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5.1 This practice is useful in identifying the major organic constituents in wastewater for support of effective in-plant or pollution control programs. Currently, the most practical means for tentatively identifying and measuring a range of volatile organic compounds is gas-liquid chromatography. Positive identification requires supplemental testing (for example, multiple columns, speciality detectors, spectroscopy, or a combination of these techniques).1.1 This practice covers general guidance applicable to certain test methods for the qualitative and quantitative determination of specific organic compounds, or classes of compounds, in water by direct aqueous injection gas chromatography (1, 2, 3, 4).21.2 Volatile organic compounds at aqueous concentrations greater than about 1 mg/L can generally be determined by direct aqueous injection gas chromatography.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method has the advantage of extreme simplicity. It is a crude and non-specific test method, but it is useful in the study of long-term trends. It requires very little investment in equipment and can be carried out without a large technically-skilled staff.5.2 This test method is useful for obtaining samples of settleable particulate matter for further chemical analysis (1).41.1 This test method covers a procedure for collection of dustfall and its measurement. This test method is not appropriate for determination of the dustfall rate in small areas affected by specific sources. This test method describes determination of both water-soluble and insoluble particulate matter.1.2 This test method is inappropriate for industrial hygiene use except where other more specific methods are also used.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is intended for use in quality control, material screening, and related problem solving where a nonvolatile content is desired or a comparison can be made with a known material of the same type.5.2 The parameters described may be altered to suit a particular analysis, provided the changes are noted in the report.1.1 This test method covers the determination of the non-volatile matter of agricultural tank mix adjuvant solutions by thermogravimetry.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This sampling procedure is used to collect a particulate filter sample containing particulates 0.2 µm or larger in size to be used to measure the size and concentration of particulates in a gaseous fuel stream.1.1 This practice is primarily for sampling particulates in gaseous fuels up to a nominal working pressure (NWP) of 70 MPa (10 152 psi) using an in-stream filter. This practice describes sampling apparatus design, operating procedures, and quality control procedures required to obtain the stated levels of precision and accuracy.1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Test Method D1770 for the determination of neps, vegetable matter, and colored fiber may be used for the acceptance testing of commercial shipments of wool top but caution is advised because the between-laboratory precision is known to be poor. Comparative tests as directed in 5.1.1 may be advisable. In case of a dispute arising from differences in reported test results when using Test Method D1770 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens that are as homogeneous as possible and that are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test for unpaired data and an acceptable probability level chosen by the two parties before the testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.1.1 This test method covers the determination of the number of neps and pieces of vegetable matter by size classes, and the number of colored fibers, in 15 g samples of wool top. 1.2 This test method is applicable to wool top in any form. Note 1—For the determination of number of neps per specified mass of cotton samples, refer to Test Method D1446. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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3.1 This test method describes the analytical measurement of residual matter in solvents that are intended to be 100 % volatile at 105 °C ± 5 °C. Volatile solvents are used in the manufacture of paint, varnish, lacquer, and other related products, and the presence of any residue may affect the product quality or efficiency of the process. This test method is useful in manufacturing control and assessing compliance with specifications.1.1 This test method covers the determination of the nonvolatile matter in volatile solvents for use in paint, varnish, lacquer, and related products.1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 For hazard information and guidance, see the supplier’s Material Safety Data Sheet for materials listed in this test method.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 5.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 The measurement of particulate matter is widely performed to characterize emissions from stationary sources in terms of emission concentrations and emission rates to the atmosphere for engineering and regulatory purposes.5.2 This test method provides near real-time measurement results and is particularly well suited for use in performance assessment and optimization of particulate matter controls achieved by air pollution control devices or process modifications (including fuel, feed, or process operational changes) and performance assessments of particulate matter continuous emissions monitoring systems (PM CEMS)5.3 This test method is well suited for measurement of particulate matter-laden gas streams in the range of 0.2 mg/m3 to 50 mg/m3, especially at low concentrations.5.4 The U.S. EPA has concurred that this test method has been demonstrated to meet the Method 301 bias3 and precision criteria for measuring particulate matter from coal fired utility boilers when compared with EPA Method 17 and Method 5 (40CFR60, Appendix A).5.5 This test method can accurately measure relative particulate matter concentrations over short intervals and can be used to assess the uniformity of particulate concentrations at various points on a measurement traverse within a duct or stack.1.1 This test method describes the procedures for determining the mass concentration of particulate matter in gaseous streams using an automated, in-stack test method. This test method, an in-situ, inertial microbalance, is based on inertial mass measurement using a hollow tube oscillator. This test method is describes the design of the apparatus, operating procedure, and the quality control procedures required to obtain the levels of precision and accuracy stated.1.2 This test method is suitable for collecting and measuring filterable particulate matter concentrations in the ranges 0.2 mg/m3 and above taken in effluent ducts and stacks.1.3 This test method may be used for calibration of automated monitoring systems (AMS). If the emission gas contains unstable, reactive, or semi-volatile substances, the measurement will depend on the filtration temperature, and this test method (and other in-stack methods) may be more applicable than out-stack methods for the calibration of automated monitoring systems.1.4 This test method can be employed in sources having gas temperature up to 200°C (392°F) and having gas velocities from 3 to 27 m/s.1.5 This test method includes a description of equipment and methods to be used for obtaining and analyzing samples and a description of the procedure used for calculating the results.1.6 This test method may also be limited from use in sampling gas streams that contain fluoride, or other reactive species having the potential to react with or within the sample train.1.7 Appendix X1 provides procedures for assessment of the spatial variation in particulate matter (PM) concentration within the cross section of a stack or duct test location to determine whether a particular sampling point or limited number of sampling points can be used to acquire representative PM samples.1.8 Appendix X2 provides procedures for reducing the sampling time required to perform calibrations of automated monitoring systems where representative PM samples can be acquired from a single sample point and certain other conditions are met.1.9 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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1.1 This test method is applicable for the determination of particulate matter emissions from solid-fuel-burning appliances including woodstoves, pellet-burning appliances, factory-built fireplaces, masonry fireplaces, masonry heaters, indoor furnaces, and indoor and outdoor hydronic heaters within a laboratory environment.1.2 Analytes will be a particulate matter (PM) with no CAS number assigned. For data quality objectives, see Appendix X1.1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.4 This test method does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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3.1 These test methods are mainly intended for referee purposes but can also be used for quality control of rubber production.3.2 The amount of volatiles can affect processing and cure characteristics of compounded rubber.1.1 These test methods cover a hot mill method, two oven methods, and a press method for the determination of moisture and other volatile matter content in synthetic rubber.1.2 Either oven method shall be used especially when the rubber is too tacky to be handled satisfactorily on a hot mill.1.3 The press method shall be used for rubbers that are too crumbly to be retained satisfactorily on a laboratory mill.1.4 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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