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4.1 This technique is destructive, in that the glass fragments may need to be crushed, and digested in acid.4.2 Although the concentration ranges of the calibration curves shown in Appendix X1 are applicable to soda lime and borosilicate glass, this method is useful for the accurate measurement of element concentrations from a wide variety of glass samples.4.3 The determination of the element concentrations in glass yields data that can be used to compare fragments.4.4 It should be recognized that the method measures the bulk concentration of the target elements. Any extraneous material present on the glass that is not removed before digestion can result in inaccurate concentrations of the measured elements.4.5 The precision and accuracy of the method should be established in each laboratory that employs the method.1.1 One objective of a forensic glass examination is to compare glass samples to determine if they can be discriminated using their physical, optical or chemical properties (for example, color, refractive index (RI), density, elemental composition). If the samples are distinguishable in any of these observed and measured properties, it may be concluded that they did not originate from the same source of broken glass. If the samples are indistinguishable in all of these observed and measured properties, the possibility that they originated from the same source of glass cannot be eliminated. The use of an elemental analysis method such as inductively coupled plasma mass spectrometry yields high discrimination among sources of glass. (1-16)21.2 This test method covers a procedure for quantitative determination of the concentrations of magnesium (Mg), aluminum (Al), iron (Fe), titanium (Ti), manganese (Mn), rubidium (Rb), strontium (Sr), zirconium (Zr), barium (Ba), lanthanum (La), cerium (Ce), neodymium (Nd), samarium (Sm), and lead (Pb) in glass samples.1.3 This procedure is applicable to irregularly shaped samples as small as 200 micrograms, for the comparison of fragments of a known source to the recovered fragments from a questioned source. These elements are present in soda lime and borosilicate glass in μg/L to % levels.1.4 This procedure is applicable to other elements, other types of glass, and other concentration ranges with appropriate modifications of the digestion procedure (if needed for full recovery of the additional elements), calibration standards and the mass spectrometer conditions. Calcium and potassium, for example, could be added to the list of analytes in a modified analysis scheme. Alternative methods for the determination of concentrations of elements in glass are listed in the references.1.5 For any given glass, approximately 40 elements are likely to be present at detectable concentrations using this procedure with minor modifications. The element set stated here is an example of some of these elements that can be detected in glass and used for forensic comparisons.1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.7 This standard cannot replace knowledge, skills, or abilities acquired through education, training, and experience and is to be used in conjunction with professional judgment by individuals with such discipline-specific knowledge, skills, and abilities.1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The permissible level of heavy metals in certain coatings is specified by governmental regulatory agencies. This test method provides a fully documented procedure for determining low concentrations of mercury present in both water and solvent-reducible coatings to determine compliance.1.1 This test method covers the determination of the content of mercury in the range between 10 and 1000 ppm (mg/kg) present in liquid coatings, coatings vehicles, or in dried films obtained from previously coated substrates. There is no reason to believe that higher levels could not be determined by this test method, provided that appropriate dilutions and adjustments in specimen size and reagent quantities are made.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7 and 9.1.1.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The determination of endotoxin concentrations in MWF is a parameter that can be used in decision-making for prudent fluid management practices (fluid draining, cleaning, recharging, or biocide dosages).5.2 This standard provides a practice for analysts who perform quantitative endotoxin analyses of water-miscible MWF.1.1 This practice covers quantitative methods for the sampling and determination of bacterial endotoxin concentrations in water-miscible metalworking fluids (MWF).1.2 Users of this practice need to be familiar with the handling of MWF.1.3 This practice gives an estimate of the endotoxin concentration in the sampled MWF.1.4 This practice replaces Method E2250.1.5 This practice seeks to minimize interlaboratory variation of endotoxin data but does not ensure uniformity of results.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 Intended Use: 4.1.1 This guide may be used by various parties involved in sediment corrective action programs, including regulatory agencies, project sponsors, environmental consultants, toxicologists, risk assessors, site remediation professionals, environmental contractors, and other stakeholders.4.2 Updates to CSM: 4.2.1 The CSM should be updated as needed and refined to describe the physical properties, chemical composition and occurrence, biological features, and environmental conditions of the sediment corrective action project (Guide E1689).4.3 Reference Material: 4.3.1 This guide should be used in conjunction with other ASTM guides listed in 2.1 (especially Guides E3163, E3164, E3240, E3242, and E3344), as well as the material in the References section (including (1)).4.4 Flexible Site-Specific Implementation: 4.4.1 This guide provides a systematic but flexible framework to accommodate variations in approaches by regulatory agencies and by the user based on project objectives, site complexity, unique site features, regulatory requirements, newly developed guidance, newly published scientific research, changes in regulatory criteria, advances in scientific knowledge and technical capability, and unforeseen circumstances.4.5 Regulatory Frameworks: 4.5.1 This guide is intended to be applicable to a broad range of local, state, tribal, federal, or international jurisdictions, each with its own unique regulatory framework. As such, this guide does not provide a detailed discussion of the requirements or guidance associated with any of these regulatory frameworks, nor is it intended to supplant applicable regulations and guidance. The user of this guide will need to be aware of the regulatory requirements and guidance in the jurisdiction where the work is being performed.4.6 Systematic Project Planning and Scoping Process: 4.6.1 When applying this guide, the user should undertake a systematic project planning and scoping process to collect information to assist in making site-specific, user-defined decisions for a particular project, including assembling an experienced team of project professionals. These practitioners should have the appropriate expertise to scope, plan, and execute a sediment data acquisition and analysis program. This team may include, but is not limited to, project sponsors, environmental consultants, toxicologists, site remediation professionals, analytical chemists, geochemists, and statisticians.4.7 Other Considerations: 4.7.1 This guide does not provide a detailed description of all topics of a program to derive representative sediment background concentrations. It is meant to be used in conjunction with other guides (such as Guides E3163, E3164, E3240, E3242, and E3344) to do so.4.7.2 Sediment sampling and laboratory analyses are not covered in detail in this guide. Guides E3163 and E3164 contain extensive information concerning sediment sampling and laboratory analysis methodologies.4.7.3 Data quality objectives are not covered in this guide. Data quality objectives are described in (2).4.7.4 The selection of a background reference area(s) is not covered in detail in this guide but is extensively described in Guide E3344.4.7.5 Background study design considerations are not covered in detail in this guide, but are extensively described in other references, including Guide E3164 and (3).4.7.6 The use of data evaluation methodologies to obtain representative background data sets from candidate background data sets is not covered in detail in this guide but is discussed in more depth in Guide E3242.4.7.6.1 Identification and removal of high nondetect values from candidate background data sets are discussed in detail in Guide E3242.4.7.6.2 Identification and removal of outliers from candidate background data sets are discussed in detail in Practice E178, as well as Guide E3242.4.7.6.3 Geochemical methodologies used in evaluating candidate background data sets to obtain representative background data sets are discussed in detail in Guide E3242; their applications during reference-area selection are discussed in Guide E3344.4.7.6.4 Chemical forensics methodologies used in evaluating candidate background data sets to obtain representative background data sets are discussed in detail in Guide E3242; their applications during reference-area selection are discussed in Guide E3344.4.7.7 The use of statistical methods to calculate BTVs from representative background data sets and to compare such data sets to the site data sets are discussed in detail in Guide E3242.4.7.8 Geospatial analysis considerations are not thoroughly discussed in this guidance but are discussed in more depth relative to environmental evaluations in (4), which focuses on quality assurance concerns relative to geospatial analyses.4.7.9 In this guide, “sediment” (3.1.16) is defined as a matrix being found at the bottom of a water body. Upland soils of sedimentary origin are excluded from consideration as sediment in this guide.4.7.10 In this guide, only COC concentrations are considered. Residual background radioactivity is out of scope for this guide.4.8 Structure and Components of This Guide: The user of this guide should review the overall structure and components of this guide before proceeding with use, including:• Section 1 • Section 2 Referenced Documents• Section 3 Terminology• Section 4 • Section 5 Overview of Representative Background Concentrations• Section 6 Framework for Developing Representative Background Concentrations for Sediment Sites• Section 7 Conceptual Site Model Considerations When Developing Representative Background Concentrations for Sediment Sites• Section 8 Keywords• References  1.1 This guide provides an overarching framework for the development of representative sediment background concentrations at contaminated sediment sites. It is intended to inform, complement, and support but not supersede the guidelines established by local, state, tribal, federal, or international agencies.1.2 Technically defensible representative sediment background concentrations are critical for several purposes (Guide E3242) (1)2. These include sediment site delineation, establishing remedial goals, remedy selection, assessment of risks posed by representative background concentrations, and establishing appropriate post-remedial monitoring plans.1.3 As part of the overall framework presented in this guide, Guide E3240 provides a general discussion of how Conceptual Site Model (CSM) development fits into the risk-based corrective action framework for contaminated sediment sites. However, not all elements of a sediment CSM need to be considered when developing representative sediment background concentrations; those that do are discussed in detail in Section 7 of this guide.1.3.1 As additional data are collected and analyzed, the CSM should be updated as needed.1.3.2 This guide is related to several other guides. Guide E3344 describes how to select an appropriate background reference area(s). Guide E3164 covers the sampling methodologies used in the field to obtain sediment samples (whether from the sediment site or background reference area[s]), and Guide E3163 discusses appropriate laboratory methodologies to use for the chemical analysis of potential contaminants of concern (PCOCs) in sediment samples. Guide E3242 describes how to evaluate candidate background data to obtain representative background data sets (including statistical, geochemical, and forensic considerations) and then how to use them to calculate representative sediment background concentrations. Relevant content contained in Guides E3163, E3164, E3242, and E3344 is summarized herein, but the individual guides should be consulted for more detailed coverage of these topics.1.4 Representative sediment background concentrations are typically used in contaminated sediment corrective actions performed under various regulatory programs, including the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). Although many of the references cited in this guide are CERCLA oriented, the guide is applicable to corrective actions performed under local, state, tribal, federal, and international corrective action programs. However, this guide does not provide a detailed description of the requirements or existing background guidance for each jurisdiction.1.5 This guide would optimally be applied at the start of any sediment corrective action program but can be initiated at other points in the program as well.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method is applicable to organic solutions containing 20 to 2000 μg uranium per mL of solution presented to the spectrometer for the solution techniques or 200 to 50 000 μg uranium per g using the fused pellet technique.5.2 Either wavelength-dispersive or energy-dispersive XRF systems may be used, provided that the software accompanying the system is able to accommodate the use of internal standards.1.1 This test method covers the steps necessary for the preparation and analysis by X-ray fluorescence (XRF) of oils and organic solutions containing uranium. Two different preparation techniques are described.1.2 The procedure is valid for those solutions containing 20 to 2000 μg uranium per mL as presented to the spectrometer for the solution technique and 200 to 50 000 μg uranium per g for the pellet technique.1.3 This test method requires the use of an appropriate internal standard. Care must be taken to ascertain that samples analyzed by this test method do not contain the internal standard or that this contamination, whenever present, has been corrected for mathematically. Such corrections are not addressed in this procedure. Care must be taken that the internal standard and sample medium are compatible; that is, samples must be miscible with tri- n-butyl phosphate (TBP) and must not remove the internal standard from solution. Alternatively, a scatter line may be used as the internal standard.21.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9 and Note 2.

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