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5.1 Differential scanning calorimetry provides a rapid method for determining the transformation temperature(s) of nickel-titanium shape memory alloys.5.2 This test method uses small, stress-free, annealed samples to determine whether a sample of nickel-titanium alloy containing nominally 54.5 to 57.0 % nickel by weight is austenitic or martensitic at a particular temperature. Since chemical analysis of these alloys does not have sufficient precision to determine the transformation temperature by measuring the nickel-to-titanium ratio of the alloy, direct measurement of the transformation temperature of an annealed sample of known thermal history is recommended.5.3 This test method is useful for quality control, specification acceptance, and research.5.4 Transformation temperatures derived from differential scanning calorimetry (DSC) may not agree with those obtained by other test methods due to the effects of strain and load on the transformation. For example, transformation temperatures measured in accordance with Test Method F2082 will differ from those measured by the current standard.5.5 The use of this test method for finished or semi-finished components without annealing (as in 8.2) shall be agreed upon between the purchaser and the supplier.1.1 This test method defines procedures for determining the transformation temperatures of nickel-titanium shape memory alloys, produced in accordance with Specification F2063, by differential scanning calorimetry.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 Sieve analyses are carried out to determine the particle size distribution of powders which, in turn, are used to qualify those materials as to their usefulness in the process under consideration. Since particle size analyses have only relative significance, the results should be considered only where they correlate with process characteristics. The parameter that is being measured in this test is the amount of material that will pass through a cloth having theoretically square openings. It must be remembered that all the holes are not square, nor uniform in size, and the question of whether a given particle will go through is a statistical one. Since each particle size analysis method measures a unique physical parameter, the results from one method may not agree with those from another. Particle size distributions play a role in such properties as bulk density, dustiness, and handling characteristics. Care should be taken, however, when interpretations are made from one or two points (sieves) on the distribution curve.1.1 This test method covers the determination of the particle size distribution of nonplastic ceramic powders such as alumina, silica, feldspar, pyrophyllite, nepheline syenite, talc, titanates, and zircon using wire cloth sieves.1.2 Materials containing a large amount of fines, containing agglomerates, or that are nonfree-flowing, are wet-sieved to remove excessive fines or to disperse agglomerates before performing the test. This technique is not applicable to materials that are, to any degree, water soluble.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units, or are other customary units (in the case of sieve frame diameter and sieve number), that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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