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ASTM C1145-19 Standard Terminology of Advanced Ceramics Active 发布日期 :  1970-01-01 实施日期 : 

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4.1 This guide establishes a minimum standard for training rope rescuers in regard to their rope rescue specific knowledge and skills. A person trained to this guide is an advanced rope rescuer.4.1.1 Every person who is identified as an advanced rope rescuer shall have met the requirements of this guide.4.1.2 This guide is the third level of training for rope rescue personnel and, in conjunction with Guides F2751, F2752, and F2954, only establishes the minimum knowledge and skills required for a person to perform or lead advanced rope rescue. No other skills are included or implied.4.1.3 In addition to meeting the requirements of this guide, an advanced rope rescuer shall also be adequately trained to operate safely and effectively in the environment in which he or she is expected to work (i.e., wilderness, urban, etc.).4.2 Advanced rope rescue endorsement is an indication that a person possesses adequate field skills and knowledge to make mission-critical decisions. A person so endorsed is qualified to support or direct a rope rescue team in an area with high fall exposure and/or falling hazard potential, including high angle environments.4.3 This guide by itself is not a complete training document. It is only an outline of the topics required for training or evaluating an advanced rope rescuer. It may, however, be used in the development of, or as part of, a complete training document or program.4.3.1 This guide does not stand alone and must be used with the referenced documents to provide the specific information needed by an advanced rope rescuer or for an authority having jurisdiction (AHJ) to properly evaluate a training program or text.4.4 Though this guide establishes only minimum standards, it does not imply that an advanced rope rescuer is a “trainee,” “probationary,” or other similar term member of an organization.4.4.1 Determining the requirements and qualifications for land rescue team members is the responsibility of the AHJ.4.4.2 Nothing in this guide precludes an AHJ from adding additional requirements for its own members.4.5 Because technical rope rescue is inherently dangerous, and rope rescuers are frequently required to perform rigorous activities in adverse conditions, regional and national safety standards shall be included in agency and organization policies and procedures. Personnel endorsed as advanced rope rescuers shall complete all activities based on an analysis of risk versus benefit, and shall follow all applicable national, federal, state, provincial, and local safety standards.4.6 This guide can be used to evaluate a document to determine if its content includes the topics necessary for training an advanced rope rescuer. Likewise, this guide can be used to evaluate an existing training program to see if it meets the requirements of this guide.4.7 The knowledge and skills defined in the following sections are not presented in any particular order and do not represent a training sequence.4.8 Except where a physical skill needs to be shown, it is up to the AHJ to determine the best way to evaluate a person’s knowledge. This may be by written exam, oral exam, demonstration, or by some combination of the three.4.8.1 An advanced rope rescuer shall document his or her training by completion of a position task book, compliant with Guide F3068, or by field demonstration under qualified supervision.4.8.2 Unless stated otherwise, an ability or proficiency in a skill shall be demonstrated for initial qualification and then as often as required by the AHJ.1.1 This guide, in conjunction with, and as an add-on to, Guides F2751, F2752, and F2954 (or equivalent for other environments), defines the basic training required for a person who participates in rope rescue at the highest level of responsibility and complexity, as part of a larger rescue duty.1.1.1 Specifically, this guide defines the knowledge, skills, and abilities required for a person to support or direct a rope rescue team in advanced rope rescue functions including pre-planning and size-up of rope rescue operations, designing and directing the construction of rope systems for moving a victim in low and high angle environments, directing the construction and operation of highline and related rope systems, and performing advanced rope rigging functions, in conjunction with other rescue duties.1.1.2 This guide establishes the minimum training standard for an advanced rope rescue endorsed person in regard to general, field, and rope rescue-specific knowledge and skills.1.2 An advanced rope rescuer performs rope rescues in all terrain and is capable of directing basic and intermediate rope rescuers.1.2.1 An advanced rope rescuer endorsement applies only to rescues on the surface of the land; additional endorsements are required to perform this level of rope rescue in other environments. This guide alone does not define the minimum training requirements for performing or assisting with rescues in partially or fully collapsed structures, in or on water, in confined spaces, or underground (such as in caves, mines, and tunnels).1.2.2 This guide alone does not define the minimum training requirements for climbing Class 52 or higher rock and/or ice to perform a rescue.1.3 An advanced rope rescuer is required to have knowledge and skill sets pertaining to the advanced roped evacuation components of rescue. These include, but are not limited to, advanced knots and rigging, functioning as a litter attendant in a high angle lowering or raising operation, and directing a rope rescue team in the rescue of a subject suspended in a high angle environment.1.4 An advanced rope rescuer may be part of a rope rescue team as defined in Classification F1993.1.4.1 Further training may be required before an advanced rope rescuer may actually participate on a particular kind of rope rescue team, depending on the regulations or policies of the authority having jurisdiction.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 For many structural ceramic components in service, their use is often limited by lifetimes that are controlled by a process of slow crack growth. This test method provides the empirical parameters for appraising the relative slow crack growth susceptibility of ceramic materials under specified environments at elevated temperatures. This test method is similar to Test Method C1368 with the exception that provisions for testing at elevated temperatures are given. Furthermore, this test method may establish the influences of processing variables and composition on slow crack growth as well as on strength behavior of newly developed or existing materials, thus allowing tailoring and optimizing material processing for further modification. In summary, this test method may be used for material development, quality control, characterization, and limited design data generation purposes.NOTE 3: Data generated by this test method do not necessarily correspond to crack velocities that may be encountered in service conditions. The use of data generated by this test method for design purposes may entail considerable extrapolation and loss of accuracy.4.2 In this test method, the flexural stress computation is based on simple beam theory, with the assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one fiftieth (1/50) of the beam thickness.4.3 In this test method, the test specimen sizes and test fixtures were chosen in accordance with Test Method C1211, which provides a balance between practical configurations and resulting errors, as discussed in Refs (5, 6). Only the four-point test configuration is used in this test method.4.4 In this test method, the slow crack growth parameters (n and D) are determined based on the mathematical relationship between flexural strength and applied stress rate, log σf = [1/(n + 1)] log σ˙ + log D, together with the measured experimental data. The basic underlying assumption on the derivation of this relationship is that slow crack growth is governed by an empirical power-law crack velocity, v = A[KI /KIC]n (see Appendix X1).NOTE 4: There are various other forms of crack velocity laws which are usually more complex or less convenient mathematically, or both, but may be physically more realistic (7). The mathematical analysis in this test method does not cover such alternative crack velocity formulations.4.5 In this test method, the mathematical relationship between flexural strength and stress rate was derived based on the assumption that the slow crack growth parameter is at least n ≥ 5 (1, 8). Therefore, if a material exhibits a very high susceptibility to slow crack growth, that is, n < 5, special care should be taken when interpreting the results.4.6 The mathematical analysis of test results according to the method in 4.4 assumes that the material displays no rising R-curve behavior, that is, no increasing fracture resistance (or crack-extension resistance) with increasing crack length. It should be noted that the existence of such behavior cannot be determined from this test method. The analysis further assumes that the same flaw types control strength over the entire test range. That is, no new flaws are created, and the flaws that control the strength at the highest stress rate control the strength at the lowest stress rate.4.7 Slow crack growth behavior of ceramic materials can vary as a function of mechanical, material, thermal, and environmental variables. Therefore, it is essential that test results accurately reflect the effects of specific variables under study. Only then can data be compared from one investigation to another on a valid basis, or serve as a valid basis for characterizing materials and assessing structural behavior.4.8 The strength of advanced ceramics is probabilistic in nature. Therefore, slow crack growth that is determined from the flexural strengths of a ceramic material is also a probabilistic phenomenon. Hence, a proper range and number of test rates in conjunction with an appropriate number of specimens at each test rate are required for statistical reproducibility and design (2). Guidance is provided in this test method.NOTE 5: For a given ceramic material/environment system, the SCG parameter n is independent of specimen size, although its reproducibility is dependent on the variables previously mentioned. By contrast, the SCG parameter D depends significantly on strength, and thus on specimen size (see Eq X1.7).4.9 The elevated-temperature strength of a ceramic material for a given test specimen and test fixture configuration is dependent on its inherent resistance to fracture, the presence of flaws, test rate, and environmental effects. Analysis of a fracture surface, fractography, though beyond the scope of this test method, is highly recommended for all purposes, especially to verify the mechanism(s) associated with failure (refer to Practice C1322).1.1 This test method covers the determination of slow crack growth (SCG) parameters of advanced ceramics by using constant stress-rate flexural testing in which flexural strength is determined as a function of applied stress rate in a given environment at elevated temperatures. The strength degradation exhibited with decreasing applied stress rate in a specified environment is the basis of this test method which enables the evaluation of slow crack growth parameters of a material.NOTE 1: This test method is frequently referred to as “dynamic fatigue” testing (1-3)2 in which the term “fatigue” is used interchangeably with the term “slow crack growth.” To avoid possible confusion with the “fatigue” phenomenon of a material which occurs exclusively under cyclic loading, as defined in Terminology E1823, this test method uses the term “constant stress-rate testing” rather than “dynamic fatigue” testing.NOTE 2: In glass and ceramics technology, static tests of considerable duration are called “static fatigue” tests, a type of test designated as stress-rupture (Terminology E1823).1.2 This test method is intended primarily to be used for negligible creep of test specimens, with specific limits on creep imposed in this test method.1.3 This test method applies primarily to advanced ceramics that are macroscopically homogeneous and isotropic. This test method may also be applied to certain whisker- or particle-reinforced ceramics that exhibit macroscopically homogeneous behavior.1.4 This test method is intended for use with various test environments such as air, vacuum, inert, and any other gaseous environments.1.5 Values expressed in this standard test are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose flexural strength is ∼50 MPa (∼7 ksi) or greater.4.2 The flexure stress is computed based on simple beam theory, with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than 1/50 of the beam thickness. The homogeneity and isotropy assumptions in the test method rule out the use of it for continuous fiber-reinforced composites for which Test Method C1341 is more appropriate.4.3 The flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the testing rate, test environment, specimen size, specimen preparation, and test fixtures. Specimen and fixture sizes were chosen to provide a balance between the practical configurations and resulting errors as discussed in Test Method C1161, and Refs (1-3).4 Specific fixture and specimen configurations were designated in order to permit the ready comparison of data without the need for Weibull size scaling.4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws. Variations in these cause a natural scatter in test results for a sample of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this test method, is highly recommended for all purposes, especially if the data will be used for design as discussed in Ref (4) and Practices C1322 and C1239.4.5 This method determines the flexural strength at elevated temperature and ambient environmental conditions at a nominal, moderately fast testing rate. The flexural strength under these conditions may or may not necessarily be the inert flexural strength. Flexure strength at elevated temperature may be strongly dependent on testing rate, a consequence of creep, stress corrosion, or slow crack growth. If the purpose of the test is to measure the inert flexural strength, then extra precautions are required and faster testing rates may be necessary.NOTE 6: Many ceramics are susceptible to either environmentally assisted slow crack growth or thermally activated slow crack growth. Oxide ceramics, glasses, glass ceramics, and ceramics containing boundary phase glass are particularly susceptible to slow crack growth. Time-dependent effects that are caused by environmental factors (for example, water as humidity in air) may be minimized through the use of inert testing atmosphere such as dry nitrogen gas or vacuum. Alternatively, testing rates faster than specified in this standard may be used if the goal is to measure the inert strength. Thermally activated slow crack growth may occur at elevated temperature even in inert atmospheres. Testing rates faster than specified in this standard should be used if the goal is to measure the inert flexural strength. On the other hand, many ceramics such as boron carbide, silicon carbide, aluminum nitride, and many silicon nitrides have no sensitivity to slow crack growth at room or moderately elevated temperatures and for such materials, the flexural strength measured under laboratory ambient conditions at the nominal testing rate is the inert flexural strength.4.6 The three-point test configuration exposes only a very small portion of the specimen to the maximum stress. Therefore, three-point flexural strengths are likely to be much greater than four-point flexural strengths. Three-point flexure has some advantages. It uses simpler test fixtures, it is easier to adapt to high temperature, and it is sometimes helpful in Weibull statistical studies. However, four-point flexure is preferred and recommended for most characterization purposes.4.7 The three-point test configuration exposes only a very small portion of the specimen to the maximum stress. Therefore, three-point flexural strengths are likely to be much greater than four-point flexural strengths. Three-point flexure has some advantages. It uses simpler test fixtures, it is easier to adapt to high temperature, and it is sometimes helpful in Weibull statistical studies. However, four-point flexure is preferred and recommended for most characterization purposes.1.1 This test method covers determination of the flexural strength of advanced ceramics at elevated temperatures.2 Four-point-1/4-point and three-point loadings with prescribed spans are the standard as shown in Fig. 1. Rectangular specimens of prescribed cross-section are used with specified features in prescribed specimen-fixture combinations. Test specimens may be 3 by 4 by 45 to 50 mm in size that are tested on 40-mm outer span four-point or three-point fixtures. Alternatively, test specimens and fixture spans half or twice these sizes may be used. The test method permits testing of machined or as-fired test specimens. Several options for machining preparation are included: application matched machining, customary procedures, or a specified standard procedure. This test method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The test method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.4.2 Continuous fiber-reinforced ceramic matrix composites generally are characterized by glass or fine grain-sized (<50 μm) ceramic matrices and ceramic fiber reinforcements. CFCCs are candidate materials for high-temperature structural applications requiring high degrees of corrosion and oxidation resistance, wear and erosion resistance, and inherent damage tolerance, that is, toughness. In addition, continuous fiber-reinforced glass (amorphous) matrix composites are candidate materials for similar but possibly less demanding applications. Although shear test methods are used to evaluate shear interlaminar strength (τZX, τZY) in advanced ceramics, there is significant difficulty in test specimen machining and testing. Improperly prepared notches can produce nonuniform stress distribution in the shear test specimens and can lead to ambiguity of interpretation of strength results. In addition, these shear test specimens also rarely produce a gage section that is in a state of pure shear. Uniaxially forced transthickness tensile strength tests measure the tensile interlaminar strengthavoid the complications listed above, and provide information on mechanical behavior and strength for a uniformly stressed material. The ultimate strength value measured is not a direct measure of the matrix strength, but a combination of the strength of the matrix and the level of bonding between the fiber, fiber/matrix interphase, and the matrix.4.3 CFCCs tested in a transthickness tensile test (TTT) may fail from a single dominant flaw or from a cumulative damage process; therefore, the volume of material subjected to a uniform tensile stress for a single uniaxially forced TTT may be a significant factor in determining the ultimate strength of CFCCs. The probabilistic nature of the strength distributions of the brittle matrices of CFCCs requires a sufficient number of test specimens at each testing condition for statistical analysis and design, with guidelines for test specimen size and sufficient numbers provided in this test method. Studies to determine the exact influence of test specimen volume on strength distributions for CFCCs have not been completed. It should be noted that strengths obtained using other recommended test specimens with different volumes and areas may vary due to these volume differences.4.4 The results of TTTs of test specimens fabricated to standardized dimensions from a particular material, or selected portions of a part, or both, may not totally represent the strength and deformation properties of the entire full-size end product or its in-service behavior in different environments.4.5 For quality control purposes, results derived from standardized TTT specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.4.6 The strength of CFCCs is dependent on their inherent resistance to fracture, the presence of flaws, damage accumulation processes, or a combination thereof. Analysis of fracture surfaces and fractography, though beyond the scope of this test method, is highly recommended.1.1 This test method covers the determination of transthickness tensile strengthunder monotonic uniaxial tensile loading of continuous fiber-reinforced ceramics (CFCC) at ambient temperature. This test method addresses, but is not restricted to, various suggested test specimen geometries, test fixtures, data collection, and reporting procedures. In general, round or square test specimens are tensile tested in the direction normal to the thickness by bonding appropriate hardware to the samples and performing the test. For a Cartesian coordinate system, the x-axis and the y-axis are in the plane of the test specimen. The transthickness direction is normal to the plane and is labeled the z-axis for this test method. For CFCCs, the plane of the test specimen normally contains the larger of the three dimensions and is parallel to the fiber layers for unidirectional, bidirectional, and woven composites. Note that transthickness tensile strength as used in this test method refers to the tensile strength obtained under monotonic uniaxial tensile loading, where “monotonic” refers to a continuous nonstop test rate with no reversals from test initiation to final fracture.1.2 This test method is intended primarily for use with all advanced ceramic matrix composites with continuous fiber reinforcement: unidirectional (1D), bidirectional (2D), woven, and tridirectional (3D). In addition, this test method also may be used with glass (amorphous) matrix composites with 1D, 2D, and 3D continuous fiber reinforcement. This test method does not directly address discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics, although the test methods detailed here may be equally applicable to these composites. It should be noted that 3D architectures with a high volume fraction of fibers in the “z” direction may be difficult to test successfully.1.3 Values are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Additional recommendations are provided in 6.7 and Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Advanced ceramics can be candidate materials for structural applications requiring high degrees of wear and corrosion resistance, often at elevated temperatures.5.2 Joints are produced to enhance the performance and applicability of materials. While the joints between similar materials are generally made for manufacturing complex parts and repairing components, those involving dissimilar materials usually are produced to exploit the unique properties of each constituent in the new component. Depending on the joining process, the joint region may be the weakest part of the component. Since under mixed-mode and shear loading the load transfer across the joint requires reasonable shear strength, it is important that the quality and integrity of joint under in-plane shear forces be quantified. Shear strength data are also needed to monitor the development of new and improved joining techniques.5.3 Shear tests provide information on the strength and deformation of materials under shear stresses.5.4 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.5.5 For quality control purposes, results derived from standardized shear test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.1.1 This test method covers the determination of shear strength of joints in advanced ceramics at ambient temperature using asymmetrical four-point flexure. Test specimen geometries, test specimen fabrication methods, testing modes (that is, force or displacement control), testing rates (that is, force or displacement rate), data collection, and reporting procedures are addressed.1.2 This test method is used to measure shear strength of ceramic joints in test specimens extracted from larger joined pieces by machining. Test specimens fabricated in this way are not expected to warp due to the relaxation of residual stresses but are expected to be much straighter and more uniform dimensionally than butt-jointed test specimens prepared by joining two halves, which is not recommended. In addition, this test method is intended for joints, which have either low or intermediate strengths with respect to the substrate material to be joined. Joints with high strengths should not be tested by this test method because of the high probability of invalid tests resulting from fractures initiating at the reaction points rather than in the joint. Determination of the shear strength of joints using this test method is appropriate particularly for advanced ceramic matrix composite materials but also may be useful for monolithic advanced ceramic materials.1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are noted in 8.1.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The high-temperature capabilities of advanced ceramics are a key performance benefit for many demanding engineering applications. In many of those applications, advanced ceramics will have to perform across a broad temperature range. The thermal expansion, thermal diffusivity/conductivity, specific heat, and emittance/emissivity are crucial engineering factors in integrating ceramic components into aerospace, automotive, and industrial systems.5.2 This guide is intended to serve as a reference and information source for testing the thermal properties of advanced ceramics, based on an understanding of the relationships between the composition and microstructure of these materials and their thermal properties.5.3 The use of this guide assists the testing community in correctly applying the ASTM thermal test methods to advanced ceramics to ensure that the thermal test results are properly measured, interpreted, and understood. This guide also assists the user in selecting the appropriate thermal test method to evaluate the particular thermal properties of the advanced ceramic of interest.5.4 The thermal properties of advanced ceramics are critical data in the development of ceramic components for aerospace, automotive, and industrial applications. In addition, the effect of environmental exposure on thermal properties of the advanced ceramics must also be assessed.1.1 This guide covers the thermal property testing of advanced ceramics, to include monolithic ceramics, particulate/ whisker-reinforced ceramics, and continuous fiber-reinforced ceramic composites. It is intended to provide guidance and information to users on the special considerations involved in determining the thermal properties of these ceramic materials.1.2 Five thermal properties (specific heat capacity, thermal conductivity, thermal diffusivity, thermal expansion, and emittance/emissivity) are presented in terms of their definitions and general test methods. The relationship between thermal properties and the composition, microstructure, and processing of advanced ceramics (monolithic and composite) is briefly outlined, providing guidance on which material and specimen characteristics have to be considered in evaluating the thermal properties of advanced ceramics. Additional sections describe sampling considerations, test specimen preparation, and reporting requirements.1.3 Current ASTM test methods for thermal properties are tabulated in terms of test method concept, testing range, specimen requirements, standards/reference materials, capabilities, limitations, precision, and special instructions for monolithic and composite ceramics.1.4 This guide is based on the use of current ASTM standards for thermal properties, where appropriate, and on the development of new test standards, where necessary. It is not the intent of this guide to rigidly specify particular thermal test methods for advanced ceramics. Guidance is provided on how to utilize the most commonly available ASTM thermal test methods, considering their capabilities and limitations.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. See IEEE/ASTM SI 10.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The requirements for radiographic examination in this practice are applicable to all types of metallic and nonmetallic material used in designated applications such as gas turbines and flight structures.4.2 This practice establishes the basic parameters for the application and control of the radiographic process. This practice may be specified on an engineering drawing, specification, or contract; however, it is not a detailed radiographic technique and must be supplemented. Section 7 and Practices E1030/E1030M and E1032 contain information to help develop detailed radiographic techniques.1.1 This practice establishes the minimum requirements for radiographic examination of metallic and nonmetallic materials and components used in designated applications such as gas turbine engines and flight structures.1.2 The requirements in this practice are intended to control the radiographic process to ensure the quality of radiographic images produced for use in designated applications such as gas turbine engines and flight structures; this practice is not intended to establish acceptance criteria for material or components. When examination is performed in accordance with this practice, engineering drawings, specifications, or other applicable documents shall indicate the acceptance criteria.1.3 All areas of this practice may be open to agreement between the cognizant engineering organization and the supplier, or specific direction from the cognizant engineering organization.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides information on the uniaxial tensile properties and tensile stress-strain response of a ceramic composite tube—tensile strength and strain, fracture strength and strain, proportional limit stress and strain, tensile elastic modulus, etc. The information may be used for material development, material comparison, quality assurance, characterization, and design data generation.5.2 Continuous fiber-reinforced ceramic composites (CFCCs) are composed of continuous ceramic-fiber directional (1D, 2D, and 3D) reinforcements in a fine-grain-sized (<50 µm) ceramic matrix with controlled porosity. Often these composites have an engineered thin (0.1 to 10 µm) interface coating on the fibers to produce crack deflection and fiber pull-out. These ceramic composites offer high-temperature stability, inherent damage tolerance, and high degrees of wear and corrosion resistance. As such, these ceramic composites are particularly suited for aerospace and high-temperature structural applications (1, 2).35.3 CFCC components have a distinctive and synergistic combination of material properties, interface coatings, porosity control, composite architecture (1D, 2D, and 3D), and geometric shape that are generally inseparable. Prediction of the mechanical performance of CFCC tubes (particularly with braid and 3D weave architectures) cannot be made by applying measured properties from flat CFCC plates to the design of tubes. Direct uniaxial tensile strength tests of CFCC tubes are needed to provide reliable information on the mechanical behavior and strength of tube geometries.5.4 CFCCs generally experience “graceful” fracture from a cumulative damage process, unlike monolithic advanced ceramics which fracture catastrophically from a single dominant flaw. The tensile behavior and strength of a CFCC are dependent on its inherent resistance to fracture, the presence of flaws, and any damage accumulation processes. These factors are affected by the composite material composition and variability in material and testing—components, reinforcement architecture and volume fraction, porosity content, matrix morphology, interface morphology, methods of material fabrication, test specimen preparation and conditioning, and surface condition.5.5 The results of tensile tests of test specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the strength and deformation properties of the entire, full-size end product or its in-service behavior in different environments.5.6 For quality control purposes, results derived from standardized tubular tensile test specimens may be considered indicative of the response of the material from which they were taken, given primary processing conditions and post-processing heat treatments.1.1 This test method determines the axial tensile strength and stress-strain response of continuous fiber-reinforced advanced ceramic composite tubes at ambient temperature under monotonic loading. This test method is specific to tube geometries, because fiber architecture and specimen geometry factors are often distinctly different in composite tubes, as compared to flat plates.1.2 In the test method a composite tube/cylinder with a defined gage section and a known wall thickness is fitted/bonded into a loading fixture. The test specimen/fixture assembly is mounted in the testing machine and monotonically loaded in uniaxial tension at ambient temperature while recording the tensile force and the strain in the gage section. The axial tensile strength and the fracture strength are determined from the maximum applied force and the fracture force. The strains, the proportional limit stress, and the tensile modulus of elasticity are determined from the stress-strain data.1.3 This test method applies primarily to advanced ceramic matrix composite tubes with continuous fiber reinforcement: unidirectional (1D, filament wound and tape lay-up), bidirectional (2D, fabric/tape lay-up and weave), and tridirectional (3D, braid and weave). These types of ceramic matrix composites are composed of a wide range of ceramic fibers (oxide, graphite, carbide, nitride, and other compositions) in a wide range of crystalline and amorphous ceramic matrix compositions (oxide, carbide, nitride, carbon, graphite, and other compositions).1.4 This test method does not directly address discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics, although the test methods detailed here may be equally applicable to these composites.1.5 The test method describes a range of test specimen tube geometries based on past tensile testing of ceramic composite tubes. These geometries are applicable to tubes with outer diameters of 10 to 150 mm and wall thicknesses of 1 to 25 mm, where the ratio of the outer diameter-to-wall thickness (dO /t) is typically between 5 and 30.1.5.1 This test method is specific to ambient temperature testing. Elevated temperature testing requires high-temperature furnaces and heating devices with temperature control and measurement systems and temperature-capable grips and loading fixtures, which are not addressed in this test method.1.6 The test method addresses test equipment, gripping methods, testing modes, allowable bending stresses, interferences, tubular test specimen geometries, test specimen preparation, test procedures, data collection, calculation, reporting requirements, and precision/bias in the following sections.  Section 1Referenced Documents 2Terminology 3Summary of Test Method 4 5Interferences 6Apparatus 7Hazards 8Test Specimens 9Test Procedure 10Calculation of Results 11Report 12Precision and Bias 13Keywords 14Annexes  Interferences Annex A1Test Specimen Geometry Annex A2Grip Fixtures and Load Train Couplers Annex A3Allowable Bending and Load Train Alignment Annex A4Test Modes and Rates Annex A51.7 Units—The values stated in SI units are to be regarded as standard.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Advanced ceramics usually display a linear stress-strain behavior to failure. Lack of ductility combined with flaws that have various sizes and orientations leads to scatter in failure strength. Strength is not a deterministic property, but instead reflects an intrinsic fracture toughness and a distribution (size and orientation) of flaws present in the material. This practice is applicable to brittle monolithic ceramics that fail as a result of catastrophic propagation of flaws present in the material. This practice is also applicable to composite ceramics that do not exhibit any appreciable bilinear or nonlinear deformation behavior. In addition, the composite must contain a sufficient quantity of uniformly distributed reinforcements such that the material is effectively homogeneous. Whisker-toughened ceramic composites may be representative of this type of material.5.2 Two- and three-parameter formulations exist for the Weibull distribution. This practice is restricted to the two-parameter formulation. An objective of this practice is to obtain point estimates of the unknown parameters by using well-defined functions that incorporate the failure data. These functions are referred to as “estimators.” It is desirable that an estimator be consistent and efficient. In addition, the estimator should produce unique, unbiased estimates of the distribution parameters (6). Different types of estimators exist, including moment estimators, least-squares estimators, and maximum likelihood estimators. This practice details the use of maximum likelihood estimators due to the efficiency and the ease of application when censored failure populations are encountered.5.3 Tensile and flexural test specimens are the most commonly used test configurations for advanced ceramics. The observed strength values are dependent on test specimen size and geometry. Parameter estimates can be computed for a given test specimen geometry ( m^, ^σθ), but it is suggested that the parameter estimates be transformed and reported as material-specific parameters ( m^, ^σ0). In addition, different flaw distributions (for example, failures due to inclusions or machining damage) may be observed, and each will have its own strength distribution parameters. The procedure for transforming parameter estimates for typical test specimen geometries and flaw distributions is outlined in 8.6.5.4 Many factors affect the estimates of the distribution parameters. The total number of test specimens plays a significant role. Initially, the uncertainty associated with parameter estimates decreases significantly as the number of test specimens increases. However, a point of diminishing returns is reached when the cost of performing additional strength tests may not be justified. This suggests that a practical number of strength tests should be performed to obtain a desired level of confidence associated with a parameter estimate. The number of test specimens needed depends on the precision required in the resulting parameter estimate. Details relating to the computation of confidence bounds (directly related to the precision of the estimate) are presented in 9.3 and 9.4.1.1 This practice covers the evaluation and reporting of uniaxial strength data and the estimation of Weibull probability distribution parameters for advanced ceramics that fail in a brittle fashion (see Fig. 1). The estimated Weibull distribution parameters are used for statistical comparison of the relative quality of two or more test data sets and for the prediction of the probability of failure (or, alternatively, the fracture strength) for a structure of interest. In addition, this practice encourages the integration of mechanical property data and fractographic analysis.1.6 The values stated in SI units are to be regarded as the standard per IEEE/ASTM SI 10.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Surface grinding can cause a significant decrease4 in the flexure strength of advanced ceramic materials. The magnitude of the loss in strength is determined by the grinding conditions and the response of the material. This test method can be used to obtain a detailed characterization of the relationship between grinding conditions and flexure strength for an advanced ceramic material. The effect on flexure strength of varying a single grinding parameter or several grinding parameters can be measured. The method may also be used to compare and rank different materials according to their response to one or more different grinding conditions. Results obtained by this method can be used to develop an optimum grinding process with respect to maximizing material removal rate for a specified flexure strength requirement. The test method can assist in the development of improved grinding-damage-tolerant ceramic materials. It may also be used for quality control purposes to monitor and assure the consistency of a grinding process in the fabrication of parts from advanced ceramic materials. The test method is applicable to grinding methods that generate a planar surface and is not directly applicable to grinding methods that produce non-planar surfaces such as cylindrical and centerless grinding.1.1 This test method covers the determination of the effect of surface grinding on the flexure strength of advanced ceramics. Surface grinding of an advanced ceramic material can introduce microcracks and other changes in the near surface layer, generally referred to as damage (see Fig. 1 and Ref. (1)).2 Such damage can result in a change—most often a decrease—in flexure strength of the material. The degree of change in flexure strength is determined by both the grinding process and the response characteristics of the specific ceramic material. This method compares the flexure strength of an advanced ceramic material after application of a user-specified surface grinding process with the baseline flexure strength of the same material. The baseline flexure strength is obtained after application of a surface grinding process specified in this standard. The baseline flexure strength is expected to approximate closely the inherent strength of the material. The flexure strength is measured by means of ASTM flexure test methods.FIG. 1 Microcracks Associated with Grinding (Ref. (1))21.2 Flexure test methods used to determine the effect of surface grinding are C1161 Test Method for Flexure Strength of Advanced Ceramics at Ambient Temperatures and C1211 Test Method for Flexure Strength of Advanced Ceramics at Elevated Temperatures.1.3 Materials covered in this standard are those advanced ceramics that meet criteria specified in flexure testing standards C1161 and C1211.1.4 The flexure test methods supporting this standard (C1161 and C1211) require test specimens that have a rectangular cross section, flat surfaces, and that are fabricated with specific dimensions and tolerances. Only grinding processes that are capable of generating the specified flat surfaces, that is, planar grinding modes, are suitable for evaluation by this method. Among the applicable machine types are horizontal and vertical spindle reciprocating surface grinders, horizontal and vertical spindle rotary surface grinders, double disk grinders, and tool-and-cutter grinders. Incremental cross-feed, plunge, and creep-feed grinding methods may be used.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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