4.1 A supply well provides groundwater for household, domestic, commercial, agricultural, or industrial uses.4.2 Using a standardized protocol based on an existing industry standard or approved regulatory methods and procedures to collect water samples from a supply well is essential to obtain representative water quality data. These data can be critical to efforts to protect water uses, and human health, and identify changes when they occur. Use of this guide will help the project team to design and execute an effective water supply sampling program.4.3 It is important to understand the objectives of the sampling program before designing it. Water supplies may be sampled for various reasons including any or all of the following:(1) baseline sampling before an operation of concern,(2) periodic sampling during such an operation,(3) investigative responses to perceived changes in water quality, or(4) ongoing monitoring related to known or potential groundwater constituents of concern in the area.Sampling programs should be based on these objectives and be developed in coordination with the prospective laboratory(ies) to ensure its procedures, capabilities, and limitations meet the needs of the program, protect human health and fulfill regulatory requirements.1.1 This guide presents a methodology for obtaining representative groundwater samples from domestic or commercial water wells that are in proximity to oil and gas exploration and production (E&P) operations. E&P operations include, but are not necessarily limited to, site preparation, drilling, completion, and well stimulation (including hydraulic fracturing), and production activities. The goal is to obtain representative groundwater samples from domestic or commercial water wells that can be used to identify the baseline groundwater quality and any subsequent changes that may be identified. While this guide focuses on baseline sampling in conjunction with oil and gas E&P activities, the principles and practices recommended are based on well-established methods that have been in use for many years in other industrial situations. This guide recommends sampling and analytical testing procedures that can identify various chemical species present including metals, dissolved gases (such as methane), hydrocarbons (and other organic compounds), as well as overall water quality.1.2 This guide provides information on typical residential and commercial water supply well systems and guidance on developing and implementing a sampling program, including determining sampling locations, suggested purging techniques, selection of potential analyses and laboratory certifications, data management, and integrity. It also includes guidance on personal safety. The information included pertains to baseline sampling before beginning any activities that could present potential risks to local aquifers, periodic sampling during and after such work, and ongoing monitoring relating to known or potential groundwater constituents in the area. This guide does not address policy issues related to frequency or timing of sampling or sampling distances from the wellhead. In addition, it does not address reporting limits, sample preservation, holding times, laboratory quality control, regulatory action levels, or interpretation of analytical results.1.3 These guidelines are not intended to replace or supersede regulatory requirements and technical methodology or guidance nor are these guidelines intended for inclusion by reference in regulations. Instances where this guide is in conflict with statutory or regulatory requirements, practitioners shall defer to the latter. These guidelines are intended to assist in developing sampling programs to meet project goals and objectives. However, site-specific conditions, regulatory requirements, site-specific health and safety issues, technical manuals and directives, and program data quality objectives should be evaluated and consulted along with the information contained in this guide for each individual site and sampling program.1.4 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.1.5 Users are responsible for investigating and identifying all the legal and regulatory requirements that are applicable for the location where the sampling is being performed.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method covers the determination of the dissolved gases methane, ethane, ethylene, and propane in drinking, waste, and ground waters, including domestic wells; whether naturally occurring or resulting from commercial activities, dissolved gases can be hazardous both to the environment and humans. Due to increased scrutiny of dissolved gases, developing a valid method for the testing of dissolved gases in water has become more imperative. Static headspace sampling is generally applicable for sampling these compounds. However, as these compounds are extremely volatile, a closed sampling system is recommended. This test method can be used for quantitatively determining dissolved gases in ground, waste, and drinking waters.5.2 This test method is suitable for analysis of domestic drinking water samples from residential and commercial water supply wells prior to oil and gas exploration activities to form a baseline for monitoring potential impacts during exploration; development, including hydraulic fracturing; operation; closure; and reclamation of nearby oil and gas production and injection wells.1.1 This test method covers the determination of the dissolved gases methane, ethane, ethylene, and propane in drinking, waste, and ground waters, including domestic wells whether naturally occurring or resulting from commercial activities, or both. This test method has an analytical range from 10 µg/L to 11 000 µg/L for methane, and 10 µg/L to 5000 µg/L for ethane, ethylene, and propane. If a sample has a dissolved gas concentration above the calibration range, the sample would require dilution. Other analytical ranges may be used as long as the instrument calibration encompasses the desired range and demonstrates adequate linearity.1.2 This test method is applicable to samples collected at a nominal ambient pressure. Samples collected under high pressures, that is, above ambient pressure, may not be accurately analyzed using this method.1.3 This test method is applicable to a variety of dissolved gases; however, for the present standard, only methane, ethane, ethylene, and propane were validated. In order to validate for a gas not listed in this method, the analyst would need to establish the saturation concentration of the new gas, and establish a valid curve, method detection limits, and demonstration of capability following the procedures outlined in this method.1.4 It is the analyst’s responsibility to ensure the validity of this test method for dissolved gases other than methane, ethane, ethylene, and propane and other sample matrices.1.5 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.6 A single laboratory study was done in order to establish precision and bias for the surrogate (see Section 16).1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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