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3.1 This guide provides techniques for obtaining representative samples of oil and water mixtures. This information is necessary in the calculation of oil recovery efficiency and oil recovery rates for oil collection devices.3.2 Sampling Stationary Mixtures—When recovered oil/water mixtures are contained within a holding tank and the relative oil content of the recovered fluid is needed, the sampling technique is somewhat dependent on the container. Two techniques are outlined in this guide. If the container has a flat bottom with straight sides perpendicular to the base (or nearly so), either stationary technique can be implemented, with the stratified sampling method preferred. If the container is irregular in either the horizontal or vertical cross section, the mixing method is preferred.3.3 Sampling Flowing Mixtures—To sample flowing mixtures containing both oil and water, turbulence is induced, to create a homogenous mixture while sampling. The oil content in the sample taken from the flowing stream can then be used to quantify the performance-rating criterion (see Procedure Section of Test Method D1796).1.1 This guide is intended for sampling flowing or stationary oil/water mixtures. It is intended for use with oil spill recovery devices either in testing or in documentation of field performance.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Purgeable organic compounds, including organohalides, have been identified as contaminants in raw and drinking water. These contaminants may be harmful to the environment and man. Dynamic headspace sampling is a generally applicable method for concentrating these components prior to gas chromatographic analysis (1-5).3 This test method can be used to quantitatively determine purgeable organic compounds in raw source water, drinking water, and treated effluent water.1.1 This test method covers the determination of most purgeable organic compounds that boil below 200°C and are less than 2 % soluble in water. It covers the low μg/L to low mg/L concentration range (see Section 15 and Appendix X1).1.2 This test method was developed for the analysis of drinking water. It is also applicable to many environmental and waste waters when validation, consisting of recovering known concentrations of compounds of interest added to representative matrices, is included.1.3 Volatile organic compounds in water at concentrations above 1000 μg/L may be determined by direct aqueous injection in accordance with Practice D2908.1.4 It is the user's responsibility to assure the validity of the test method for untested matrices.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 8.5.5.1.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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