1.6 The values stated in SI units are to be regarded as standard.1.6.1 Exception—The values given in parentheses are provided for information only.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The heating value is a measure of the suitability of a pure gas or a gas mixture for use as a fuel; it indicates the amount of energy that can be obtained as heat by burning a unit of gas. For use as heating agents, the relative merits of gases from different sources and having different compositions can be compared readily on the basis of their heating values. Therefore, the heating value is used as a parameter for determining the price of gas in custody transfer. It is also an essential factor in calculating the efficiencies of energy conversion devices such as gas-fired turbines. The heating values of a gas depend not only upon the temperature and pressure, but also upon the degree of saturation with water vapor. However, some calorimetric methods for measuring heating values are based upon the gas being saturated with water at the specified conditions.5.2 The relative density (specific gravity) of a gas quantifies the density of the gas as compared with that of air under the same conditions.1.1 This practice covers procedures for calculating heating value, relative density, and compressibility factor at base conditions (14.696 psia and 60°F (15.6°C)) for natural gas mixtures from compositional analysis.2 It applies to all common types of utility gaseous fuels, for example, dry natural gas, reformed gas, oil gas (both high and low Btu), propane-air, carbureted water gas, coke oven gas, and retort coal gas, for which suitable methods of analysis as described in Section 6 are available. Calculation procedures for other base conditions are given.1.2 The values stated in inch-pound units are to be regarded as the standard. The SI units given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Insulating materials are used to isolate components of an electrical system from each other and from ground, as well as to provide mechanical support for the components. For this purpose, it is generally desirable to have the insulation resistance as high as possible, consistent with acceptable mechanical, chemical, and heat-resisting properties. Since insulation resistance or conductance combines both volume and surface resistance or conductance, its measured value is most useful when the test specimen and electrodes have the same form as is required in actual use. Surface resistance or conductance changes rapidly with humidity, while volume resistance or conductance changes slowly although the final change may eventually be greater.4.2 Resistivity or conductivity is used to predict, indirectly, the low-frequency dielectric breakdown and dissipation factor properties of some materials. Resistivity or conductivity is often used as an indirect measure of moisture content, degree of cure, mechanical continuity, and deterioration of various types. The usefulness of these indirect measurements is dependent on the degree of correlation established by supporting theoretical or experimental investigations. A decrease of surface resistance will result either in an increase of the dielectric breakdown voltage because the electric field intensity is reduced, or a decrease of the dielectric breakdown voltage because the area under stress is increased.4.3 All the dielectric resistances or conductances depend on the length of time of electrification and on the value of applied voltage (in addition to the usual environmental variables). These must be known to make the measured value of resistance or conductance meaningful.4.4 Volume resistivity or conductivity is used as an aid in designing an insulator for a specific application. The change of resistivity or conductivity with temperature and humidity may be great, and must be known when designing for operating conditions. Volume resistivity or conductivity determinations are often used in checking the uniformity of an insulating material, either with regard to processing or to detect conductive impurities that affect the quality of the material and that may not be readily detectable by other methods.4.5 Volume resistivities above 1021 Ω·cm (1019 Ω·m), obtained on specimens under usual laboratory conditions, are of doubtful validity, considering the limitations of commonly used measuring equipment.4.6 Surface resistance or conductance cannot be measured accurately, only approximated, because some degree of volume resistance or conductance is always involved in the measurement. The measured value is also affected by the surface contamination. Surface contamination, and its rate of accumulation, is affected by many factors including electrostatic charging and interfacial tension. These, in turn, may affect the surface resistivity. Surface resistivity or conductivity can be considered to be related to material properties when contamination is involved but is not a material property in the usual sense.1.1 These test methods cover procedures for testing adhesives in liquid, highly viscous, solid, or set states, that are intended to be cured by electronic heating, or that are intended to provide electrical insulation, or that are intended for use in electrical apparatus.1.2 The procedures appear in the following order:(1) Procedure for Testing Adhesives Before Use:  SectionPower Factor and Dielectric Constant of Liquid Adhesives  7Direct-Current Conductivity  8Extract Conductivity  9Acidity and Alkalinity 10pH Value 11(2) Procedures for Testing Properties of Adhesives As Used:  SectionPower Factor and Dielectric Constant of a Dried or Cured Adhesive  Film  12Dielectric Strength 13Volume and Surface Resistivity 14Arc Resistance 151.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see 8.2.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This classification establishes categories of insulating coatings based on their chemical nature, relative insulating ability, and typical applications. These categories describe general physical and chemical characteristics of the coatings that are useful in making broad estimates of their insulating ability and suitability for various applications.1.1 This document classifies insulating coatings for electrical steels according to their composition, relative insulating ability, and functionality. The purpose of this classification is to assist users of insulating coatings by providing general information about the chemical nature and use of the coatings, as well as to provide important data concerning limits to their use, that is, relative insulating ability, punchability, temperature stability, weldability, and fabricability. Specific surface insulation resistivity values for each coating are not included in this classification. The user is referred to the flat-rolled electrical steel specifications noted in 1.2 should more detailed information concerning surface insulation resistivity values be required.1.2 This classification is to be used in conjunction with the various specifications for flat-rolled electrical steels under the jurisdiction of Committee A06, including Specifications A345, A677, A683, A726, A840, A876, and A1086. However, in those instances in which the coating descriptions and characteristics differ between this classification and any of the specifications, this classification shall supersede the specification.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to customary (cgs-emu and inch-pound) units which are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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The content of dissolved decay products in insulating oils is made up of a variety of compounds, such as peroxides, aldehydes, ketones, and organic acids. Each of them is partially adsorbed on the large surface of paper insulation leading to the premature aging of power transformers. The relative assessment of byproduct formation, therefore, can be used as an indicator of the aging of the mineral oil.1.1 This test method characterizes by spectrophotometry the relative level of dissolved decay products in mineral insulating oils of petroleum origin. While new oil is almost transparent to a monochromatic beam of light in the visible spectrum, the increasing concentration of dissolved decay products shift the absorbance curve to longer wavelengths.1.2 This test method is applicable to compare the extent of dissolved decay products for oils in service. It can assess the effectiveness of used or stored oil purification during the reclamation process, as well.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

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5.1 Workability is one of the main factors that influence the compaction quality and ultimately the performance of asphalt pavement. This method uses the relative rotation measured by the wireless particle-size sensor to evaluate the workability of the asphalt mixture.5.2 This test method is used to generate information concerning the workability of an asphalt mixture. Workability characteristics, in turn, can give users insight as to how the mixture will handle and compact in the field.5.3 This method is used to evaluate workability of the mix in a situation where it is being used for research or mix design. It is not intended to be a quality control (QC) evaluation.5.4 This test method can be used to evaluate conventional and modified asphalt mixtures to achieve the best workability at an appropriate compaction temperature. The test method can be used to determine the compaction temperature and optimal dosage rate of additives or modifiers to achieve the best workability for the modified asphalt mixtures, such as polymer modified, crumb rubber modified, waste plastic modified, etc.5.5 This test method is appropriate for laboratory-produced mixtures and plant-produced mixtures, regardless of the type or grade of the binder, the type or gradation of the aggregates, and whether RAP, WMA additives, or other modifiers are used in the asphalt mixture.NOTE 1: The quality of the results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.1.1 This test method covers the determination of relative rotation to evaluate the workability of asphalt mixture during compaction using a wireless particle-size sensor. It is applicable to asphalt mixture being compacted using the Superpave Gyratory Compactor (SGC).1.2 This test method is appropriate for use to determine the relative rotation of laboratory-produced and plant-produced asphalt mixtures, regardless of the type or gradation of the aggregates, and whether reclaimed asphalt pavement (RAP), warm mix asphalt (WMA) additives, or any type of modifiers are used in the asphalt mixture.1.3 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered requirements of the standard.1.5 Since a complete precision and bias statement for this standard has not been developed, the test method is to be used for research and informational purposes only. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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