5.1 Building products made with caulks and sealants are often used for applications for which Test Method E84 is used for compliance with building code, life safety code or mechanical code requirements. This practice describes, in detail, specimen mounting procedures for those caulks and sealants which are not able to be supported by their own structural characteristics during the test.5.2 Codes are often silent with regard to testing caulks and sealants for the assessment of flame spread index and smoke developed index as surface burning characteristics. This practice describes specimen preparation and mounting procedures for such materials and products.5.3 The material shall be representative of the materials used in actual field installations.5.4 The limitations for this procedure are those associated with Test Method E84.1.1 This practice describes procedures for specimen preparation and mounting when testing caulks and sealants to assess flame spread and smoke development as surface burning characteristics using Test Method E84.1.1.1 Caulks and sealants up to 8 in. (203.2 mm) in width shall follow the requirements of 7.1.1.1.2 Caulks and sealants in excess of 8 in. (203.2 mm) in width shall follow the requirements of 7.2.1.1.2.1 Caulks and sealants in excess of 8 in. (203.2 mm) in width can be considered coatings.1.2 This practice applies to caulks and sealants intended for various uses within buildings. The caulks and sealants addressed in this practice are not able to be supported by their own structural characteristics during the test.1.2.1 This practice does not apply to adhesives that are used to adhere or bind together surfaces. Annex A12 of Test Method E84 provides a procedure for testing adhesives.1.3 Testing is conducted in accordance with Test Method E84.1.4 This practice does not provide pass/fail criteria that can be used as a regulatory tool.1.5 This practice does not apply to materials for which the test specimen does not remain in place before and during the test until maximum flame propagation has occurred.1.6 This practice is not for system evaluation. It is for the comparison of the materials only.1.7 The results obtained by using this mounting procedure are confined to the materials themselves as tested and are not comparable to those obtained with materials that are tested in a full tunnel width application.1.8 This fire standard cannot be used to provide quantitative measures.1.9 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.1.10 This standard gives instructions on specimen preparation and mounting, but the fire-test-response method is given in Test Method E84. See also Section 9.1.11 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes shall not be considered requirements of the standard.1.12 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.13 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.14 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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1.1 This guide covers the test method selection and associated test specimen design to produce test data to be used for typical bolted joint analyses. These test methods are limited to use with multi-directional polymer matrix composite laminates reinforced by high-modulus fibers. This standard is intended to be used by persons requesting these test types.1.2 Test requestors designing these specimens need to be familiar with the referenced Test Method and Practice standards, CMH-17 Volume 3 Chapter 11, and the stress analysis methods that will use the resulting design data.1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.1.3.1 Within the text the inch-pound units are shown in brackets.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 Under the severe conditions of this test method, the specimens undergo degradation at a rate that is dependent upon the thermal endurance of the polypropylene material under examination.5.2 The thermal level of this test method is considered sufficiently severe to cause failure of commercial grades of heat-stable polypropylene within a reasonable period of time. If desired, lower temperatures can be applied to estimate the performance of polypropylene materials with lower heat stability.5.3 The technique of specimen rotation described in this test method provides an estimate of the life-temperature relationship of polypropylene. If this test method is conducted at different temperatures on the same material, a more reliable estimate of the life-temperature relationship of polypropylene is determined. This test method can be conducted at several temperatures and the data interpreted through use of the Arrhenius relation, by plotting the logarithms of times to failure against the reciprocals of the temperatures in kelvins (K). Temperatures in the range from 100 to 150°C, with intervals of 10°C, are suggested for this purpose.5.4 The stability as determined under the prescribed test method is not directly related to the suitability of the compound for a use where different conditions prevail.5.5 The specimen rotation technique of thermal aging increases the probability that all specimens will be exposed similarly and that the effect of temperature gradients in an oven will be minimized.1.1 This test method provides a means for estimating the resistance of polypropylene, in molded form, to accelerated aging by heat in the presence of air using a forced draft oven.1.2 The stability determined by this test method is not directly related to the suitability of the material for use when different environmental conditions prevail and shall not be used to predict performance.NOTE 1: The specified thermal levels in this test method are considered sufficiently severe to cause failure of commercial grades of heat-stable polypropylene within a reasonable period of time. If desired, lower temperatures can be applied to estimate the performance of polypropylene with lower heat stabilities.1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.NOTE 2: This test method and ISO 4577–1983 are technically similar but different in preparation of test specimens, thickness of test specimen, measurement of the number of air flow changes in the ovens, and the number of air changes per hour required.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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4.1 Single-lap specimens are economical, practical, and easy to make. They are the most widely used specimens for development, evaluation, and comparative studies involving adhesives and bonded products, including manufacturing quality control.4.2 Special specimens and test methods have been developed that yield accurate estimates of the true shear strength of adhesives. These methods eliminate or minimize many of the deficiencies of the thin-adherend single-lap specimens, but are more difficult to make and test. (See Test Methods D3983, D4027, D4562, and E229.)4.3 The misuse of strength values obtained from such Test Methods or Practices as D906, D1002, D1144, D1151, D1183, D1780, D2294, D2295, D2339, D3163, D3164, D3165, D3434, D3528, D3632, and D5868, as allowable design-stress values for structural joints could lead to product failure, property damage, and human injury.1.1 This guide is directed toward the safe and appropriate use of strength values obtained from test methods using single-lap adhesive joint specimens.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 The discussion focuses on shear strength as measured with small thin-adherend, single-lap specimens. Many factors, however, apply to shear modulus, tensile strength, and tensile modulus measured by small laboratory specimens in general. This discussion is limited to single-lap specimens and shear strength only for simplification.
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5.1 Pipe and duct insulation systems are often evaluated with Test Method E84 to comply with building or mechanical code requirements. This practice describes, in detail, specimen preparation and mounting procedures for single-component pipe or duct insulation systems and for multi-component pipe or duct insulation systems.5.2 The material, system, composite, or assembly tested shall be representative of the completed insulation system used in actual field installations, in terms of the components, including their respective thicknesses.5.3 Pipe and duct insulation systems consist of a variety of materials and constructions.5.4 Some testing laboratories have developed a number of protocols for testing pipe or duct insulation systems which utilize one generic type of materials, all of them with an insulation core and a jacket. Those protocols are the origin of this practice, which makes them generic, to reduce material bias in the standard; they have resulted in the procedures presented in 6.1. The procedures presented in 6.2 – 6.5 address other types of pipe or duct insulation systems.5.5 This practice addresses specimen preparation and mounting of systems of the types described in 5.5.1 – 5.5.3 and testing of supplementary materials as described in 5.6.5.5.1 Multi-component systems containing an insulation core and a jacket, with or without adhesive between insulation core and jacket, not intended to be bonded to a pipe or duct substrate. Specimen preparation and mounting for such systems is described in 6.1 if they are self-supporting and in 6.2 if they are not self-supporting.5.5.2 Single component systems, not intended to be bonded to a pipe or duct substrate. Specimen preparation and mounting for such systems is described in 6.3 if they are self-supporting and in 6.4 if they are not self-supporting.5.5.3 Systems intended to be bonded to a pipe or duct substrate. Specimen preparation and mounting for such systems is described in 6.5.5.5.4 Reflective insulation materials (see 3.2.10 and 3.2.11) intended to be used as pipe or duct insulation materials and installed with an air gap shall be tested using the procedures for specimen preparation and mounting procedures described in Practice E2599. Reflective insulation materials intended to be used as pipe or duct insulation materials and installed without an air gap shall be tested using the specimen preparation and mounting procedures described in Section 6 of this practice.5.5.5 Specimen preparation and mounting procedures for systems not described in this practice shall be added as the information becomes available.5.6 Supplementary Materials: 5.6.1 It is recognized that supplementary materials for pipe or duct insulation systems are normally able to generate heat, flame or smoke. Thus, the fire safety of the entire system depends, at least to some extent, on the fire performance of supplementary materials. Consequently, the fire-test-response characteristics of all supplementary materials shall be assessed to obtain a full assessment of the fire-test-response of the pipe or duct insulation system. See Appendix X1.5.6.2 Supplementary materials are often present intermittently spaced, and not for an extended length, in a pipe or duct insulation system. Thus, it is not always possible to suitably test them in conjunction with a pipe or duct insulation system.5.6.3 Testing of Supplementary Materials—Supplementary materials that have not been fully tested in conjunction with the pipe or duct insulation system, in accordance with Section 6, shall be tested for flame spread and smoke development as single-component systems, in accordance with Test Method E84.5.7 The limitations for this procedure are those associated with Test Method E84.1.1 This practice describes procedures for specimen preparation and mounting when testing pipe and duct insulation materials to assess flame spread and smoke development as surface burning characteristics using Test Method E84.1.2 If the pipe or duct insulation materials to be tested are reflective insulation materials (see 3.2.10 and 3.2.11), the materials shall be tested using the procedures for specimen preparation and mounting described in Practice E2599 and not the procedures described in 6.1 through 6.6.1.3 Testing is conducted with Test Method E84.1.4 This practice does not provide pass/fail criteria that can be used as a regulatory tool.1.5 Use the values stated in inch-pound units as the standard, in referee decisions. The values in the SI system of units are given in parentheses, for information only; see IEEE/ASTM SI-10 for further details.1.6 This fire standard cannot be used to provide quantitative measures.1.7 Fire testing of products and materials is inherently hazardous, and adequate safeguards for personnel and property shall be employed in conducting these tests. Fire testing involves hazardous materials, operations, and equipment. This standard gives instructions on specimen preparation and mounting, but the fire-test-response method is given in Test Method E84. See also Section 8.1.8 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered requirements of the standard.1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This practice provides a standard method of testing damaged composite laminates which are too thin to be tested using typical anti-buckling fixtures, such as those used in Test Method D7137/D7137M. The laminate is first impacted or indented in order to produce a damage state representative of actual monolithic solid laminate structure. Impacting or static indentation is not performed on an assembled sandwich panel, as the damage state is altered by energy absorption in the core and by support of the core during the impact or indentation event. After damaging, the laminate is bonded onto the core with the impacted or indentation side of the laminate against the core, and with a localized un-bonded area encompassing the damage site. Fig. 1 illustrates the adhesive removal to avoid the damaged area and the assembly of the sandwich specimen with the impacted damaged laminate flipped over from the impacting or indentation orientation. The final assembled sandwich specimen is then tested using a long beam flexure setup with the damaged laminate being on the compression side. The sandwich panel configuration is used as a form of anti-buckling support for the thin damaged laminate.5.2 Susceptibility to damage from concentrated out-of-plane forces is one of the major design concerns of many structures made of advanced composite laminates. Knowledge of the damage resistance and damage tolerance properties of a laminated composite plate is useful for product development and material selection.5.3 The residual strength data obtained using this test method is used in research and development activities as well as for design allowables; however the results are specific to the geometry and physical conditions tested and are generally not scalable to other configurations.5.4 The properties obtained using this test method can provide guidance in regard to the anticipated damage tolerance capability of composite structures of similar material, thickness, stacking sequence, and so forth. However, it must be understood that the damage tolerance of a composite structure is highly dependent upon several factors including geometry, stiffness, support conditions, and so forth. Significant differences in the relationships between the existent damage state and the residual compressive strength can result due to differences in these parameters. For example, residual strength and stiffness properties obtained using this test method would more likely reflect the damage tolerance characteristics of an un-stiffened monolithic skin or web than that of a skin attached to substructure which resists out-of-plane deformation.5.5 The reporting section requires items that tend to influence residual compressive strength to be reported; these include the following: material, methods of material fabrication, accuracy of lay-up orientation, laminate stacking sequence and overall thickness, specimen geometry, specimen preparation, specimen conditioning, environment of testing, void content, volume percent reinforcement, type, size and location of damage (including method of non-destructive inspection (NDI)), fixture geometry, time at temperature, and speed of testing.5.6 Properties that result from the residual strength assessment include the following: compressive residual strength FCAI.1.1 This practice covers an approach for compressive testing thin damaged multidirectional polymer matrix composite laminates reinforced by high-modulus fibers using a sandwich long beam flexure specimen. It provides a test configuration in which the core does not constrain any protruding back side damage. It is limited to testing of monolithic solid laminates which are too thin to be tested using typical anti-buckling fixtures. It does not cover compressive testing of damaged sandwich panel facings. The composite material forms are limited to continuous-fiber or discontinuous-fiber (tape or fabric, or both) reinforced composites in which the laminate is balanced and symmetric with respect to the test direction1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.1.2.1 Within the text the inch-pound units are shown in brackets.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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4.1 It has been shown that bending stresses that inadvertently occur due to misalignment between the applied force and the specimen axes during the application of tensile and compressive forces can affect the test results. In recognition of this effect, some test methods include a statement limiting the misalignment that is permitted. The purpose of this practice is to provide a reference for test methods and practices that require the application of tensile or compressive forces under conditions where alignment is important. The objective is to implement the use of common terminology and methods for verification of alignment of testing machines, associated components and test specimens.4.2 Alignment verification intervals when required are specified in the methods or practices that require the alignment verification. Certain types of testing can provide an indication of the current alignment condition of a testing frame with each specimen tested. If a test method requires alignment verification, the frequency of the alignment verification should capture all the considerations that is, time interval, changes to the testing frame and when applicable, current indicators of the alignment condition through test results.4.3 Whether or not to improve axiality should be a matter of negotiation between the interested parties.1.1 Included in this practice are methods covering the determination of the amount of bending that occurs during the application of tensile and compressive forces to notched and unnotched test specimens during routine testing in the elastic range. These methods are particularly applicable to the force levels normally used for tension testing, compression testing, creep testing, and uniaxial fatigue testing. The principal objective of this practice is to assess the amount of bending exerted upon a test specimen by the ordinary components assembled into a materials testing machine, during routine tests.1.2 This practice is valid for metallic and nonmetallic testing.1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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5.1 This method provides a simple means of characterizing the cure behavior of a thermosetting resin specimen that is a representation of a composite part. The diameter of the specimen is approximately 38 mm and the thickness ranges from 2.6 mm to 3.2 mm. This corresponds to a sample volume of approximately 3 cm3 to 4 cm3. The data may be used for quality control, research and development, and verifying the cure within processing equipment including autoclaves.5.2 Dynamic mechanical testing provides a sensitive method for determining cure characteristics by measuring the elastic and loss moduli as a function of temperature or time, or both. Plots of cure behavior and tan delta of a material provide graphical representation indicative of cure behavior under a specified time-temperature profile. The presence of fibers within the resin may change the dynamic properties measured within a material. However, it is still possible to compare different resins with the same fiber structure and obtain the relative difference due to the resin cure properties.5.3 This method can be used to assess the following:5.3.1 Cure behavior, as well as changes as a function of temperature or time, or both,5.3.2 Processing behavior, as well as changes as a function of temperature or time, or both,5.3.3 The effects of processing treatments,5.3.4 Relative resin behavioral properties, including cure behavior, damping and impact resistance,5.3.5 The effects of reinforcement on cure; the reinforcement can be a fiber or a filler,5.3.6 The effects of materials used to bond the resin and reinforcement,5.3.7 The effect of formulation additives that might affect processability or performance.5.4 This provides a method to assess the cure properties of a thermosetting resin containing woven fiber or other reinforcing materials.5.5 This method is valid for a wide range of oscillation frequencies typically from 0.002 Hz to 50 Hz.NOTE 1: It is recommended that low-frequency test conditions, generally 1 Hz to 2 Hz, be used to generate more definitive cure-behavior information. Slower frequencies will miss important cure properties. Faster frequencies will reduce sensitivity to cure.1.1 This method covers the use of dynamic mechanical instrumentation for determination and reporting of the thermal advancement of cure behavior of thermosetting resin on an inert filler or fiber in a laboratory. It may also be used for determining the cure properties of resins without fillers or fibers. These encapsulated specimens are deformed in torsional shear using dynamic mechanical methods.1.2 This method is intended to provide means for determining the cure behavior of thermosetting resins on fibers over a range of temperatures from room temperature to 250 °C by forced-constant amplitude techniques (in accordance with Practice D4065). Plots of complex modulus, complex viscosity, and damping ratio or tan delta as a function of time or temperature, or both, quantify the thermal advancement or cure characteristics of a resin or a resin on filler or fiber.1.3 Test data obtained by this method is relevant and appropriate for optimizing cure cycles.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4.1 Exception—The Fahrenheit temperature measurement in 10.1 is provided for information only and is not considered standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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