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1.1 This test method covers the optical emission spectrometric analysis of stainless Type 18-8 steels for the following elements: Element Concentration Range, % Chromium 17.0 to 20.0 Nickel 8.0 to 15.0 Manganese 0.8 to 2.0 Silicon 0.4 to 0.8 Copper 0.1 to 0.2 1.2 This test method is designed for routine analysis of chill-cast disks or inspection testing of stainless Type 18-8 steel flats upon which a surface of at least 13-mm (1/2-in.) diameter may be prepared. The samples must be sufficiently massive to prevent overheating during the discharge and of similar metallurgical condition and composition as the standards used. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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5.1 This test method is based upon the stereological principle that a grid with a number of regularly arrayed points, when systematically placed over an image of a two-dimensional section through the microstructure, can provide, after a representative number of placements on different fields, an unbiased statistical estimation of the volume fraction of an identifiable constituent or phase (1, 2, 3).35.2 This test method has been described (4) as being superior to other manual methods with regard to effort, bias, and simplicity.5.3 Any number of clearly distinguishable constituents or phases within a microstructure (or macrostructure) can be counted using the method. Thus, the method can be applied to any type of solid material from which adequate two-dimensional sections can be prepared and observed.5.4 A condensed step-by-step guide for using the method is given in Annex A1.1.1 This test method describes a systematic manual point counting procedure for statistically estimating the volume fraction of an identifiable constituent or phase from sections through the microstructure by means of a point grid.1.2 The use of automatic image analysis to determine the volume fraction of constituents is described in Practice E1245.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 Pitch does not go through a solid-liquid phase change when heated, and therefore it does not have a true melting point. As the temperature rises, pitch softens and becomes less viscous. The softening point is arbitrarily defined and shall be established by a closely controlled method which shall be carefully followed if test results are to be reproducible.5.2 This test is useful in determining the consistency of pitch as one element in establishing the uniformity of shipments or sources of supply.1.1 This test method covers the determination of the softening point of pitches below 176 °F (80 °C). Pitches of higher softening point should be tested by Test Method D2319 or Test Method D3104.1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D97-17b(2022) Standard Test Method for Pour Point of Petroleum Products Active 发布日期 :  1970-01-01 实施日期 : 

5.1 The pour point of a petroleum specimen is an index of the lowest temperature of its utility for certain applications.1.1 This test method covers and is intended for use on any petroleum product.3 A procedure suitable for black specimens, cylinder stock, and nondistillate fuel oil is described in 8.8. The cloud point procedure formerly part of this test method now appears as Test Method D2500.1.2 Currently there is no ASTM test method for automated Test Method D97 pour point measurements.1.3 Several ASTM test methods offering alternative procedures for determining pour points using automatic apparatus are available. None of them share the same designation number as Test Method D97. When an automatic instrument is used, the ASTM test method designation number specific to the technique shall be reported with the results. A procedure for testing the pour point of crude oils is described in Test Method D5853.1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is adequate for use with other ASTM standards that specify the ice point as a reference. It is also intended to be adequate for most other ice-point reference purposes.5.2 The ice point is a common practical industrial reference point of thermometry. The ice point is relatively simple to realize and provides a readily available natural fixed-point reference temperature.5.3 Use in Resistance Thermometry: 5.3.1 The ice point was a defining fixed point on practical temperature scales prior to 1960.5.3.2 The ITS-90 defines W(T90) = R(T90)/R(273.16 K), the measured resistance ratio of a Standard Platinum Resistance Thermometer (SPRT), in reference to the water triple point, not the ice point (1).3 In many instances, where the water triple point is not available, or when the accuracy obtainable with the water triple point is not required, reference to a properly established and maintained ice-point reference is used. For industrial-quality resistance thermometers, the resistance value is determined for 0 °C, and an uncertainty that is appropriate for the quality of the ice-point realization is assigned.5.4 Use in Thermoelectric Thermometry: 5.4.1 In thermoelectric thermometry, the ice point is ordinarily used as the reference temperature (2).5.4.2 Adequate thermoelectric reference requires that thermocouple junctions be well-coupled thermally to the bath, electrically isolated from each other and from the bath, and adequately immersed to avoid perturbing the reference-junction temperatures by radiation and longitudinal conduction of heat along the thermoelements (3 and 4).5.5 Use in Liquid-in-Glass Thermometry: 5.5.1 In liquid-in-glass thermometry, the ice point is ordinarily used as the reference temperature (5).5.5.2 The periodic recalibration of a liquid-in-glass thermometer at the ice point provides a reliable indication of the effect of gradual relaxation of residual mechanical strains in the glass that have a significant effect on the volume of the bulb (5).1.1 This practice covers a method of preparing, maintaining, and using a temperature reference bath of a mixture of shaved ice and water, saturated with air at a pressure of 101 325 Pa (1 atm).1.2 An industrial practice for relating values referenced to the ice point and to the water triple point on the ITS-90 is included.1.3 Methods to promote uniformity of bath temperature by mechanical stirring or agitation are not described in detail.1.4 Methods of approximating the ice point, as by thermostatically-controlled refrigeration, are not covered by this practice.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3117-03 Standard Test Method for Wax Appearance Point of Distillate Fuels (Withdrawn 2010) Withdrawn, No replacement 发布日期 :  1970-01-01 实施日期 : 

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5.1 This test method is intended for determining the breaking strength and modulus of rupture of ceramic tiles and glass tiles for compliance with requirements that may appear in specifications.1.1 This test method covers the determination of breaking strength and modulus of rupture of ceramic tiles and glass tiles by three-point loading.1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method determines methane (nC1) to hexane (nC6), cut point carbon fraction intervals to nC24 and recovery (nC24+) of live crude oils and condensates without depressurizing, thereby avoiding the loss of highly volatile components and maintaining sample integrity. This test method provides a highly resolved light end profile which can aid in determining and improving appropriate safety measures and product custody transport procedures. Decisions in regards to marketing, scheduling, and processing of crude oils may rely on light end compositional results.5.2 Equation of state calculations can be applied to variables provided by this method to allow for additional sample characterization.1.1 This test method covers the determination of light hydrocarbons and cut point intervals by gas chromatography in live crude oils and condensates with VPCR4 (see Note 1) up to 500 kPa at 37.8 °C.NOTE 1: As described in Test Method D6377.1.2 Methane (C1) to hexane (nC6) and benzene are speciated and quantitated. Samples containing mass fractions of up to 0.5 % methane, 2.0 % ethane, 10 % propane, or 15 % isobutane may be analyzed. A mass fraction with a lower limit of 0.001 % exists for these compounds.1.3 This test method may be used for the determination of cut point carbon fraction intervals (see 3.2.1) of live crude oils and condensates from initial boiling point (IBP) to 391 °C (nC24). The nC24 plus fraction is reported.1.4 Dead oils or condensates sampled in accordance with 12.1 may also be analyzed.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5.1 Exception—Where there is no direct SI equivalent such as tubing size.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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