4.1 This test method is used to determine the amount of expansion of a mortar bar when it is stored in water. The amount of mortar-bar expansion may relate to the amount of sulfate in the cement; expansion may become excessive when the cement contains too much sulfate.4.2 Some cement specifications limit the amount of sulfate contained in hydraulic cement by requiring that the amount of expansion in water not exceed a specified value.1.1 This test method covers the determination of the expansion of mortar bars made using hydraulic cement, of which sulfate is an integral part.1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Coefficients of linear thermal expansion are used, for example, for design purposes and to determine if failure by thermal stress may occur when a solid body composed of two different materials is subjected to temperature variations.5.2 This test method is comparable to Test Method D3386 for testing electrical insulation materials, but it covers a more general group of solid materials and it defines test conditions more specifically. This test method uses a smaller specimen and substantially different apparatus than Test Methods E228 and D696.5.3 This test method may be used in research, specification acceptance, regulatory compliance, and quality assurance.1.1 This test method determines the technical coefficient of linear thermal expansion of solid materials using thermomechanical analysis techniques.1.2 This test method is applicable to solid materials that exhibit sufficient rigidity over the test temperature range such that the sensing probe does not produce indentation of the specimen.1.3 The recommended lower limit of coefficient of linear thermal expansion measured with this test method is 5 μm/(m·°C). The test method may be used at lower (or negative) expansion levels with decreased accuracy and precision (see Section 11).1.4 This test method is applicable to the temperature range from −120 °C to 900 °C. The temperature range may be extended depending upon the instrumentation and calibration materials used.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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