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5.1 Uranium and plutonium are used in nuclear reactor fuel and must be analyzed to insure that they meet certain criteria for isotopic composition as described in Specifications C833 and C1008. This practice is used to chemically separate the same mass peak interferences from uranium and plutonium and from other impurities prior to isotopic abundance determination by thermal ionization mass spectrometry.5.2 In those facilities where perchloric acid use is tolerated, the separation in Test Method C698 may be used prior to isotopic abundance determination. Uranium and plutonium concentrations as well as isotopic abundances using thermal ionization mass spectrometry can be determined using this separation and following Test Method C1625.1.1 This practice is for the ion exchange separation of uranium and plutonium from each other and from other impurities for subsequent isotopic analysis by thermal ionization mass spectrometry. Plutonium-238 and uranium-238, and plutonium-241 and americium-241, will appear as the same mass peak and must be chemically separated prior to analysis. Only high purity solutions can be analyzed reliably using thermal ionization mass spectrometry.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 This  practice  is  applicable  when  small amounts of 241Am are present in plutonium samples (see Test Methods C758 and C759). An example is the determination of 241Am in a 238Pu sample. The high specific activity of 238Pu presents a safety hazard that precludes its presence in a counting facility. Therefore, it is necessary to remove the 238Pu prior to the determination of 241Am. 4.2 When a plutonium solution contains fission or activation products, this practice does not separate all radionuclides that interfere in the determination of 241Am, such as the rare earths. 1.1 This practice describes the use of an ion exchange technique to separate plutonium from solutions containing low concentrations  of americium  prior  to measurement of the 241Am by gamma counting. 1.2 This practice covers the removal of plutonium, but not all the other radioactive isotopes that may interfere in the determination of 241Am. 1.3 This practice can be used when 241Am is to be determined in samples in which the plutonium is in the form of metal, oxide, or other solid provided that the solid is appropriately sampled and dissolved (See Test Methods C758, C759, and C1168). 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is for the quantitative determination of fluoride and glycol degradation products in engine coolants. By this method, analysis can be performed directly without pretreatment, other than dilution, as required by the linear ranges of the equipment. Table 1 indicates applicable analytes and approximate detection limits.(A) Sample diluted 1/10 with reagent water, suppressed conductivity detection, IonPac AS20 column with AG20 guard column. Other systems will require MQL determinations using chosen dilution factors, eluents, columns, and detector.1.1 This test method covers the determination of fluoride in engine coolants by ion chromatography. Several glycol degradation products (different carboxylates including, but not limited to, formate and glycolate) can be determined by this test method.1.2 This test method applies to both new and used engine coolants.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice can be used to evaluate unused oxygen removal ion exchange cartridges for conformance to specifications.5.2 This practice provides for the calculation of capacity in terms of the volume of water treated to an end point level of dissolved oxygen.5.3 The practice as written assumes that the oxygen removal ion exchange resins in the cartridge are either partially or fully regenerated. Regeneration of the resins is not part of this practice.5.4 This practice provides for the calculation of capacity on a cartridge basis.5.5 This practice may be used to test different size oxygen removal resin cartridges. The flow rate of test water and the frequency of sampling are varied to compensate for the approximate volume of resin in the test cartridge.1.1 This practice covers the determination of the performance of oxygen removal ion exchange resin cartridges in the regenerated form when used for removing dissolved oxygen from water. The test can be used to determine the initial capacity of unused cartridges or the remaining capacity of used cartridges. In this case, performance is defined as oxygen removal capacity (or throughput) to a defined endpoint.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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7.1 The particle size distribution of powdered ion exchange resins and, more importantly, the derived parameters of mean particle size and percent above and below specified size limits are useful for determining batch to batch variations and, in some cases, can be related to certain aspects of product performance.7.2 Although automatic multichannel particle size analyzers, of the type described in Section 9, yield information on the entire distribution of sizes present in a given sample, it has been found that, for this application, the numerical value of three derived parameters may adequately describe the particle size characteristics of the samples: the mean particle diameter (in micrometres), the percent of the sample that falls below some size limit, and the percent of the sample that falls above some size limit.1.1 These test methods cover the determination of the physical and chemical properties of powdered ion exchange resins and are intended for use in testing new materials. The following test methods are included:  SectionsTest Method A—Particle Size Distribution 5 to 15Test Method B—Solids Content 16 to 231.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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