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3.1 Low temperatures are often needed for conditioning of rubber prior to testing, as well as during the test. Conditioning is required to attain a specific temperature that is uniform throughout the specimen or for producing time-dependent effects. Specimens may be conditioned and tested in the same or different chambers.3.2 This practice is intended to apply particularly, but not exclusively, to the following ASTM Standards: Test Methods D746, D945, D1053, D1229, D1329, D1415, D2136, D2137, D2240, D2632, Practice D832, and Specification E197.1.1 This practice covers the general requirements for achieving and maintaining temperatures below 21°C for thermal conditioning and physical testing of rubber.1.2 This practice describes the acceptable types and construction of low-temperature cabinets for conditioning and testing of rubber, the composition and circulation of heat-transfer media, and the required uniformity and precision of temperature control.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Differential scanning calorimetry and differential thermal analysis provide a rapid method for determining the fusion and crystallization temperatures of crystalline materials.5.2 This test is useful for quality control, specification acceptance, and research.1.1 This test method describes the determination of melting (and crystallization) temperatures of pure materials by differential scanning calorimetry (DSC) and differential thermal analysis (DTA).1.2 This test method is generally applicable to thermally stable materials with well-defined melting temperatures.1.3 The normal operating range is from −120 to 600°C for DSC and 25 to 1500°C for DTA. The temperature range can be extended depending upon the instrumentation used.1.4 Computer or electronic based instruments, techniques, or data treatment equivalent to those in this test method may be used.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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4.1 The compressive strength or crush-extrusion resistance of a gasket material is a major factor with regard to the selection of a given material for use in a particular sealing application. The significance of the test method is based, in part, on the assumption that a material, once it has been crushed or extruded, will no longer function as effectively as a seal. This assumption can only be used as a guide, however, since exact yield or failure points are difficult to define for gasket materials (which are usually viscoelastic in nature). Two or more materials can be compared to determine differences in their resistance to compressive stress. A sample of material can be compared to an established standard or previously determined characteristics on original lots of the same material, for quality assurance purposes. See 6.2 for discussion of specimen area and geometry effects.1.1 This test method covers the determination of compressive strength characteristics (crush-extrusion resistance) of gasket materials at elevated temperature.1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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