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5.1 This test method is used to measure chemical permeation through specimens of protective clothing under the condition of intermittent contact of a test chemical with the specimen. In many applications, protective clothing is contacted intermittently to chemicals, not continuously as is tested by Test Method F739.5.2 This test method is normally used to evaluate flat specimens and seams from finished items of protective clothing and of materials that are candidates for items of protective clothing.5.2.1 Finished items of protective clothing include gloves, sleeves, aprons, suits, coveralls, hoods, boots, respirators, and the like.5.2.2 The phrase “specimens from finished items” encompasses seams or other discontinuous regions as well as continuous regions of protective clothing items.5.2.3 Selected seams for testing are representative of seams used in the principal construction of the protective clothing item and typically include seams of both the base material and where the base material is joined with other types of materials.5.3 In some cases, it may be of interest to compare permeation behaviors that occur under conditions of intermittent contact with those that occur during continuous contact. Test Method F739 is recommended for measuring permeation under the conditions of continuous contact of the test chemical with the protective clothing specimen.5.4 The breakthrough detection time, standardized breakthrough time, and the cumulative permeation are key measures of the effectiveness of a clothing material to be a barrier to the test chemical. Such information is used in the comparison of clothing materials during the process of selecting clothing for protection from hazardous chemicals. Long breakthrough detection times and standardized breakthrough times and low amounts of cumulative permeation are characteristics of more effective barrier materials than materials with higher permeation characteristics.NOTE 1: At present, there is limited quantitative information about acceptable levels of dermal contact with most chemicals. Therefore, the data obtained using this test method cannot be used to infer safe exposure levels.5.4.1 The reporting of a standardized breakthrough time greater than a specific time period does not mean that no chemical permeated through the protective clothing material since the standard breakthrough time is determined based on the permeation rate reaching a level of 0.1 μg/cm2/min. Some chemical had already permeated the specimen prior to the reported standardized breakthrough time.5.4.2 The reporting of cumulative permeation over a specified test period is another means to report barrier performance of protective clothing for resistance to permeation. This measurement quantifies the total amount of chemical that passed through a known area of the material during the specified test period.NOTE 2: It is possible to relate cumulative permeation test results to the total amount of chemical to which an individual wearer may be exposed by accounting for the exposed surface area and the underlying air layer. This information has potential value when there are known maximum permitted skin exposure doses for specific chemicals.5.5 The sensitivity of the test method in detecting low permeation rates or amounts of the test chemical permeated is determined by the combination of: (1) the analytical technique and collection system selected, and (2) the ratio of material specimen area to collection medium volume or flow rate.5.5.1 The analytical technique employed shall be capable of measuring the concentration of the test chemical in the collection medium at or below 0.05 μg/cm2/min.5.5.2 Often, permeation tests will require measurement of the test chemical over several orders of magnitude in concentration, requiring adjustments in either the sample collection volume or concentration/dilution, or the analytical instrument settings over the course of the test.5.5.3 Higher ratios of material specimen area to collection medium volume or flow rate permit earlier detection of permeation because higher concentrations of the test chemical in the collection medium will develop in a given time period, relative to those that would occur at lower ratios.5.5.4 The sensitivity of an open-loop system is characterized by its minimum detectable permeation rate. A method for determining this value is presented in Appendix X1.5.5.5 The sensitivity of a closed-loop system is characterized by its minimum detectable mass permeated.5.6 Comparison of results of tests performed with different permeation test systems requires specific information on the test cell, procedures, contact and purge times, and analytical techniques. Results obtained from closed-loop and open-loop testing may not be directly comparable.5.7 While this method specifies standardized breakthrough time as the time at which the permeation rate reaches 0.1 μg/cm2/min, it is acceptable to continue the testing and also report a normalized breakthrough time at a permeation rate of 1.0 µg/cm2/min.5.7.1 It is permitted to terminate tests early if there is catastrophic permeation of the chemical through the protective clothing material and the rate of permeation could overwhelm the capability of the selected analytical technique.5.8 A group of chemicals that is commonly used in permeation testing is given in Guide F1001.5.9 Guide F1194 provides a recommended approach for reporting permeation test results.1.1 This test method measures the permeation of liquids and gases through protective clothing materials under the condition of intermittent contact.1.2 This test method is designed for use when the test chemical is a gas or a liquid, where the liquid is either volatile (that is, having a vapor pressure greater than 1 mm Hg at 25 °C) or soluble in water or another liquid that does not interact with the clothing material.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method establishes a standard procedure for rapidly (in 1 h or less) determining the chemical resistance of specimens of protective clothing materials. This test method can be used to rank materials as to their suitability for use with liquids of known or unknown composition.5.2 The breakthrough detection time, permeation rate, or cumulative permeation can be used to identify protective clothing materials that are more likely to limit potential exposures to chemicals. Longer breakthrough detection times and lower cumulative amounts permeated and permeation rates are characteristics of materials that are better barriers to the test chemical.5.3 In general this test method is less sensitive than Test Method F739 coupled with sensitive analytical procedures. In cases where the chemical of concern is highly toxic and contact of even a very small amount with the skin may be detrimental to health, the permeation cup method is not recommended. Use Test Method F739.5.4 Upon permeating the clothing material, the chemical must evaporate in order for a weight loss to occur and permeation to be detected. Consequently, the test method may not be applicable for chemicals having low volatility (that is, vapor pressure). The vapor pressure below which this test method is not applicable has not been determined.5.4.1 A procedure for assessing volatility is described in Section 10.5.5 The results of this test method are highly dependent on the test temperature. If the objective is to compare different clothing materials, all tests shall be conducted at the same temperature (±3 °C).1.1 This test method measures the barrier effectiveness of a specimen of protective clothing upon continuous contact with a liquid.1.1.1 Procedure A—For use when a value for the cumulative amount of chemical permeated in 1 h is desired.1.1.2 Procedure B—For use when breakthrough detection time and permeation rate values are desired.1.2 Although not addressed herein, the effect of the test chemical on the clothing material can be determined by comparing the weight or other physical properties of the specimen before and after the permeation test.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The purpose of this test method is to provide a measurable criterion of performance about the level of cut resistance provided by different types of protective garments and protected coverings worn by chainsaw operators.5.2 This test method is intended to show to what level a protective garment can offer resistance to the cutting action of a chainsaw.5.3 The protection which can be demonstrated by the garments and coverings tested in accordance with this test method is achieved by: (1) the cut resistance of the material to cutting when put in contact with saw chain; (2) pulling a part of the material or yarns in the material so that they are drawn into the chain and drive mechanism to block the chain movement; (3) the fibers of the materials used to demonstrate both high resistance to cutting and the capacity to absorb rotational energy, so that chain speed can be slowed down sufficiently to stop the movement of the saw chain; or (4) any combination of these.5.4 This test method does not purport to evaluate comfort of lower body protective garments.5.5 In case of a dispute arising from differences in reported test results when using this test method for acceptance testing of commercial shipments, the purchaser and the supplier should perform comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens from the same lot of components to be evaluated. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. If a bias is found, either its cause must be determined and corrected or the purchaser and the supplier must agree to interpret future test results in light of the known bias.1.1 This test method measures cut resistance of garments and devices worn to protect the lower body (legs) when operating a chainsaw.1.2 This test method may be used to test for compliance to minimum performance requirements in established safety standards.1.2.1 By agreement between the purchaser and the supplier, or as required by established safety standards, it will be decided if this test method will be used to determine one or both of the following: (1) chain speed 50 (CS50), and (2) success/failure (jamming/chain stop or no cut in less than 1.5 s) at specified chain speed.1.3 This test method may be used to determine levels of protection for areas of coverage as stipulated in established safety standards.1.4 The values stated in SI units are to be regarded as standard.NOTE 1: The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining values in any way.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is intended for the determination of the cylinder heat transfer performance value of a flame-resistant material or combination of materials when exposed to a continuous and constant heat source. This is used to compare materials used in flame-resistant clothing for workers when exposed to combined convective and radiant thermal hazards.NOTE 3: Air movement at the face of the specimen and around the calorimeter can affect the measured heat transferred due to forced convective heat losses. Minimizing air movement around the specimen and test apparatus will aid in the repeatability of the results.5.2 This test method maintains the specimen with and without air gaps in a static, horizontal position and does not involve movement unless the test specimen naturally changes due to the thermal exposure.5.3 This test method specifies a standardized 84 ± 2 kW/m2 (2 ± 0.05 cal/cm2·s) exposure condition. Different exposure conditions have the potential to produce different results. Use of other exposure conditions that are representative of the expected hazard are allowed but shall be reported with the results, along with a determination of the exposure energy level stability.5.4 This test method does not predict skin burn injury from the heat exposure.5.5 This test method is similar to Test Method F2700 in that it uses the same energy heat source, water-cooled shutter, data acquisition, and measures the heat transfer through protective clothing materials using a copper calorimeter. This test method differs from Test Method F2700 in the usage of an eccentric instrumented cylinder mounted horizontally that allows for the thermal shrinkage of materials when tested.1.1 This test method measures the thermal response of a material or combination of materials using a combined convective/radiant heat transmission apparatus consisting of an eccentric cylindrical test sensor. It can be used to estimate the non-steady state thermal transfer through flame-resistant materials used in clothing when subjected to a continuous, combined convective and radiant heat exposure. The average incident heat flux is 84 kW/m2 (2 cal/cm2·s), with durations up to 30 s.1.1.1 This test method is not applicable to materials that melt, drip, or cause falling debris during the test.NOTE 1: Because of the arrangement of the equipment, if materials melt, drip, or cause falling debris during the test, the test result is invalid.1.2 Heat transmission through clothing is largely determined by its thickness, including any air gaps. The air gaps can vary considerably in different areas of the human body. This method provides a means of grading materials when tested under standard test conditions and an air gap exists between the fabric and the sensor. During the exposure, fabric temperatures can exceed 400 °C. At these temperatures some fabrics are not dimensionally stable and can shrink or stretch. The cylindrical geometry used in this test method allows such motion to occur, which will affect the time to achieve the end point of the test. These effects are not demonstrated in planar geometry test methods such as Test Method F2700.1.3 This test method is used to measure and describe the response of materials, products, or assemblies to heat under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.4 The measurements obtained and observations noted only apply to the particular material(s) tested using the specified heat flux, flame distribution, and duration.1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units or other units commonly used for thermal testing. If appropriate, round the non-SI units for convenience.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This specification provides minimum requirements for labeling protective clothing offering heat, flame, and melting resistance for applications where the potential exists for incidental exposure to open flame, radiant heat sources, or hot surfaces which could melt or ignite materials.1.1.1 Examples of possible applications for this specification include safety apparel, including high-visibility safety apparel, in situations where the possibility exists for accidental contact with hot surfaces, radiant heat sources, or an open flame; clothing worn by individuals for chemical, liquid, or particle protection where the possibility exists for clothing to similarly contact a burner or similar low-intensity flame source; or other clothing worn by individuals that comes in contact with torch flames, hot piping, or other surfaces that melt, degrade, or ignite clothing materials by proximity or contact.1.1.2 This specification is not to be used for separate claims for flame resistance (“FR”), heat resistance, or protection against the transfer of thermal energy. Instead, clothing materials are required to be evaluated for the combination of flame and heat resistance tests.1.1.3 This specification does not include a test for establishing protection levels against specific hazards where clothing insulation is needed such as from flash fires, exposure to high-energy electrical arc, or extended duration fires. This specification does not replace and shall not be used in lieu of existing standards where well-defined criteria are established for protection of workers from known characterized intense thermal hazards such as flash fires (NFPA 2112), high-energy electrical arc (Specification F1506), or wildland firefighting (NFPA 1977). See Appendix X1 for a list of standards for heat and flame-resistant protective clothing.1.1.4 This specification includes requirements that define resistance to melting and combustion of materials used in personal protective clothing in a manner to limit the contribution of the clothing for causing injury to the wearer when exposed to low levels of heat or flame. The primary mechanisms by which a garment can contribute to injury are by the garment igniting and supporting combustion, and if the garment melts onto the wearer’s skin.1.1.5 This specification is applicable to all materials used in the construction of the protective clothing, including lining materials and materials that contact the skin or underclothing of the wearer. Exclusions are permitted for some materials such as labels and small components that do not come in contact with the wearer’s skin or underclothing.1.1.6 This specification does not include testing for the evaluation of the entire clothing item.1.1.7 This specification does not include procedures for testing of gloves or footwear.1.1.8 This specification is applicable to hoods, balaclavas, shrouds, neck gaiters, barrier face coverings, and other items of apparel that are primarily worn on the individual wearer’s head.1.2 This specification does not apply to protective clothing that is addressed in other standards for specific applications including electrical arc flash, flash fire, and various types of firefighting or emergency response. See Appendix X1 for a list of standards for heat and flame-resistant protective clothing.1.3 The values stated in SI units or in other units shall be regarded separately as standard. The values stated in each system must be used independently of the other, without combining values in any way.1.4 This standard measures and describes the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.1.5 The following precautionary caveat pertains only to the test methods portion, Section 8, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Measurements made by this test method are related to the night time brightness of retroreflective marking materials approximately facing the driver of a mid-sized automobile equipped with tungsten filament headlights at about 200 m distance.Retroreflective marking material used for pedestrian safety can degrade with time, exposure to sunlight, wear and cleaning, and the material requires periodic measurement to ensure that the performance of the retroreflective material provides adequate safety to the wearer.This test method is not intended to be used for the measurement of retroreflective marking material for pedestrian safety at observation and entrance angles other than those specified herein.5.3.1 For most materials, the values for the coefficient of retroreflection obtained at −4° entrance angle and 0.2° observation angle using this test method will be nearly the same as the values corresponding to +5° entrance angle and 0.2° observation angle, a geometry that is specified in some high-visibility clothing standards.1.1 This test method covers the measurement of the retroreflective properties of high visibility pedestrian garments, such as vests, using a portable retroreflectometer that can be used in the field. The portable retroreflectometer is a hand-held instrument with a defined standard geometry that can be placed in contact with retroreflective marking material to measure the retroreflection. The measurements can be compared to minimum requirements to determine the need for replacement of the retroreflective material.1.2 This test method is designed for measuring retroreflective marking materials that have an area equal to or greater than that of the aperture of the retroreflectometer.1.3 This test method is intended to be used for field measurement of retroreflective marking materials, but may be used to measure the performance of materials before placing the clothing in use.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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